Pb4.32Sb3.68S8.68Cl2.32 Kostov-Kytin V V, Petrova R, Macicek J European Journal of Mineralogy 9 (1997) 1191-1197 Crystal structure of synthetic Pb4.32Sb3.68S8.68Cl2.32 A chlorine-bearing alternative to Pb4Sb4S11 _database_code_amcsd 0006706 CELL PARAMETERS: 15.0400 15.5100 4.0900 90.000 90.000 90.000 SPACE GROUP: Pbam X-RAY WAVELENGTH: 1.541838 Cell Volume: 954.076 Density (g/cm3): 5.930 MAX. ABS. INTENSITY / VOLUME**2: 64.78828337 RIR: 3.558 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.77 4.12 7.5200 2 0 0 2 13.08 28.06 6.7666 2 1 0 4 20.85 21.51 4.2603 2 3 0 4 21.10 37.19 4.2102 3 2 0 4 21.73 11.35 4.0900 0 0 1 2 22.94 5.01 3.8775 0 4 0 2 23.26 48.68 3.8248 1 1 1 8 23.70 65.60 3.7547 1 4 0 4 24.36 3.85 3.6542 4 1 0 4 24.74 2.44 3.5991 3 3 0 4 24.78 48.55 3.5930 2 0 1 4 25.32 2.43 3.5174 1 2 1 8 25.45 4.68 3.5003 2 1 1 8 25.85 8.91 3.4463 2 4 0 4 26.34 100.00 3.3833 4 2 0 4 27.36 40.09 3.2601 2 2 1 8 28.45 4.91 3.1371 1 3 1 8 28.75 28.75 3.1050 3 1 1 8 29.37 1.17 3.0408 4 3 0 4 29.40 5.92 3.0381 1 5 0 4 30.27 1.80 2.9530 5 1 0 4 30.29 30.40 2.9504 2 3 1 8 30.47 14.71 2.9336 3 2 1 8 31.19 6.35 2.8676 2 5 0 4 31.80 39.88 2.8139 0 4 1 4 31.91 32.26 2.8044 5 2 0 4 32.37 69.37 2.7659 1 4 1 8 33.16 40.47 2.7019 3 3 1 8 33.99 1.82 2.6379 3 5 0 4 34.02 4.04 2.6355 2 4 1 8 34.40 2.48 2.6070 4 2 1 8 34.50 6.48 2.6000 5 3 0 4 36.30 1.19 2.4746 6 1 0 4 36.62 2.11 2.4538 3 4 1 8 36.76 7.19 2.4446 2 6 0 4 36.85 1.57 2.4388 1 5 1 8 37.57 15.19 2.3942 5 1 1 8 38.34 13.97 2.3480 2 5 1 8 38.94 30.14 2.3129 5 2 1 8 39.21 11.79 2.2976 3 6 0 4 39.97 2.29 2.2555 6 3 0 4 40.70 4.32 2.2168 3 5 1 8 41.14 2.10 2.1942 5 3 1 8 41.77 2.70 2.1624 1 6 1 8 42.29 12.89 2.1372 6 0 1 4 42.43 4.67 2.1301 4 6 0 4 42.47 1.92 2.1282 7 1 0 4 42.96 2.06 2.1051 6 4 0 4 43.11 1.82 2.0984 2 6 1 8 43.94 10.29 2.0604 6 2 1 8 44.29 29.76 2.0450 0 0 2 2 44.72 9.85 2.0266 3 7 0 4 45.27 3.32 2.0031 3 6 1 8 45.95 13.91 1.9751 6 3 1 8 46.31 3.01 1.9605 5 6 0 4 46.38 1.93 1.9576 2 1 2 8 46.58 1.63 1.9497 6 5 0 4 46.86 2.88 1.9388 0 8 0 2 47.03 4.36 1.9321 1 7 1 8 47.64 1.73 1.9089 4 7 0 4 48.16 32.50 1.8893 4 6 1 8 48.20 9.99 1.8879 7 1 1 8 48.42 