Owyheeite Laufek F, Pazout R, Makovicky E European Journal of Mineralogy 19 (2007) 557-566 Crystal structure of owyheeite, Ag1.5Pb4.43Sb6.07S14: refinement from powder synchrotron X-ray diffraction Locality: Kutna Hora, central Bohemia, Czech Republic _database_code_amcsd 0007225 CELL PARAMETERS: 4.1035 27.3144 22.9366 90.000 90.359 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2570.790 Density (g/cm3): 5.858 MAX. ABS. INTENSITY / VOLUME**2: 35.81651001 RIR: 1.991 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 5.03 4.73 17.5648 0 1 1 4 6.47 2.96 13.6572 0 2 0 2 7.53 12.22 11.7345 0 2 1 4 10.07 2.59 8.7824 0 2 2 4 10.45 4.51 8.4624 0 3 1 4 12.02 8.05 7.3624 0 1 3 4 12.41 6.56 7.1307 0 3 2 4 15.10 5.02 5.8672 0 4 2 4 17.99 1.68 4.9319 0 5 2 4 19.50 1.44 4.5524 0 6 0 2 19.62 1.43 4.5239 0 1 5 4 19.88 2.82 4.4653 0 6 1 4 19.98 5.01 4.4448 0 5 3 4 20.22 1.78 4.3912 0 4 4 4 20.42 6.05 4.3485 0 2 5 4 21.00 4.25 4.2312 0 6 2 4 21.90 12.71 4.0579 1 1 0 4 22.22 13.04 4.0001 -1 1 1 4 22.27 8.43 3.9916 1 1 1 4 22.73 46.89 3.9115 0 6 3 4 22.97 1.57 3.8712 -1 0 2 2 23.07 1.48 3.8559 1 0 2 2 23.21 3.42 3.8329 -1 1 2 4 23.27 10.65 3.8227 0 0 6 2 23.30 5.97 3.8180 1 1 2 4 23.36 8.62 3.8078 0 4 5 4 23.50 14.06 3.7858 0 1 6 4 23.78 8.80 3.7410 1 3 0 4 23.98 3.03 3.7108 1 2 2 4 24.08 11.87 3.6956 -1 3 1 4 24.09 3.29 3.6941 0 7 2 4 24.13 9.06 3.6889 1 3 1 4 24.18 14.73 3.6812 0 2 6 4 24.78 11.86 3.5935 -1 1 3 4 24.91 19.55 3.5751 1 1 3 4 24.97 13.83 3.5654 0 6 4 4 24.99 16.43 3.5626 -1 3 2 4 25.08 7.93 3.5506 1 3 2 4 25.35 1.85 3.5130 0 5 5 4 25.60 2.22 3.4794 -1 4 1 4 25.63 100.00 3.4756 0 7 3 4 25.64 4.03 3.4738 1 4 1 4 26.39 1.50 3.3771 0 8 1 4 26.46 1.06 3.3679 -1 3 3 4 26.47 20.18 3.3677 -1 4 2 4 26.55 27.49 3.3576 1 4 2 4 26.59 1.16 3.3528 1 3 3 4 26.63 22.41 3.3469 -1 0 4 2 26.80 16.24 3.3271 1 0 4 2 27.18 1.97 3.2809 1 5 0 4 27.42 77.35 3.2533 0 1 7 4 27.44 1.42 3.2507 -1 2 4 4 27.65 60.31 3.2260 0 7 4 4 27.86 5.75 3.2018 -1 4 3 4 27.98 2.97 3.1888 1 4 3 4 28.33 3.84 3.1502 1 5 2 4 28.41 9.60 3.1414 -1 3 4 4 28.50 1.06 3.1320 0 5 6 4 28.56 16.75 3.1250 1 3 4 4 28.63 1.36 3.1175 0 8 3 4 29.29 7.15 3.0487 -1 1 5 4 29.55 15.90 3.0232 -1 6 1 4 29.58 2.17 3.0196 1 6 1 4 29.68 2.68 3.0096 1 5 3 4 29.73 4.59 3.0053 -1 4 4 4 29.85 6.22 2.9933 -1 2 5 4 30.03 14.50 2.9756 1 2 5 4 30.07 1.56 2.9722 0 7 5 4 30.31 1.52 2.9491 -1 6 2 4 30.47 5.56 2.9339 0 9 2 4 30.47 26.84 2.9336 0 8 4 4 30.75 44.65 2.9073 -1 3 5 4 30.93 44.26 2.8911 1 3 5 4 31.20 7.23 2.8670 0 0 8 2 31.37 4.76 2.8514 0 1 8 4 31.48 2.94 2.8416 1 5 4 4 31.55 25.14 2.8358 -1 6 3 4 31.64 46.40 2.8277 1 7 0 4 31.65 20.94 2.8267 1 6 3 4 31.72 