Na1.265Mn3.475(PO4)3 Yakubovich O V, Massa W, Gavrilenko P G, Dimitrova O V European Journal of Mineralogy 17 (2005) 741-747 The crystal structure of a new synthetic member in the wyllieite group: Na1.265Mn2+2.690Mn3+0.785(PO4)3 Note: Uiso's for Mn2 and Mn3 corrected by authors _database_code_amcsd 0007131 CELL PARAMETERS: 6.5291 12.6530 10.9520 90.000 97.180 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 897.679 Density (g/cm3): 3.700 MAX. ABS. INTENSITY / VOLUME**2: 12.96618790 RIR: 1.141 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.73 4.29 8.2435 0 1 1 4 13.67 5.40 6.4779 1 0 0 2 14.00 54.81 6.3265 0 2 0 2 16.31 16.60 5.4331 0 0 2 2 16.58 7.38 5.3456 -1 1 1 4 18.20 2.74 4.8739 1 1 1 4 19.61 6.77 4.5261 1 2 0 4 19.97 1.46 4.4453 -1 0 2 2 20.59 4.07 4.3140 -1 2 1 4 21.18 10.30 4.1940 -1 1 2 4 21.56 3.72 4.1218 0 2 2 4 21.92 2.08 4.0543 1 2 1 4 22.64 1.54 3.9281 1 0 2 2 25.20 1.70 3.5345 1 3 0 4 25.58 30.16 3.4822 0 1 3 4 25.97 2.21 3.4307 -1 3 1 4 27.59 1.20 3.2334 -1 1 3 4 28.21 2.01 3.1632 0 4 0 2 28.45 1.44 3.1378 2 1 0 4 28.64 34.76 3.1169 -2 1 1 4 29.19 11.91 3.0597 -1 3 2 4 29.41 3.94 3.0372 0 4 1 4 30.31 15.75 2.9489 -2 0 2 2 30.60 34.96 2.9218 2 1 1 4 31.02 11.72 2.8831 2 2 0 4 31.11 3.67 2.8745 1 3 2 4 31.20 2.35 2.8668 -2 2 1 4 32.11 16.62 2.7876 -1 4 1 4 32.59 9.99 2.7478 0 3 3 4 32.76 100.00 2.7337 0 4 2 4 32.97 41.75 2.7165 0 0 4 2 33.01 4.53 2.7137 1 4 1 4 33.53 9.92 2.6728 -2 2 2 4 33.95 18.09 2.6407 2 0 2 2 34.81 3.46 2.5773 -1 4 2 4 34.91 2.26 2.5702 -1 1 4 4 35.09 39.20 2.5574 -2 3 1 4 35.51 19.91 2.5279 -2 1 3 4 35.98 10.33 2.4961 0 2 4 4 36.72 1.26 2.4476 1 3 3 4 36.88 7.78 2.4369 2 2 2 4 38.18 5.38 2.3571 1 5 0 4 39.83 1.29 2.2630 2 4 0 4 40.48 2.60 2.2286 -1 3 4 4 40.59 1.01 2.2227 -2 0 4 2 41.01 3.40 2.2008 -2 3 3 4 42.19 10.12 2.1419 0 1 5 4 42.47 23.59 2.1285 3 1 0 4 42.88 4.28 2.1088 0 6 0 2 43.63 10.23 2.0744 0 5 3 4 43.72 1.41 2.0704 -3 1 2 4 43.73 2.31 2.0702 0 6 1 4 43.93 1.56 2.0609 0 4 4 4 44.33 1.44 2.0435 3 2 0 4 44.70 1.38 2.0272 2 4 2 4 45.26 12.03 2.0037 2 3 3 4 45.62 1.11 1.9887 -2 5 1 4 46.16 1.06 1.9665 3 2 1 4 46.18 7.87 1.9659 0 6 2 4 46.22 2.77 1.9640 2 0 4 2 46.95 2.30 1.9351 2 5 1 4 47.04 6.49 1.9318 0 3 5 4 47.29 2.83 1.9220 3 3 0 4 47.99 1.02 1.8956 1 2 5 4 48.54 3.21 