KNa3SrSi8O19*4.3H2O Cadoni M, Ferraris G European Journal of Mineralogy 21 (2009) 485-493 Two new members of the rhodesite mero-plesiotype series close to delhayelite and hydrodelhayelite: synthesis and crystal structure Note: Sample TRO4 Note: cell parameters, occupancy and positional parameters corrected by author _database_code_amcsd 0007279 CELL PARAMETERS: 6.6599 23.7225 7.0225 90.000 91.810 90.000 SPACE GROUP: P2_1/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 1108.928 Density (g/cm3): 2.428 MAX. ABS. INTENSITY / VOLUME**2: 4.970058148 RIR: 0.667 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.45 100.00 11.8612 0 2 0 2 12.61 81.68 7.0190 0 0 1 2 13.15 1.74 6.7306 0 1 1 4 13.30 34.66 6.6566 1 0 0 2 13.82 45.55 6.4090 1 1 0 4 14.66 9.78 6.0406 0 2 1 4 14.94 15.57 5.9306 0 4 0 2 15.26 4.08 5.8049 1 2 0 4 17.41 25.42 5.0924 1 3 0 4 18.07 2.94 4.9080 -1 0 1 2 18.46 21.45 4.8062 -1 1 1 4 18.66 6.59 4.7555 1 0 1 2 19.03 15.74 4.6628 1 1 1 4 19.57 2.34 4.5351 -1 2 1 4 19.60 3.58 4.5301 0 4 1 4 20.05 62.26 4.4281 1 4 0 4 21.81 9.79 4.0753 1 3 1 4 22.49 12.67 3.9537 0 6 0 2 22.62 1.37 3.9307 0 5 1 4 23.02 8.31 3.8636 1 5 0 4 23.53 15.00 3.7811 -1 4 1 4 23.99 20.09 3.7101 1 4 1 4 25.38 7.43 3.5095 0 0 2 2 25.86 46.22 3.4448 0 6 1 4 26.22 27.85 3.3993 1 6 0 4 26.49 2.19 3.3653 0 2 2 4 26.54 7.67 3.3588 1 5 1 4 26.79 3.12 3.3283 2 0 0 2 27.05 16.33 3.2960 2 1 0 4 28.37 10.80 3.1457 -1 0 2 2 28.63 25.14 3.1184 -1 1 2 4 29.00 17.12 3.0790 -1 6 1 4 29.11 11.79 3.0676 2 3 0 4 29.14 15.57 3.0648 1 0 2 2 29.33 34.66 3.0448 -2 0 1 2 29.38 24.11 3.0402 1 6 1 4 29.39 30.00 3.0395 1 1 2 4 29.58 23.22 3.0203 0 4 2 4 29.58 18.29 3.0201 1 7 0 4 30.08 17.65 2.9712 2 0 1 2 30.12 2.40 2.9673 1 2 2 4 30.14 24.85 2.9653 0 8 0 2 30.32 2.46 2.9482 2 1 1 4 30.59 37.43 2.9229 -1 3 2 4 30.81 45.66 2.9025 2 4 0 4 31.03 2.15 2.8822 2 2 1 4 31.30 33.32 2.8577 1 3 2 4 32.10 1.31 2.7887 -1 7 1 4 32.18 13.30 2.7813 2 3 1 4 32.21 58.35 2.7790 -1 4 2 4 32.44 3.56 2.7598 1 7 1 4 32.87 5.19 2.7247 2 5 0 4 32.90 31.76 2.7227 1 4 2 4 33.07 2.08 2.7087 1 8 0 4 34.16 5.72 2.6247 0 6 2 4 35.02 5.43 2.5625 -2 5 1 4 35.25 23.75 2.5462 2 6 0 4 35.37 6.86 2.5380 -1 8 1 4 36.41 1.30 2.4676 0 9 1 4 36.50 11.08 2.4616 -1 6 2 4 36.62 5.83 2.4540 -2 0 2 2 36.67 10.11 2.4507 1 9 0 4 36.82 1.04 2.4410 -2 1 2 4 37.12 9.71 2.4223 1 6 2 4 37.27 7.04 2.4124 -2 6 1 4 37.42 1.93 2.4031 -2 2 2 4 37.84 1.36 2.3778 2 0 2 2 37.88 1.54 2.3753 2 6 1 4 38.48 2.49 2.3397 0 0 3 2 38.62 2.40 2.3314 2 2 2 4 38.78 1.51 2.3221 -1 9 1 4 39.07 1.05 2.3055 -1 7 2 4 39.07 2.66 2.3054 1 9 1 4 39.25 2.51 2.2954 0 2 3 4 40.12 5.14 2.2474 0 10 1 4 40.20 1.59 2.2435 0 3 3 4 