Pb3Fe2(PO4)4(H2O) Mills S J, Kolitsch U, Miyawaki R, Hatert F, Poirier G, Kampf A R, Matsubara S, Tillmanns E European Journal of Mineralogy 22 (2010) 595-604 Pb3Fe3+2(PO4)4(H2O), a new octahedral-tetrahedral framework structure with double-strand chains Locality: synthetic T = 220 C _database_code_amcsd 0017730 CELL PARAMETERS: 9.0440 9.0440 16.7660 90.000 90.000 90.000 SPACE GROUP: P4_12_12 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1371.357 Density (g/cm3): 5.489 MAX. ABS. INTENSITY / VOLUME**2: 50.70992853 RIR: 3.008 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.12 5.75 7.9598 1 0 1 8 13.85 11.77 6.3951 1 1 0 4 14.41 12.96 6.1481 1 0 2 8 14.83 43.38 5.9752 1 1 1 8 17.44 4.20 5.0845 1 1 2 8 18.66 22.03 4.7542 1 0 3 8 20.34 8.24 4.3660 2 0 1 8 21.11 100.00 4.2082 1 1 3 8 21.20 33.06 4.1915 0 0 4 2 21.98 26.39 4.0446 2 1 0 8 22.34 2.80 3.9799 2 0 2 8 22.61 46.80 3.9318 2 1 1 8 23.39 14.87 3.8029 1 0 4 8 24.44 17.23 3.6428 2 1 2 8 25.34 4.36 3.5154 2 0 3 8 25.41 4.32 3.5056 1 1 4 8 27.22 19.45 3.2766 2 1 3 8 27.90 41.37 3.1975 2 2 0 4 28.39 4.30 3.1441 1 0 5 8 28.42 2.03 3.1409 2 2 1 8 29.91 94.47 2.9876 2 2 2 8 30.09 81.97 2.9697 1 1 5 8 30.12 12.06 2.9671 3 0 1 8 30.72 31.06 2.9105 2 1 4 8 31.54 52.17 2.8368 3 0 2 8 31.74 81.77 2.8192 3 1 1 8 32.25 1.78 2.7754 2 2 3 8 33.10 5.78 2.7068 3 1 2 8 33.78 20.87 2.6533 3 0 3 8 34.75 32.40 2.5814 2 1 5 8 35.25 24.69 2.5460 3 1 3 8 35.80 1.27 2.5084 3 2 0 8 36.21 2.97 2.4807 3 2 1 8 36.72 2.19 2.4474 3 0 4 8 37.42 2.33 2.4031 3 2 2 8 37.85 8.78 2.3771 2 0 6 8 38.09 2.26 2.3624 3 1 4 8 38.90 4.52 2.3153 1 0 7 8 39.18 6.24 2.2990 2 1 6 8 39.37 3.37 2.2884 3 2 3 8 39.87 8.86 2.2610 4 0 0 4 40.21 12.35 2.2430 1 1 7 8 41.15 6.04 2.1935 4 1 0 8 41.50 13.09 2.1760 3 1 5 8 41.52 12.10 2.1750 4 1 1 8 41.98 1.55 2.1524 3 2 4 8 42.40 1.89 2.1317 3 3 0 4 42.60 1.32 2.1221 4 1 2 8 42.76 2.77 2.1147 3 3 1 8 42.99 39.94 2.1041 2 2 6 8 43.17 15.54 2.0958 0 0 8 2 43.93 2.44 2.0609 2 1 7 8 44.19 9.76 2.0494 3 0 6 8 44.37 20.12 2.0419 4 1 3 8 44.37 6.38 2.0417 1 0 8 8 45.16 2.82 2.0077 4 2 1 8 45.38 2.50 1.9987 3 1 6 8 45.54 10.75 1.9917 3 3 3 8 45.59 24.98 1.9899 4 0 4 8 46.18 2.20 1.9659 4 2 2 8 46.74 10.83 1.9435 4 1 4 8 47.43 2.68 1.9170 2 2 7 8 47.83 1.78 1.9016 4 2 3 8 47.87 4.01 1.9001 3 3 4 8 48.55 5.58 1.8753 3 0 7 8 48.56 2.62 1.8747 4 0 5 8 48.79 4.16 1.8666 3 2 6 8 48.95 10.80 1.8608 2 1 8 8 49.65 3.51 1.8363 3 1 7 8 49.67 6.65 1.8356 4 1 5 8 50.08 2.82 1.8214 4 2 4 8 50.45 2.43 1.8088 4 3 0 8 50.75 33.04 1.7990 3 3 5 8 50.77 8.99 1.7984 4 3 1 8 51.70 11.04 1.7681 4 3 2 8 51.83 18.40 1.7638 5 1 1 8 52.18 1.55 1.7528 2 2 8 8 52.75 4.05 1.7353 5 1 2 8 52.85 1.11 1.7323 3 2 7 8 53.23 9.79 1.7209 4 3 3 8 54.21 13.08 1.6920 2 1 9 8 54.26 6.77 1.6906 5 1 3 8 54.26 1.45 1.6905 3 1 8 8 54.65 13.03 1.6794 5 2 0 8 