Na(NaMn)7Mn22(PO4)18*0.5H2O Keller P, Hatert F, Lissner F, Schleid T, Fransolet A M European Journal of Mineralogy 18 (2006) 765-774 Hydrothermal synthesis and crystal structure of Na(NaMn)7Mn22(PO4)18*0.5H2O, a new compund of fillowite structure type _database_code_amcsd 0007182 CELL PARAMETERS: 15.2741 15.2741 43.3340 90.000 90.000 120.000 SPACE GROUP: R-3 X-RAY WAVELENGTH: 1.541838 Cell Volume: 8755.293 Density (g/cm3): 3.578 MAX. ABS. INTENSITY / VOLUME**2: 11.42661210 RIR: 1.040 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.12 9.22 14.4447 0 0 3 2 7.83 16.11 11.2901 0 1 2 6 10.56 11.63 8.3813 1 0 4 6 12.21 1.35 7.2494 0 1 5 6 12.25 6.20 7.2223 0 0 6 2 13.11 2.99 6.7515 1 1 3 6 14.00 5.51 6.3257 2 0 2 6 15.70 8.79 5.6450 0 2 4 6 16.90 2.36 5.2474 1 1 6 6 16.90 6.14 5.2474 2 -1 6 6 17.69 3.76 5.0127 0 1 8 6 18.21 1.65 4.8716 -1 3 2 6 19.56 3.47 4.5395 3 -1 4 6 19.56 5.65 4.5395 2 1 4 6 20.14 2.38 4.4093 3 0 0 6 20.51 4.27 4.3307 -1 3 5 6 21.07 6.62 4.2172 0 3 3 6 21.20 5.54 4.1907 2 0 8 6 21.58 4.83 4.1181 1 0 10 6 23.29 3.35 3.8185 2 2 0 6 23.64 20.89 3.7634 0 3 6 6 24.11 3.51 3.6917 4 -2 3 6 24.11 2.64 3.6917 2 2 3 6 24.23 1.72 3.6739 1 2 8 6 24.35 1.30 3.6556 1 3 1 6 24.61 21.55 3.6172 4 -1 2 6 24.61 21.76 3.6172 3 1 2 6 24.65 16.22 3.6112 0 0 12 2 25.64 8.87 3.4749 -1 4 4 6 25.64 1.59 3.4749 1 3 4 6 26.33 3.59 3.3846 2 0 11 6 26.38 1.70 3.3785 4 -1 5 6 26.38 4.30 3.3785 3 1 5 6 26.40 2.59 3.3757 2 2 6 6 27.23 3.98 3.2746 2 1 10 6 27.43 3.17 3.2518 3 0 9 6 28.21 5.97 3.1629 4 0 4 6 28.85 1.20 3.0943 -1 3 11 6 29.40 2.15 3.0376 3 1 8 6 29.64 20.95 3.0139 0 1 14 6 29.73 19.21 3.0053 2 3 2 6 29.73 21.38 3.0053 -2 5 2 6 29.86 2.11 2.9919 4 -2 9 6 30.59 3.84 2.9222 3 2 4 6 30.98 8.43 2.8865 4 1 0 6 31.23 3.07 2.8642 -2 5 5 6 31.61 8.08 2.8306 1 4 3 6 31.61 1.07 2.8306 4 1 3 6 31.61 13.61 2.8306 -1 5 3 6 31.70 1.45 2.8225 0 4 8 6 31.92 28.29 2.8035 2 0 14 6 31.96 7.77 2.8000 1 3 10 6 31.96 4.94 2.8000 -1 4 10 6 32.04 43.67 2.7938 3 0 12 6 32.04 56.33 2.7938 0 3 12 6 32.87 1.56 2.7249 3 2 7 6 33.37 4.14 2.6848 4 -1 11 6 33.43 5.57 2.6804 4 1 6 6 33.43 1.00 2.6804 -1 5 6 6 33.43 1.08 2.6804 5 -1 6 6 33.86 1.68 2.6475 2 3 8 6 33.86 4.55 2.6475 -2 5 8 6 34.07 3.04 2.6317 -1 3 14 6 34.07 2.10 2.6317 1 2 14 6 34.11 4.57 2.6289 4 0 10 6 34.91 3.91 2.5700 0 5 4 6 35.26 59.06 2.5457 3 3 0 6 35.99 2.43 2.4957 -2 6 1 6 35.99 5.63 2.4957 2 4 1 6 36.17 2.13 2.4833 4 2 2 6 36.29 1.31 2.4757 1 4 9 6 36.29 1.02 2.4757 -1 5 9 6 36.90 2.26 2.4358 -2 6 4 6 36.90 1.93 2.4358 2 4 4 6 37.46 2.22 2.4009 3 3 6 6 37.46 7.68 2.4009 6 -3 6 6 37.78 4.37 2.3814 3 -1 16 6 37.93 1.03 2.3722 6 -1 1 6 38.04 1.07 2.3658 4 -1 14 6 38.04 4.06 2.3658 3 1 14 6 38.11 4.36 2.3616 1 5 2 6 38.81 1.22 2.3206 6 -1 4 6 39.69 1.20 2.2709 1 2 17 6 39.99 1.62 2.2547 4 1 12 6 39.99 1.12 2.2547 -1 5 12 6 40.68 1.64 2.2180 6 -1 7 6 40.94 2.87 2.2046 6 0 0 6 41.58 3.93 