40.65 1.66 2.2196 -1 1 3 4 40.75 14.78 2.2140 2 8 0 4 40.89 2.21 2.2070 2 4 2 4 41.20 7.61 2.1911 -1 2 3 4 41.49 1.53 2.1766 1 1 3 4 41.87 11.69 2.1578 -1 8 2 4 42.31 7.52 2.1363 3 3 0 4 42.32 1.75 2.1358 -1 10 1 4 42.33 2.11 2.1351 -3 0 1 2 42.42 12.07 2.1311 1 8 2 4 42.53 1.63 2.1258 2 5 2 4 42.56 2.83 2.1243 -2 8 1 4 42.59 1.60 2.1228 1 10 1 4 42.93 2.35 2.1068 1 3 3 4 43.10 1.97 2.0989 2 8 1 4 43.11 1.14 2.0984 0 5 3 4 43.15 3.16 2.0967 3 0 1 2 43.32 1.08 2.0886 3 1 1 4 43.36 1.99 2.0868 -1 4 3 4 43.55 2.97 2.0782 3 4 0 4 43.92 1.85 2.0615 0 11 1 4 43.92 2.48 2.0613 -3 3 1 4 44.14 1.94 2.0516 1 11 0 4 44.92 2.03 2.0178 -1 5 3 4 45.11 1.56 2.0099 3 5 0 4 45.13 1.88 2.0089 -3 4 1 4 45.64 1.78 1.9876 -2 7 2 4 45.91 2.04 1.9768 3 4 1 4 46.22 2.15 1.9641 1 11 1 4 46.65 3.65 1.9471 -3 5 1 4 46.66 6.46 1.9465 2 7 2 4 46.78 1.54 1.9420 -1 6 3 4 46.96 3.35 1.9350 3 6 0 4 47.04 5.37 1.9318 2 10 0 4 47.40 1.42 1.9178 3 5 1 4 47.53 6.40 1.9129 1 6 3 4 47.80 1.17 1.9028 0 12 1 4 47.80 16.74 1.9028 -3 0 2 2 48.01 9.40 1.8951 1 12 0 4 48.04 6.92 1.8940 -1 10 2 4 48.13 3.75 1.8906 -2 8 2 4 48.23 2.23 1.8870 -2 3 3 4 48.45 6.79 1.8788 -3 2 2 4 48.45 1.09 1.8787 -3 6 1 4 48.53 5.45 1.8759 1 10 2 4 48.66 1.63 1.8713 -2 10 1 4 49.07 3.93 1.8564 3 7 0 4 49.11 3.14 1.8550 2 8 2 4 49.15 2.82 1.8539 2 10 1 4 49.19 1.54 1.8524 3 6 1 4 49.28 15.08 1.8493 3 0 2 2 49.35 1.30 1.8466 -2 4 3 4 49.69 3.10 1.8348 2 3 3 4 49.72 4.49 1.8337 -1 12 1 4 49.91 6.22 1.8272 3 2 2 4 49.96 3.55 1.8254 1 12 1 4 50.36 3.92 1.8118 -3 4 2 4 50.52 1.57 1.8065 -3 7 1 4 50.79 5.94 1.7975 2 4 3 4 51.78 2.06 1.7654 3 4 2 4 52.12 22.78 1.7547 0 0 4 2 52.43 2.87 1.7453 2 11 1 4 52.47 1.72 1.7439 -2 6 3 4 52.73 2.98 1.7359 0 2 4 4 53.16 1.82 1.7230 3 5 2 4 53.18 5.25 1.7224 0 12 2 4 53.44 1.48 1.7146 -3 6 2 4 53.53 1.68 1.7120 3 8 1 4 53.59 1.12 1.7101 -1 0 4 2 53.74 5.28 1.7056 -2 10 2 4 53.95 10.81 1.6997 2 12 0 4 54.50 1.28 1.6837 1 0 4 2 54.65 6.22 1.6794 2 10 2 4 54.80 2.27 1.6751 3 6 2 4 54.85 9.00 1.6738 -1 12 2 4 55.14 5.70 1.6658 0 10 3 4 55.19 7.45 1.6641 4 0 0 2 55.30 6.77 1.6613 1 12 2 4 55.78 1.17 1.6480 4 2 0 4 55.96 2.54 1.6432 -1 4 4 4 56.37 2.62 1.6321 -3 1 3 4 56.51 1.17 1.6285 4 3 0 4 56.66 1.31 1.6246 -1 10 3 4 56.84 2.15 1.6197 1 4 4 4 57.32 2.92 1.6075 1 10 3 4 57.46 1.01 1.6039 0 6 4 4 58.20 1.18 1.5852 3 0 3 2 58.34 2.87 1.5817 3 1 3 4 58.53 1.26 1.5771 -3 4 3 4 58.71 3.83 1.5725 -4 4 1 4 58.83 1.11 1.5696 -1 6 4 4 58.84 1.25 1.5694 -2 1 4 4 59.57 1.85 1.5519 4 4 1 4 59.69 1.58 1.5491 1 6 4 4 59.80 1.58 1.5466 -3 5 3 4 59.80 7.70 1.5465 3 11 0 4 59.97 1.03 1.5426 -2 3 4 4 60.29 1.36 1.5352 1 11 3 4 60.35 3.35 1.5338 4 6 0 4 60.94 5.78 