Phengite Mookherjee M, Redfern S A T, Zhang M European Journal of Mineralogy 13 (2001) 545-555 Thermal response of structure and hydroxyl ion of phengite-2M_1: an in situ neutron diffraction and FTIR study Sample: T1 = 300 degrees C _database_code_amcsd 0006875 CELL PARAMETERS: 5.2276 9.0701 20.0830 90.000 95.726 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 947.481 Density (g/cm3): 2.707 MAX. ABS. INTENSITY / VOLUME**2: 9.512719799 RIR: 1.144 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.85 100.00 9.9914 0 0 2 2 17.75 17.15 4.9957 0 0 4 2 19.67 16.65 4.5122 1 1 0 4 19.79 48.84 4.4856 -1 1 1 4 20.08 17.38 4.4226 0 2 1 4 20.55 2.05 4.3217 1 1 1 4 20.89 3.75 4.2527 -1 1 2 4 21.52 15.62 4.1296 0 2 2 4 22.83 14.45 3.8956 -1 1 3 4 23.74 13.07 3.7487 0 2 3 4 25.43 19.56 3.5027 -1 1 4 4 26.55 22.47 3.3578 0 2 4 4 26.77 32.83 3.3305 0 0 6 2 27.77 20.96 3.2131 1 1 4 4 28.52 1.01 3.1292 -1 1 5 4 29.80 20.05 2.9984 0 2 5 4 31.15 18.71 2.8710 1 1 5 4 31.99 9.28 2.7978 -1 1 6 4 34.31 1.02 2.6139 1 3 0 4 34.38 9.71 2.6087 -1 3 1 4 34.49 4.75 2.6008 2 0 0 2 34.77 14.32 2.5804 -2 0 2 2 34.84 23.76 2.5753 1 3 1 4 35.73 2.66 2.5127 -1 1 7 4 35.95 1.57 2.4978 0 0 8 2 36.28 7.79 2.4758 -1 3 3 4 36.56 5.44 2.4578 2 0 2 2 37.35 11.63 2.4073 -2 0 4 2 37.59 28.11 2.3928 1 3 3 4 39.82 1.19 2.2638 -2 2 1 4 40.02 1.89 2.2531 0 4 1 4 40.27 4.92 2.2396 -1 3 5 4 40.63 3.91 2.2205 2 2 1 4 40.68 1.94 2.2180 2 0 4 2 40.81 1.49 2.2113 0 4 2 4 41.12 3.15 2.1954 -2 2 3 4 41.80 1.13 2.1609 2 2 2 4 41.88 5.33 2.1569 -2 0 6 2 42.25 12.54 2.1390 1 3 5 4 43.85 1.25 2.0648 0 4 4 4 45.39 7.89 1.9983 0 0 10 2 45.88 5.54 1.9778 -1 3 7 4 46.39 3.23 1.9573 2 0 6 2 46.63 1.06 1.9478 -2 2 6 4 47.91 1.13 1.8987 -2 0 8 2 48.38 1.14 1.8814 1 3 7 4 48.57 2.56 1.8743 0 4 6 4 49.87 1.23 1.8286 0 2 10 4 51.47 1.18 1.7756 0 4 7 4 52.23 2.52 1.7514 -2 2 8 4 52.74 2.00 1.7357 -1 3 9 4 53.50 1.79 1.7128 1 5 0 4 53.55 1.02 1.7114 -1 5 1 4 53.62 2.27 1.7091 2 4 0 4 53.94 2.56 1.6999 2 2 7 4 54.27 1.54 1.6902 -3 1 3 4 55.09 6.41 1.6669 -2 0 10 2 55.11 1.50 1.6666 2 4 2 4 55.50 1.31 1.6558 -2 2 9 4 55.63 1.76 1.6522 3 1 2 4 55.64 12.10 1.6518 1 3 9 4 56.20 3.27 1.6368 -1 5 4 4 56.64 2.93 1.6252 -3 1 5 4 57.12 1.12 1.6124 3 1 3 4 57.21 1.01 1.6101 -2 4 5 4 57.35 2.14 1.6065 2 2 8 4 57.45 2.15 1.6042 1 5 4 4 58.39 1.23 1.5803 -3 1 6 4 58.99 1.03 1.5657 3 1 4 4 59.12 1.05 1.5628 -2 4 6 4 59.40 1.40 1.5559 1 5 5 4 59.91 1.15 1.5440 -1 5 6 4 60.60 5.39 1.5281 -1 3 11 4 61.25 2.22 1.5133 2 0 10 2 61.32 5.91 1.5117 0 6 0 2 61.42 12.61 1.5096 -3 3 1 4 62.07 1.27 1.4952 -3 3 3 4 62.10 1.71 1.4947 0 6 2 4 62.31 2.22 1.4902 3 3 1 4 62.71 1.02 1.4816 2 4 6 4 63.23 1.07 1.4706 -2 0 12 2 63.85 2.69 1.4579 1 3 11 4 69.14 1.21 1.3587 2 2 11 4 69.35 9.31 1.3550 -1 3 13 4 70.07 4.45 1.3429 2 0 12 2 70.11 2.26 1.3422 0 4 12 4 71.17 1.60 1.3248 -2 2 13 4 72.29 1.89 1.3069 2 6 0 4 72.34 1.41 1.3063 -4 0 2 2 72.46 4.24 1.3043 -2 6 2 4 72.72 1.70 1.3004 4 0 0 2 72.84 2.04 1.2985 -3 3 9 4 72.94 1.02 1.2969 1 3 13 4 73.18 1.89 1.2933 0 6 8 4 73.69 2.12 1.2856 3 3 7 4 74.05 3.05 1.2802 -2 6 4 4 74.52 1.98 1.2733 4 0 2 2 75.68 1.45 1.2567 -1 7 1 4 75.70 1.16 1.2563 -2 2 14 4 75.84 1.34 1.2545 -4 0 6 2 76.22 2.37 1.2492 2 6 4 4 76.23 1.21 1.2489 0 0 16 2 76.28 1.01 1.2482 -3 5 3 4 77.42 1.01 1.2327 3 5 2 4 77.85 1.30 1.2270 -4 2 5 4 87.01 2.77 1.1198 -2 6 10 4 88.08 1.28 1.1090 4 0 8 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.