1.8757 2 2 4 4 50.07 7.55 1.8218 -1 5 4 4 50.16 1.21 1.8186 -2 4 4 4 50.52 1.47 1.8066 -2 5 3 4 51.03 3.00 1.7896 -3 4 1 4 51.15 1.17 1.7857 -3 1 4 4 51.16 7.14 1.7855 -1 1 6 4 51.32 1.24 1.7804 2 3 4 4 51.73 5.48 1.7673 2 6 0 4 52.38 14.57 1.7467 -2 3 5 4 52.56 5.72 1.7411 1 7 0 4 54.07 2.11 1.6960 3 2 3 4 54.54 2.63 1.6825 1 4 5 4 55.04 12.33 1.6686 2 4 4 4 55.40 2.56 1.6584 -3 3 4 4 55.41 1.80 1.6583 -1 3 6 4 55.76 1.08 1.6487 0 5 5 4 55.80 3.20 1.6475 -3 5 1 4 55.98 2.61 1.6426 3 5 0 4 56.26 1.51 1.6353 -1 5 5 4 56.89 1.14 1.6184 -4 1 1 4 56.96 3.09 1.6167 -2 2 6 4 57.01 6.77 1.6154 -3 5 2 4 57.30 12.71 1.6080 -4 0 2 2 57.80 1.20 1.5952 -4 1 2 4 58.00 1.21 1.5902 -1 7 3 4 58.20 1.94 1.5853 -3 2 5 4 58.27 1.30 1.5834 3 1 4 4 58.34 1.81 1.5816 0 8 0 2 58.75 12.30 1.5717 0 4 6 4 59.18 1.95 1.5613 4 1 1 4 59.71 8.72 1.5487 2 7 1 4 60.04 1.54 1.5409 -4 1 3 4 60.05 3.12 1.5408 0 1 7 4 60.23 1.89 1.5365 1 8 0 4 60.41 3.85 1.5325 3 5 2 4 60.62 4.15 1.5276 -1 8 1 4 61.17 1.27 1.5151 1 8 1 4 61.63 1.04 1.5049 0 7 4 4 61.73 8.02 1.5027 2 0 6 2 61.79 1.18 1.5015 4 0 2 2 62.19 1.48 1.4927 3 3 4 4 62.37 4.65 1.4887 -1 7 4 4 62.43 1.12 1.4876 -3 6 2 4 62.77 7.22 1.4804 -2 7 3 4 62.86 1.14 1.4784 -2 4 6 4 63.06 1.68 1.4741 4 3 1 4 63.32 1.14 1.4687 -1 5 6 4 63.57 2.43 1.4636 -2 1 7 4 63.64 4.26 1.4620 2 2 6 4 63.89 1.33 1.4569 -4 3 3 4 63.90 4.81 1.4568 0 3 7 4 64.03 2.22 1.4542 -3 4 5 4 64.66 6.33 1.4415 4 4 0 4 64.88 3.08 1.4372 2 6 4 4 65.26 1.55 1.4298 -1 8 3 4 65.97 1.10 1.4160 2 5 5 4 66.40 1.41 1.4079 3 2 5 4 66.84 1.39 1.3996 1 8 3 4 67.10 1.02 1.3949 -1 4 7 4 67.14 1.26 1.3943 0 9 1 4 67.39 2.74 1.3897 0 7 5 4 68.51 5.33 1.3696 -3 7 2 4 69.16 2.05 1.3583 0 0 8 2 70.46 5.37 1.3364 -4 4 4 4 70.47 1.10 1.3362 4 5 1 4 70.73 1.59 1.3320 1 4 7 4 71.42 1.22 1.3207 1 8 4 4 71.60 4.43 1.3179 3 7 2 4 71.86 1.47 1.3137 3 4 5 4 71.94 1.45 1.3125 -2 0 8 2 73.40 6.54 1.2900 -4 0 6 2 73.52 1.03 1.2882 -2 9 1 4 77.07 1.19 1.2374 1 8 5 4 77.30 1.47 1.2344 4 5 3 4 77.45 1.09 1.2323 -3 8 3 4 78.50 1.30 1.2185 4 4 4 4 79.06 2.41 1.2112 -4 7 1 4 81.73 2.52 1.1783 4 3 5 4 84.91 2.70 1.1421 -2 7 7 4 85.39 2.33 1.1369 -2 3 9 4 86.79 2.64 1.1222 2 4 8 4 87.61 1.15 1.1137 4 7 3 4 87.62 1.68 1.1136 -1 11 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.