6.82 2.8208 0 9 3 4 31.90 7.29 2.8058 -1 0 6 2 31.91 1.62 2.8050 1 7 1 4 31.98 5.19 2.7985 -1 4 5 4 32.10 8.61 2.7883 1 0 6 2 32.58 10.83 2.7484 -1 2 6 4 32.65 1.32 2.7427 1 7 2 4 32.78 8.88 2.7320 1 2 6 4 33.22 3.53 2.6966 -1 6 4 4 33.36 3.09 2.6862 1 6 4 4 33.40 3.31 2.6824 0 9 4 4 33.42 6.20 2.6814 -1 3 6 4 33.61 2.61 2.6661 1 3 6 4 33.66 3.84 2.6623 1 5 5 4 34.38 14.98 2.6087 -1 8 1 4 34.41 7.05 2.6064 1 8 1 4 35.04 1.43 2.5607 -1 8 2 4 35.37 1.60 2.5374 0 1 9 4 35.46 1.54 2.5317 1 7 4 4 35.47 2.29 2.5311 0 9 5 4 35.57 1.61 2.5241 -1 2 7 4 36.17 2.40 2.4835 1 5 6 4 36.44 1.71 2.4660 0 10 4 4 36.62 5.07 2.4541 0 3 9 4 36.84 5.98 2.4401 1 9 0 4 37.04 3.26 2.4269 0 11 2 4 37.62 1.28 2.3911 1 4 7 4 37.63 2.35 2.3901 -1 8 4 4 37.75 2.18 2.3829 1 8 4 4 38.10 1.25 2.3617 0 11 3 4 38.74 1.19 2.3243 -1 5 7 4 38.77 4.97 2.3228 -1 2 8 4 38.94 1.15 2.3126 1 5 7 4 39.00 5.42 2.3096 1 2 8 4 39.49 3.06 2.2820 -1 8 5 4 39.59 2.82 2.2762 0 12 0 2 39.63 1.41 2.2741 1 8 5 4 39.73 2.59 2.2686 1 7 6 4 39.83 10.63 2.2634 -1 10 1 4 39.85 1.28 2.2619 0 2 10 4 39.85 12.89 2.2619 1 10 1 4 40.32 6.41 2.2369 -1 6 7 4 40.40 2.02 2.2326 0 12 2 4 40.41 12.47 2.2318 -1 10 2 4 40.47 11.19 2.2289 1 10 2 4 40.48 8.57 2.2281 -1 4 8 4 40.52 9.29 2.2265 1 6 7 4 40.57 11.73 2.2237 0 6 9 4 40.71 7.50 2.2164 1 4 8 4 41.11 2.44 2.1956 0 8 8 4 41.35 1.27 2.1837 0 11 5 4 41.53 1.05 2.1742 0 4 10 4 41.73 3.24 2.1643 -1 5 8 4 41.95 2.75 2.1535 1 5 8 4 42.36 1.47 2.1337 0 7 9 4 42.55 4.69 2.1244 1 11 0 4 42.73 1.29 2.1162 -1 10 4 4 42.73 6.50 2.1160 -1 11 1 4 42.76 15.85 2.1148 0 5 10 4 42.76 2.90 2.1148 1 11 1 4 43.24 9.96 2.0923 0 13 1 4 43.42 3.78 2.0841 0 9 8 4 43.46 1.47 2.0824 0 11 6 4 43.75 6.64 2.0690 -1 4 9 4 43.99 4.92 2.0584 1 4 9 4 44.10 2.82 2.0533 1 9 6 4 44.12 8.35 2.0525 -1 8 7 4 44.14 43.57 2.0517 2 0 0 2 44.22 5.36 2.0483 0 6 10 4 44.27 1.64 2.0459 2 1 0 4 44.31 7.66 2.0444 1 8 7 4 44.36 4.10 2.0423 0 8 9 4 44.48 1.85 2.0367 2 1 1 4 44.73 1.57 2.0260 0 13 3 4 44.93 8.34 2.0176 -1 7 8 4 44.93 5.33 2.0175 -1 5 9 4 45.13 4.00 2.0089 1 7 8 4 45.16 7.89 2.0078 1 5 9 4 45.42 1.47 1.9968 1 0 10 2 45.68 1.46 1.9861 -1 2 10 4 45.93 1.98 1.9758 1 2 10 4 46.53 2.17 1.9516 0 9 9 4 46.56 1.73 1.9506 1 6 9 4 46.62 3.32 1.9480 0 5 11 4 46.73 6.17 1.9440 0 14 1 4 47.08 1.60 1.9301 -1 11 5 4 47.21 1.48 1.9254 1 11 5 4 47.26 1.16 1.9234 0 14 2 4 47.60 1.46 1.9103 0 13 5 4 47.70 2.66 1.9067 0 1 12 4 47.95 2.50 1.8972 -1 7 9 4 48.17 1.36 1.8890 1 7 9 4 48.66 3.06 1.8711 -1 10 7 4 48.69 3.52 1.8702 1 13 0 4 48.71 2.91 1.8694 0 12 7 4 48.83 2.23 1.8650 1 10 7 4 48.99 3.94 1.8595 -1 11 6 4 48.99 3.14 1.8593 -1 1 11 4 49.12 1.97 1.8548 1 9 8 