KNaCa2Si8O19*5H2O Cadoni M, Ferraris G European Journal of Mineralogy 21 (2009) 485-493 Two new members of the rhodesite mero-plesiotype series close to delhayelite and hydrodelhayelite: synthesis and crystal structure Note: Sample TRO3 _database_code_amcsd 0007280 CELL PARAMETERS: 6.5850 23.7760 7.0250 90.000 90.000 90.000 SPACE GROUP: Pn2_1m X-RAY WAVELENGTH: 1.541838 Cell Volume: 1099.869 Density (g/cm3): 2.330 MAX. ABS. INTENSITY / VOLUME**2: 3.685339560 RIR: 0.515 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.44 71.81 11.8880 0 2 0 1 13.14 30.60 6.7371 0 1 1 2 13.45 78.01 6.5850 1 0 0 2 13.95 34.05 6.3461 1 1 0 2 14.90 55.92 5.9440 0 4 0 1 15.38 9.72 5.7603 1 2 0 2 16.87 17.00 5.2570 0 3 1 2 17.51 40.41 5.0648 1 3 0 2 18.47 37.62 4.8043 1 0 1 4 19.93 1.78 4.4543 1 2 1 4 20.12 64.95 4.4123 1 4 0 2 21.63 26.49 4.1084 1 3 1 4 22.44 12.61 3.9627 0 6 0 1 22.58 11.54 3.9379 0 5 1 2 23.07 8.30 3.8551 1 5 0 2 23.81 9.00 3.7364 1 4 1 4 25.36 16.41 3.5125 0 0 2 2 26.25 32.76 3.3953 1 6 0 2 26.37 2.08 3.3797 1 5 1 4 26.46 1.33 3.3685 0 2 2 2 27.08 5.86 3.2925 2 0 0 2 27.35 18.22 3.2614 2 1 0 2 28.81 5.89 3.0992 1 0 2 4 29.06 100.00 3.0732 1 1 2 4 29.20 3.98 3.0579 0 7 1 2 29.21 3.35 3.0570 1 6 1 4 29.37 27.47 3.0406 2 3 0 2 29.54 32.00 3.0240 0 4 2 2 29.59 49.84 3.0187 1 7 0 2 29.79 6.37 2.9989 1 2 2 4 29.97 4.26 2.9813 2 0 1 4 30.07 19.95 2.9720 0 8 0 1 30.21 32.83 2.9581 2 1 1 4 30.92 2.30 2.8918 2 2 1 4 30.98 77.51 2.8863 1 3 2 4 31.05 46.80 2.8802 2 4 0 2 32.08 17.58 2.7904 2 3 1 4 32.28 67.88 2.7735 1 7 1 4 32.58 74.40 2.7481 1 4 2 4 33.07 5.37 2.7089 1 8 0 2 33.09 2.82 2.7070 2 5 0 2 33.63 10.93 2.6649 2 4 1 4 34.11 16.43 2.6285 0 6 2 2 35.45 2.44 2.5324 2 6 0 2 35.52 12.44 2.5275 1 8 1 4 35.54 11.07 2.5259 2 5 1 4 36.33 3.41 2.4727 0 9 1 2 36.65 2.49 2.4518 1 9 0 2 36.82 10.66 2.4412 1 6 2 4 37.44 3.13 2.4022 2 0 2 4 37.76 1.02 2.3824 2 6 1 4 38.06 2.24 2.3641 2 7 0 2 38.91 1.15 2.3149 1 9 1 4 39.36 2.03 2.2894 1 7 2 4 40.15 1.48 2.2457 0 3 3 2 40.25 1.79 2.2406 2 7 1 4 40.50 2.71 2.2272 2 4 2 4 40.90 1.80 2.2063 1 0 3 4 40.91 2.96 2.2062 2 8 0 2 41.63 1.41 2.1693 1 2 3 4 42.13 22.17 2.1451 1 8 2 4 42.53 1.10 2.1255 1 3 3 4 42.75 1.99 2.1154 3 3 0 2 43.18 3.65 2.0951 3 0 1 4 43.82 1.93 2.0659 0 11 1 2 43.97 11.28 2.0591 3 4 0 2 44.08 1.98 2.0542 2 6 2 4 44.10 3.24 2.0537 1 11 0 2 45.51 1.02 1.9929 3 5 0 2 45.93 7.37 1.9760 3 4 1 4 46.29 4.70 1.9612 2 7 2 4 47.15 1.04 1.9277 1 6 3 4 47.15 3.31 1.9276 2 10 0 2 47.34 6.22 1.9201 3 6 0 2 47.95 9.13 1.8973 1 12 0 2 48.24 5.25 1.8864 1 10 2 4 48.30 3.43 1.8841 2 2 3 4 48.74 11.25 1.8682 2 8 2 4 48.93 28.19 1.8614 3 0 2 4 49.09 1.79 1.8558 3 1 2 4 49.19 1.07 1.8522 3 6 1 4 49.25 3.37 1.8502 1 7 3 4 49.44 5.17 1.8435 3 7 0 2 49.57 5.13 1.8390 3 2 2 4 50.21 9.19 1.8169 2 4 3 4 50.36 1.03 1.8121 3 3 2 4 51.23 1.54 1.7832 3 7 1 4 51.41 1.12 1.7773 2 9 2 4 51.44 2.73 1.7764 3 4 2 4 51.55 1.74 1.7729 1 11 2 4 51.64 2.05 1.7699 0 13 1 2 51.78 1.40 1.7656 3 8 0 2 51.89 1.26 1.7622 1 13 0 2 52.07 29.55 1.7563 0 0 4 2 