K(H2O)Ga(H1.5AsO4)2(H2AsO4) Schwendtner K, Kolitsch U European Journal of Mineralogy 19 (2007) 399-409 Two new structure types: KFe3(AsO4)2(HAsO4)2 and K(H2O)M3+(H1.5AsO4)2(H2AsO4) (M3+ = Fe, Ga, In) - synthesis, crystal structure and spectroscopy _database_code_amcsd 0007222 CELL PARAMETERS: 4.6410 8.6960 13.7720 90.000 94.710 90.000 SPACE GROUP: P2/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 553.935 Density (g/cm3): 3.289 MAX. ABS. INTENSITY / VOLUME**2: 34.14819742 RIR: 3.381 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.17 1.47 8.6960 0 1 0 2 12.05 100.00 7.3458 0 1 1 4 12.90 18.54 6.8627 0 0 2 2 16.45 23.72 5.3872 0 1 2 4 19.75 9.45 4.4963 -1 0 1 2 20.76 5.16 4.2781 1 0 1 2 21.44 12.48 4.1450 0 2 1 4 21.76 1.32 4.0836 1 1 0 4 21.95 6.94 4.0490 0 1 3 4 23.17 4.39 3.8387 1 1 1 4 24.55 5.11 3.6268 -1 1 2 4 25.97 1.28 3.4314 0 0 4 2 26.19 19.29 3.4026 1 1 2 4 26.25 9.68 3.3951 -1 0 3 2 27.95 18.15 3.1919 0 1 4 4 28.17 29.95 3.1680 1 2 0 4 28.22 20.08 3.1626 -1 1 3 4 28.32 10.08 3.1517 0 2 3 4 28.55 12.91 3.1269 1 0 3 2 28.56 1.92 3.1256 -1 2 1 4 29.29 14.25 3.0495 1 2 1 4 30.38 16.48 2.9424 1 1 3 4 30.40 3.12 2.9399 -1 2 2 4 30.85 8.38 2.8987 0 3 0 2 31.55 2.05 2.8361 0 3 1 4 32.85 7.56 2.7262 -1 1 4 4 33.26 2.56 2.6936 0 2 4 4 33.49 32.04 2.6759 -1 2 3 4 35.36 1.04 2.5386 1 2 3 4 35.37 10.80 2.5380 1 1 4 4 36.70 2.62 2.4486 0 3 3 4 36.89 9.76 2.4363 -1 3 1 4 37.48 1.48 2.3997 1 3 1 4 37.54 2.13 2.3958 -1 2 4 4 38.38 2.76 2.3452 -1 3 2 4 38.94 4.56 2.3127 2 0 0 2 39.39 2.58 2.2876 0 0 6 2 40.11 1.38 2.2481 -2 0 2 2 40.37 3.49 2.2342 -2 1 1 4 42.34 4.67 2.1349 -1 2 5 4 42.53 2.19 2.1258 1 3 3 4 43.57 3.31 2.0771 2 1 2 4 44.38 2.10 2.0412 -2 2 1 4 44.89 5.84 2.0192 1 2 5 4 45.51 1.83 1.9932 0 3 5 4 46.14 1.68 1.9675 1 4 0 4 46.23 5.09 1.9636 0 4 3 4 46.39 1.80 1.9572 -1 4 1 4 46.71 2.04 1.9447 -2 1 4 4 47.43 2.02 1.9170 -2 2 3 4 47.54 3.62 1.9128 0 1 7 4 47.71 1.66 1.9062 -1 2 6 4 48.94 1.96 1.8610 -1 0 7 2 49.64 7.06 1.8364 0 4 4 4 50.23 1.73 1.8162 2 2 3 4 50.47 2.90 1.8083 2 1 4 4 50.48 2.10 1.8078 2 3 0 4 50.50 1.14 1.8074 -2 3 1 4 50.51 3.02 1.8070 1 2 6 4 50.85 1.30 1.7957 0 3 6 4 50.96 1.01 1.7920 1 3 5 4 51.10 1.16 1.7874 0 2 7 4 51.18 1.74 1.7850 1 4 3 4 51.40 1.81 1.7776 2 3 1 4 51.44 1.37 1.7765 -2 3 2 4 53.28 2.07 1.7194 -2 3 3 4 53.40 2.18 1.7157 0 0 8 2 53.56 1.23 1.7109 -1 2 7 4 53.79 1.03 1.7043 0 4 5 4 53.99 1.05 1.6983 -2 2 5 4 54.02 3.31 1.6975 -2 0 6 2 55.00 1.00 1.6695 2 1 5 4 55.87 2.53 1.6456 2 3 3 4 55.95 1.33 1.6435 -2 3 4 4 56.53 4.98 1.6279 1 5 0 4 56.62 1.53 1.6257 0 5 3 4 57.83 1.17 1.5943 -1 5 2 4 58.98 4.75 1.5660 -1 3 7 4 59.09 4.61 1.5634 2 0 6 2 59.38 1.58 1.5564 -2 3 5 4 59.84 1.66 1.5455 -1 2 8 4 60.27 1.54 1.5356 -2 1 7 4 60.74 2.41 1.5247 2 4 2 4 60.80 2.40 1.5236 -2 4 3 4 61.82 2.87 1.5008 1 3 7 4 63.19 2.15 1.4715 2 4 3 4 63.26 3.07 1.4700 -2 4 4 4 63.34 1.24 1.4684 -2 2 7 4 63.86 1.53 1.4576 3 1 2 4 64.08 1.13 1.4531 3 2 0 4 64.97 1.86 1.4355 -2 0 8 2 65.07 2.02 1.4335 3 2 1 4 65.15 2.09 1.4318 -3 1 4 4 65.81 1.38 1.4192 2 1 7 4 66.47 1.23 1.4067 -2 4 5 4 68.15 1.29 1.3760 2 3 6 4 68.33 1.32 1.3727 1 6 1 4 68.81 2.28 1.3643 -3 3 1 4 69.35 1.48 1.3550 3 2 3 4 69.67 1.19 1.3497 0 3 9 4 69.95 1.22 1.3449 1 2 9 4 69.95 1.36 1.3448 -1 5 6 4 70.82 1.93 1.3305 -1 1 10 4 71.01 1.09 1.3275 -3 2 5 4 71.97 1.30 1.3121 2 5 3 4 72.19 3.11 1.3086 1 5 6 4 74.61 1.36 1.2720 1 6 4 4 81.26 1.32 1.1839 -1 2 11 4 83.79 1.19 1.1545 1 7 3 4 83.86 1.25 1.1537 3 5 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.