4 49.13 4.00 1.8544 1 11 6 4 49.26 2.69 1.8499 1 1 11 4 49.35 1.21 1.8465 -1 2 11 4 49.50 4.06 1.8413 0 13 6 4 49.62 1.18 1.8373 1 2 11 4 49.63 1.12 1.8368 -1 6 10 4 49.77 1.61 1.8320 -1 8 9 4 50.26 2.09 1.8154 1 13 3 4 50.26 4.24 1.8152 0 15 1 4 50.28 8.03 1.8145 2 6 3 4 50.34 3.33 1.8125 -2 0 6 2 50.74 2.50 1.7992 2 1 6 4 50.86 1.28 1.7954 0 14 5 4 50.86 1.98 1.7952 -2 7 2 4 51.10 2.04 1.7876 2 2 6 4 51.19 1.44 1.7845 -1 10 8 4 51.25 1.52 1.7827 0 12 8 4 51.29 1.90 1.7813 -2 6 4 4 51.33 1.10 1.7799 1 11 7 4 51.34 6.88 1.7795 0 8 11 4 51.67 10.62 1.7690 -2 7 3 4 51.71 2.40 1.7677 -1 12 6 4 51.77 3.24 1.7657 -1 9 9 4 51.81 7.21 1.7646 2 7 3 4 51.84 1.77 1.7638 -1 5 11 4 51.85 4.37 1.7633 1 12 6 4 51.98 2.26 1.7592 1 9 9 4 52.09 2.19 1.7558 1 5 11 4 52.28 3.05 1.7498 0 2 13 4 52.59 6.32 1.7403 -2 1 7 4 52.67 6.79 1.7378 0 14 6 4 52.70 2.79 1.7368 -1 0 12 2 52.79 6.95 1.7340 -2 7 4 4 52.91 6.78 1.7306 2 1 7 4 52.98 3.02 1.7285 2 7 4 4 53.09 1.29 1.7250 1 1 12 4 53.16 1.89 1.7229 -1 2 12 4 53.30 2.01 1.7186 0 9 11 4 53.32 1.48 1.7180 -1 14 3 4 53.38 1.08 1.7165 0 7 12 4 53.39 1.08 1.7160 1 14 3 4 53.43 3.21 1.7148 1 2 12 4 53.69 1.05 1.7071 0 16 0 2 53.85 1.58 1.7024 0 16 1 4 54.43 2.14 1.6856 -1 14 4 4 54.49 2.08 1.6839 -2 8 4 4 54.52 1.03 1.6830 1 14 4 4 54.57 1.61 1.6818 -1 13 6 4 54.63 1.90 1.6801 2 9 2 4 54.67 3.85 1.6788 2 8 4 4 54.76 2.08 1.6764 0 14 7 4 54.86 1.24 1.6735 -2 0 8 2 55.84 1.20 1.6463 -1 14 5 4 56.58 5.03 1.6266 0 2 14 4 56.62 1.59 1.6255 1 15 3 4 57.10 4.06 1.6130 0 14 8 4 57.61 1.87 1.5999 0 16 5 4 61.31 2.87 1.5121 -2 6 9 4 61.68 1.14 1.5038 2 6 9 4 62.65 1.06 1.4828 -2 7 9 4 62.93 1.65 1.4768 -2 5 10 4 63.34 3.82 1.4683 2 5 10 4 63.48 3.61 1.4654 -2 13 1 4 64.06 1.55 1.4537 -2 6 10 4 64.31 1.91 1.4485 -1 17 4 4 64.39 1.79 1.4469 1 17 4 4 64.54 2.34 1.4438 2 8 9 4 66.08 1.01 1.4139 0 13 12 4 66.25 1.41 1.4108 2 14 1 4 66.84 1.73 1.3998 -1 18 3 4 66.90 1.64 1.3987 1 18 3 4 67.07 1.19 1.3955 1 14 10 4 67.13 1.09 1.3944 0 19 4 4 67.56 1.05 1.3866 0 5 16 4 67.88 1.11 1.3807 -1 12 12 4 67.96 1.07 1.3794 2 12 7 4 68.53 1.66 1.3693 -1 6 15 4 68.58 1.27 1.3683 2 13 6 4 68.82 1.37 1.3642 1 6 15 4 68.92 2.27 1.3625 -1 9 14 4 69.09 1.45 1.3595 -1 11 13 4 69.19 2.01 1.3578 1 9 14 4 69.35 1.48 1.3551 1 11 13 4 69.77 1.61 1.3479 -2 8 11 4 70.20 1.07 1.3408 2 8 11 4 70.52 1.50 1.3354 1 19 3 4 70.98 1.28 1.3279 -2 14 6 4 71.21 1.86 1.3242 2 14 6 4 72.77 1.29 1.2996 -3 3 5 4 73.05 1.36 1.2952 3 3 5 4 74.17 1.21 1.2785 -2 2 14 4 74.69 1.19 1.2708 2 2 14 4 74.73 1.66 1.2702 -2 14 8 4 75.53 1.23 1.2588 -1 16 11 4 75.73 1.09 1.2559 1 16 11 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.