1.5203 -2 4 4 4 61.32 2.86 1.5117 -3 6 3 4 61.39 3.47 1.5101 0 8 4 4 61.40 1.37 1.5100 2 14 0 4 61.71 1.21 1.5032 -2 10 3 4 62.34 1.15 1.4894 4 6 1 4 62.58 1.22 1.4843 -3 10 2 4 62.61 4.71 1.4837 2 4 4 4 62.66 8.01 1.4827 0 16 0 2 62.97 1.78 1.4760 3 12 0 4 63.04 1.98 1.4746 -4 4 2 4 63.67 1.30 1.4615 -2 6 4 4 64.18 3.13 1.4512 4 8 0 4 64.56 2.52 1.4436 -2 11 3 4 64.68 2.38 1.4411 4 4 2 4 65.31 3.47 1.4288 2 6 4 4 65.33 1.09 1.4284 2 15 0 4 65.73 4.28 1.4207 -4 6 2 4 66.13 2.70 1.4130 -1 15 2 4 66.25 1.37 1.4107 0 10 4 4 66.53 4.10 1.4054 1 15 2 4 67.33 3.05 1.3907 4 6 2 4 67.40 1.17 1.3895 -2 8 4 4 67.44 1.92 1.3887 -4 7 2 4 68.10 1.09 1.3768 -4 0 3 2 68.11 1.91 1.3767 -3 3 4 4 68.43 1.09 1.3709 -3 12 2 4 68.73 1.99 1.3658 0 16 2 4 68.79 1.14 1.3647 2 12 3 4 68.91 2.04 1.3627 1 1 5 4 68.93 3.12 1.3624 4 10 0 4 69.03 1.71 1.3606 4 7 2 4 69.39 1.11 1.3544 2 16 0 4 69.86 1.10 1.3463 -1 4 5 4 70.17 2.36 1.3412 -1 16 2 4 70.18 1.37 1.3410 -3 5 4 4 70.56 3.06 1.3347 1 16 2 4 70.67 2.13 1.3330 -2 16 1 4 70.96 1.35 1.3282 4 8 2 4 71.06 1.67 1.3267 2 16 1 4 71.29 2.45 1.3229 0 6 5 4 71.59 1.77 1.3180 -3 6 4 4 71.60 2.93 1.3179 0 18 0 2 72.00 1.17 1.3115 2 13 3 4 72.04 1.85 1.3109 -2 10 4 4 72.21 1.71 1.3083 -2 0 5 2 72.71 2.37 1.3005 5 0 1 2 73.05 1.12 1.2953 0 18 1 4 73.39 2.52 1.2902 1 6 5 4 73.54 1.08 1.2879 3 15 0 4 73.58 1.74 1.2872 2 10 4 4 73.94 1.83 1.2818 1 12 4 4 74.13 2.89 1.2791 2 0 5 2 74.82 2.01 1.2690 -2 16 2 4 75.02 1.22 1.2661 1 7 5 4 75.26 1.08 1.2627 2 3 5 4 75.42 1.28 1.2604 -3 12 3 4 75.58 1.66 1.2581 2 16 2 4 75.58 1.51 1.2580 -4 12 1 4 75.99 1.61 1.2524 0 16 3 4 76.34 1.74 1.2474 4 12 1 4 76.95 1.68 1.2391 5 7 0 4 77.56 2.15 1.2308 -2 12 4 4 77.60 1.26 1.2303 5 1 2 4 77.85 2.04 1.2270 -4 0 4 2 79.07 2.43 1.2111 2 12 4 4 79.46 1.37 1.2062 -4 12 2 4 80.04 1.25 1.1988 -5 6 2 4 80.19 1.32 1.1970 -2 8 5 4 80.85 1.08 1.1889 4 0 4 2 80.95 1.94 1.1876 4 12 2 4 81.91 2.47 1.1762 5 6 2 4 82.16 1.15 1.1731 -5 0 3 2 82.27 1.52 1.1719 -4 6 4 4 82.47 3.22 1.1695 -3 16 2 4 83.21 1.03 1.1611 -2 18 2 4 83.21 1.21 1.1610 5 10 0 4 83.26 1.32 1.1605 -1 19 2 4 83.59 2.71 1.1568 3 16 2 4 83.63 1.52 1.1563 1 19 2 4 84.35 1.46 1.1483 0 18 3 4 84.39 1.08 1.1477 3 11 4 4 84.58 1.73 1.1457 -2 10 5 4 84.94 1.08 1.1417 5 0 3 2 84.97 1.07 1.1414 -3 12 4 4 85.24 1.58 1.1385 4 6 4 4 85.38 1.72 1.1369 -1 4 6 4 85.68 1.01 1.1338 -4 8 4 4 85.80 4.21 1.1325 0 16 4 4 86.69 1.02 1.1232 1 12 5 4 87.03 1.40 1.1196 3 15 3 4 87.81 1.23 1.1117 -1 6 6 4 87.84 1.84 1.1114 -5 10 2 4 88.28 1.52 1.1070 4 16 0 4 88.92 1.20 1.1007 1 6 6 4 89.68 1.22 1.0933 5 10 2 4 89.97 3.02 1.0905 6 4 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.