52.20 1.19 1.7523 0 9 3 2 52.28 6.10 1.7499 2 11 1 4 52.68 1.55 1.7374 0 2 4 2 53.07 5.36 1.7257 0 12 2 2 53.28 4.19 1.7193 2 6 3 4 53.62 1.68 1.7093 1 13 1 4 53.99 4.77 1.6983 0 14 0 1 54.02 8.64 1.6977 2 12 0 2 54.04 3.23 1.6969 1 0 4 4 54.29 17.82 1.6898 2 10 2 4 54.46 1.84 1.6848 3 6 2 4 55.01 10.17 1.6693 1 12 2 4 55.21 3.66 1.6637 2 7 3 4 55.85 2.44 1.6463 4 0 0 2 55.99 1.76 1.6423 4 1 0 2 56.39 4.39 1.6317 1 4 4 4 57.15 1.03 1.6118 4 3 0 2 57.38 1.49 1.6058 2 8 3 4 57.55 10.37 1.6014 3 0 3 4 58.08 3.13 1.5883 0 11 3 2 58.51 1.60 1.5776 3 8 2 4 58.74 1.39 1.5719 3 10 1 4 59.23 1.76 1.5599 1 6 4 4 59.28 1.03 1.5590 2 13 1 4 59.76 4.33 1.5476 4 4 1 4 59.81 1.28 1.5463 2 1 4 4 59.81 1.48 1.5463 3 4 3 4 59.91 2.74 1.5440 1 11 3 4 60.03 1.29 1.5411 1 15 0 2 60.07 8.07 1.5401 3 11 0 2 60.92 4.45 1.5208 2 3 4 4 60.94 1.75 1.5203 4 6 0 2 61.04 4.32 1.5180 1 7 4 4 61.31 1.82 1.5120 0 8 4 2 61.88 8.67 1.4995 2 4 4 4 62.29 1.22 1.4907 4 0 2 4 62.40 1.29 1.4882 2 10 3 4 62.50 3.81 1.4860 0 16 0 1 63.22 2.18 1.4708 3 12 0 2 63.50 1.92 1.4650 4 3 2 4 64.26 1.95 1.4495 1 16 0 2 64.26 1.19 1.4495 4 7 1 4 64.31 2.02 1.4485 3 7 3 4 64.44 1.27 1.4459 4 4 2 4 64.73 2.63 1.4401 4 8 0 2 64.76 1.25 1.4396 3 12 1 4 65.34 1.10 1.4282 2 15 0 2 66.22 6.46 1.4112 1 15 2 4 66.30 1.45 1.4098 3 8 3 4 67.08 3.50 1.3952 4 6 2 4 67.55 2.42 1.3867 2 14 2 4 68.24 3.75 1.3745 2 12 3 4 68.26 1.94 1.3741 1 0 5 4 68.77 15.62 1.3650 4 7 2 4 69.42 1.67 1.3539 1 3 5 4 69.44 1.20 1.3535 4 10 0 2 69.57 1.30 1.3512 3 3 4 4 70.07 1.53 1.3428 1 17 1 4 70.25 4.52 1.3399 1 16 2 4 70.32 1.37 1.3388 1 4 5 4 70.47 2.69 1.3362 3 4 4 4 70.85 1.03 1.3299 2 16 1 4 70.96 1.64 1.3282 3 10 3 4 71.41 2.83 1.3209 0 18 0 1 71.51 1.76 1.3193 3 14 1 4 71.62 1.65 1.3176 3 5 4 4 71.88 1.27 1.3135 4 4 3 4 72.12 1.02 1.3096 4 11 0 2 72.85 1.09 1.2983 0 7 5 2 72.86 1.69 1.2982 2 10 4 4 73.01 1.96 1.2959 3 6 4 4 73.10 2.44 1.2944 5 0 1 4 73.37 3.20 1.2904 2 1 5 4 73.47 1.27 1.2888 1 12 4 4 73.58 1.53 1.2873 2 17 0 2 74.38 2.71 1.2754 2 3 5 4 74.42 2.11 1.2748 1 17 2 4 74.49 5.00 1.2738 1 7 5 4 74.64 1.31 1.2716 3 7 4 4 75.18 3.21 1.2637 2 16 2 4 76.36 1.74 1.2472 1 8 5 4 76.37 1.72 1.2470 2 5 5 4 77.51 1.72 1.2315 5 1 2 4 77.84 2.57 1.2271 4 11 2 4 78.32 1.06 1.2208 0 14 4 2 78.33 3.08 1.2206 2 12 4 4 78.76 1.11 1.2151 1 18 2 4 79.36 1.53 1.2075 5 4 2 4 79.62 2.28 1.2041 5 8 0 2 79.86 1.22 1.2011 4 0 4 4 80.46 1.24 1.1937 5 5 2 4 80.66 1.22 1.1912 4 12 2 4 81.48 1.65 1.1813 1 17 3 4 81.80 1.01 1.1775 5 6 2 4 82.36 1.67 1.1708 0 0 6 2 82.85 2.85 1.1651 3 14 3 4 83.18 2.66 1.1613 3 16 2 4 83.25 2.01 1.1606 3 4 5 4 83.27 1.85 1.1603 1 19 2 4 83.48 3.10 1.1579 3 11 4 4 84.01 1.90 1.1521 5 10 0 2 84.24 1.37 1.1494 4 6 4 4 84.38 1.92 1.1479 5 0 3 4 85.62 1.82 1.1344 0 16 4 2 85.88 2.18 1.1317 1 4 6 4 86.26 1.16 1.1276 3 12 4 4 87.19 2.19 1.1179 1 16 4 4 87.60 1.18 1.1138 4 12 3 4 87.62 1.04 1.1136 4 8 4 4 88.06 2.44 1.1091 2 11 5 4 88.29 2.05 1.1069 1 6 6 4 88.67 1.14 1.1032 2 0 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.