9.13 1.8800 8 0 0 2 48.44 8.90 1.8793 7 4 0 4 48.49 4.98 1.8774 2 8 0 4 48.65 1.19 1.8717 6 4 1 8 49.44 3.43 1.8436 2 3 2 8 49.55 6.32 1.8395 3 2 2 8 50.73 3.51 1.7995 6 6 0 4 50.84 12.57 1.7959 1 4 2 8 51.21 4.56 1.7840 5 7 0 4 51.71 1.72 1.7679 5 6 1 8 51.96 4.54 1.7599 6 5 1 8 52.00 1.49 1.7587 2 4 2 8 52.21 10.30 1.7519 0 8 1 4 52.27 19.58 1.7501 4 2 2 8 52.59 1.23 1.7401 1 8 1 8 52.93 1.19 1.7298 4 7 1 8 53.52 2.81 1.7121 1 9 0 4 53.67 3.97 1.7077 7 4 1 8 54.01 1.06 1.6979 8 1 1 8 54.06 1.37 1.6965 1 5 2 8 54.22 1.81 1.6917 8 4 0 4 54.64 3.40 1.6798 2 9 0 4 55.16 1.99 1.6650 2 5 2 8 55.62 9.34 1.6523 5 2 2 8 57.32 1.69 1.6074 5 3 2 8 58.88 2.56 1.5685 2 6 2 8 59.10 1.91 1.5632 8 4 1 8 60.31 3.25 1.5347 9 4 0 4 60.36 1.15 1.5336 6 8 0 4 60.62 4.46 1.5276 3 6 2 8 61.18 1.11 1.5150 6 3 2 8 61.22 1.79 1.5140 3 9 1 8 62.70 1.23 1.4817 3 10 0 4 63.01 2.61 1.4752 4 6 2 8 63.04 1.01 1.4746 7 1 2 8 63.20 2.49 1.4712 9 5 0 4 64.57 1.91 1.4432 7 7 1 8 64.76 4.12 1.4395 3 7 2 8 64.90 5.99 1.4368 9 4 1 8 64.94 1.16 1.4360 6 8 1 8 66.01 1.51 1.4152 5 6 2 8 66.20 1.82 1.4116 10 0 1 4 66.45 1.73 1.4070 0 8 2 4 66.51 2.28 1.4058 10 1 1 8 67.20 5.36 1.3931 3 10 1 8 67.60 1.14 1.3858 2 11 0 4 67.70 4.42 1.3840 8 0 2 4 67.71 4.66 1.3838 7 4 2 8 67.76 2.56 1.3830 2 8 2 8 68.01 1.33 1.3785 5 10 0 4 68.96 1.07 1.3617 10 3 1 8 69.47 1.56 1.3531 4 10 1 8 69.59 1.85 1.3510 6 6 2 8 69.67 1.30 1.3497 8 8 0 4 69.85 1.16 1.3465 11 2 0 4 69.98 2.25 1.3443 5 7 2 8 70.15 1.19 1.3415 2 0 3 4 71.35 1.16 1.3218 2 2 3 8 71.92 1.40 1.3128 1 9 2 8 72.33 3.79 1.3063 5 10 1 8 72.84 1.22 1.2985 2 3 3 8 72.87 1.92 1.2980 2 9 2 8 73.65 1.25 1.2862 0 4 3 4 73.95 6.39 1.2817 8 8 1 8 73.97 3.66 1.2815 1 4 3 8 74.14 1.04 1.2790 11 2 1 8 74.41 1.53 1.2749 3 3 3 8 75.60 1.21 1.2578 11 3 1 8 77.08 1.06 1.2373 12 2 0 4 77.75 3.33 1.2283 1 12 1 8 77.81 2.24 1.2275 9 4 2 8 77.91 2.08 1.2261 5 2 3 8 79.96 1.01 1.1999 3 10 2 8 80.24 1.08 1.1964 11 5 1 8 80.41 1.66 1.1943 9 5 2 8 82.71 1.22 1.1668 6 3 3 8 84.34 2.94 1.1483 4 6 3 8 84.82 1.12 1.1431 5 10 2 8 86.37 1.23 1.1264 8 8 2 8 87.46 1.11 1.1152 0 8 3 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.