54.95 6.36 1.6711 5 2 1 8 55.32 2.24 1.6608 4 3 4 8 56.14 1.79 1.6383 4 2 6 8 56.32 1.34 1.6334 5 1 4 8 56.92 6.05 1.6176 4 1 7 8 57.28 2.96 1.6084 5 2 3 8 57.66 11.30 1.5988 4 4 0 4 57.93 2.05 1.5920 4 3 5 8 57.94 1.70 1.5915 4 4 1 8 58.80 2.51 1.5705 4 4 2 8 59.19 11.39 1.5610 3 1 9 8 59.28 19.51 1.5589 5 2 4 8 59.70 5.22 1.5488 2 1 10 8 59.86 2.23 1.5452 4 2 7 8 59.89 1.17 1.5444 5 3 1 8 60.21 5.54 1.5370 4 0 8 8 61.02 6.84 1.5184 4 3 6 8 61.16 3.36 1.5153 4 1 8 8 61.72 2.68 1.5030 1 0 11 8 61.78 6.21 1.5016 5 2 5 8 61.97 1.83 1.4975 5 1 6 8 62.14 1.05 1.4938 4 4 4 8 62.56 7.87 1.4849 2 2 10 8 62.62 1.48 1.4835 6 0 2 8 62.66 8.29 1.4827 1 1 11 8 62.74 7.34 1.4810 6 1 1 8 63.49 3.36 1.4652 3 0 10 8 63.55 3.98 1.4640 6 1 2 8 63.98 3.39 1.4553 4 2 8 8 64.42 1.51 1.4464 3 1 10 8 64.56 5.20 1.4434 4 3 7 8 64.58 1.37 1.4431 4 4 5 8 64.85 1.62 1.4377 4 0 9 8 64.90 2.17 1.4368 6 1 3 8 65.48 9.21 1.4254 5 1 7 8 65.77 1.77 1.4199 4 1 9 8 66.31 4.19 1.4096 6 2 2 8 66.41 1.23 1.4077 5 3 5 8 66.68 1.38 1.4027 3 3 9 8 67.16 2.03 1.3939 3 2 10 8 67.50 1.50 1.3877 4 4 6 8 67.63 1.28 1.3854 6 2 3 8 67.88 1.56 1.3808 1 0 12 8 68.16 1.03 1.3759 2 2 11 8 68.20 1.07 1.3751 5 2 7 8 69.05 1.82 1.3602 3 0 11 8 69.11 3.61 1.3592 6 1 5 8 69.42 1.02 1.3539 5 1 8 8 69.45 4.47 1.3534 6 2 4 8 70.01 1.62 1.3439 6 3 1 8 70.72 1.15 1.3320 4 1 10 8 71.43 1.48 1.3206 2 1 12 8 71.94 2.53 1.3126 6 1 6 8 72.06 3.72 1.3106 6 3 3 8 72.06 6.80 1.3106 5 2 8 8 73.35 6.17 1.2907 4 2 10 8 74.28 6.50 1.2769 7 0 2 8 74.39 1.32 1.2753 5 5 1 8 74.54 3.07 1.2730 6 2 6 8 74.67 2.80 1.2711 4 4 8 8 75.14 2.77 1.2644 5 5 2 8 75.22 1.47 1.2632 6 1 7 8 75.41 1.43 1.2606 5 4 6 8 76.04 1.43 1.2517 4 1 11 8 76.09 1.79 1.2509 6 3 5 8 76.11 3.25 1.2507 6 4 1 8 76.35 3.00 1.2474 5 2 9 8 76.39 2.16 1.2468 5 5 3 8 76.89 1.06 1.2399 3 3 11 8 77.65 1.99 1.2296 4 3 10 8 77.72 3.25 1.2287 2 1 13 8 77.79 1.46 1.2278 6 2 7 8 78.10 2.71 1.2237 6 4 3 8 78.50 1.20 1.2184 5 1 10 8 79.50 1.09 1.2056 7 0 5 8 80.35 2.02 1.1950 5 5 5 8 80.35 3.08 1.1950 7 1 5 8 80.88 1.36 1.1885 4 0 12 8 80.96 2.17 1.1875 7 3 0 8 81.20 2.03 1.1846 7 3 1 8 81.95 2.36 1.1757 3 1 13 8 82.02 3.72 1.1749 6 3 7 8 82.03 2.39 1.1747 6 4 5 8 82.20 5.97 1.1727 7 0 6 8 82.82 4.21 1.1656 4 3 11 8 83.04 1.08 1.1630 7 1 6 8 83.04 2.32 1.1630 5 5 6 8 83.12 1.98 1.1621 6 1 9 8 83.51 1.17 1.1577 2 0 14 8 83.65 1.61 1.1560 5 1 11 8 84.23 2.43 1.1495 4 2 12 8 84.34 1.32 1.1483 2 1 14 8 84.46 1.53 1.1470 3 2 13 8 84.72 1.21 1.1442 6 4 6 8 84.87 3.09 1.1426 7 3 4 8 86.20 1.16 1.1282 5 5 7 8 86.90 5.19 1.1209 6 0 10 8 87.07 3.63 1.1193 8 1 1 8 87.37 1.12 1.1162 6 5 4 8 87.79 4.68 1.1119 7 4 2 8 88.64 2.11 1.1035 3 3 13 8 89.01 1.13 1.0998 8 1 3 8 89.01 1.13 1.0998 7 4 3 8 89.55 1.02 1.0945 6 5 5 8 89.56 1.78 1.0944 8 2 1 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.