2.1719 4 3 1 6 41.58 3.65 2.1719 7 -3 1 6 41.71 1.35 2.1653 2 4 10 6 41.74 1.70 2.1638 -3 7 2 6 41.74 5.06 2.1638 3 4 2 6 42.39 1.03 2.1321 4 3 4 6 42.69 2.58 2.1181 5 2 0 6 42.80 1.37 2.1130 0 3 18 6 42.89 6.13 2.1086 0 6 6 6 43.18 1.15 2.0953 4 0 16 6 43.22 1.01 2.0934 4 -1 17 6 43.50 1.48 2.0807 6 -3 12 6 43.50 4.03 2.0807 3 3 12 6 44.49 3.22 2.0365 4 -2 18 6 44.58 1.20 2.0325 5 2 6 6 44.86 1.21 2.0207 3 2 16 6 44.92 1.19 2.0181 -3 7 8 6 45.08 2.89 2.0111 5 0 14 6 45.14 1.24 2.0085 7 -1 2 6 45.63 2.49 1.9880 1 2 20 6 46.53 1.54 1.9518 2 3 17 6 46.62 3.40 1.9482 1 0 22 6 46.71 1.83 1.9448 4 2 14 6 46.71 1.49 1.9448 6 -2 14 6 46.86 2.38 1.9388 7 -2 9 6 46.91 1.59 1.9370 1 3 19 6 48.29 9.78 1.8846 1 5 14 6 48.29 2.47 1.8846 -1 6 14 6 48.35 1.31 1.8825 8 -3 2 6 48.35 1.22 1.8825 0 7 2 6 48.37 7.26 1.8817 0 6 12 6 48.37 10.47 1.8817 6 0 12 6 49.29 3.09 1.8488 1 4 18 6 49.29 3.85 1.8488 -1 5 18 6 49.29 2.86 1.8488 5 -1 18 6 49.86 4.59 1.8288 -1 7 10 6 49.86 2.65 1.8288 1 6 10 6 49.92 1.18 1.8270 5 2 12 6 49.92 1.61 1.8270 7 -2 12 6 50.55 5.40 1.8056 0 0 24 2 50.85 1.11 1.7955 7 -1 11 6 51.49 1.33 1.7748 4 4 9 6 51.49 1.74 1.7748 8 -4 9 6 51.99 1.47 1.7588 6 2 7 6 52.05 2.05 1.7571 2 -1 24 6 52.21 1.39 1.7521 1 7 0 6 52.30 1.34 1.7491 3 3 18 6 52.62 3.74 1.7393 8 -1 3 6 52.62 3.10 1.7393 7 1 3 6 52.66 2.05 1.7380 1 5 17 6 52.75 2.34 1.7354 -1 4 22 6 53.66 2.27 1.7082 -2 7 15 6 53.66 2.06 1.7082 2 5 15 6 53.84 1.48 1.7027 1 7 6 6 53.84 1.15 1.7027 -1 8 6 6 54.08 1.05 1.6957 7 -3 16 6 54.08 1.80 1.6957 4 3 16 6 54.20 1.07 1.6923 5 4 1 6 54.35 2.00 1.6879 8 -4 12 6 54.68 2.94 1.6787 4 1 21 6 54.76 2.40 1.6763 5 0 20 6 55.11 1.95 1.6665 3 6 0 6 55.58 5.56 1.6536 0 1 26 6 55.84 1.29 1.6464 8 -1 9 6 55.84 4.40 1.6464 7 1 9 6 57.11 1.87 1.6129 5 3 14 6 57.11 3.43 1.6129 8 -3 14 6 57.11 2.32 1.6129 0 7 14 6 57.89 2.75 1.5928 8 -4 15 6 57.89 2.35 1.5928 4 4 15 6 58.35 2.45 1.5814 8 0 8 6 58.49 1.23 1.5781 2 6 14 6 59.77 2.67 1.5472 -2 6 22 6 60.40 1.61 1.5326 9 -1 4 6 60.77 1.04 1.5241 -1 9 5 6 60.77 2.03 1.5241 1 8 5 6 61.07 1.56 1.5174 4 -1 26 6 61.07 1.20 1.5174 3 1 26 6 61.26 3.26 1.5132 -3 9 12 6 61.26 1.00 1.5132 3 6 12 6 61.26 1.68 1.5132 6 3 12 6 62.38 1.75 1.4886 1 8 8 6 62.56 1.58 1.4847 -3 10 2 6 62.56 1.33 1.4847 3 7 2 6 63.13 1.46 1.4727 3 3 24 6 63.27 5.79 1.4698 9 0 0 6 63.70 4.78 1.4609 2 3 26 6 63.70 4.34 1.4609 -2 5 26 6 63.85 1.12 1.4579 8 1 10 6 64.57 1.91 1.4433 2 8 0 6 64.69 1.51 1.4409 -1 9 11 6 64.93 1.14 1.4361 2 8 3 6 65.12 1.89 1.4325 7 2 14 6 66.42 1.71 1.4075 10 -3 10 6 67.55 1.33 1.3867 4 2 26 6 67.55 1.26 1.3867 6 -2 26 6 68.39 1.65 1.3717 7 4 0 6 68.74 1.91 1.3655 -4 11 3 6 68.81 1.53 1.3644 1 5 26 6 68.92 1.13 1.3624 10 -4 14 6 68.99 1.07 1.3613 9 0 12 6 71.52 1.13 1.3192 4 7 9 6 74.55 2.10 1.2728 6 6 0 6 83.45 1.53 1.1583 9 3 12 6 85.46 1.03 1.1362 0 1 38 6 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.