Gustavite Makovicky E, Topa D European Journal of Mineralogy 23 (2011) 537-550 The crystal structure of gustavite, PbAgBi3S6 Analysis of twinning and polytypism using the OD approach Locality: Rotgulden, Lungau, Salzburg Land, Austria _database_code_amcsd 0018646 CELL PARAMETERS: 7.0567 19.6905 8.2219 90.000 106.961 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1092.741 Density (g/cm3): 6.845 MAX. ABS. INTENSITY / VOLUME**2: 127.8467924 RIR: 6.081 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.98 3.27 9.8453 0 2 0 2 13.87 3.04 6.3850 1 1 0 4 14.41 3.55 6.1446 0 2 1 4 15.27 1.36 5.8020 -1 1 1 4 15.92 2.94 5.5671 1 2 0 4 18.86 1.36 4.7056 1 3 0 4 22.35 19.95 3.9773 1 4 0 4 23.93 1.63 3.7185 1 3 1 4 24.37 17.83 3.6525 -1 2 2 4 24.38 17.71 3.6517 0 2 2 4 26.20 100.00 3.4015 1 5 0 4 26.41 16.78 3.3749 2 0 0 2 26.42 31.54 3.3738 -1 3 2 4 26.42 31.99 3.3731 0 3 2 4 26.80 21.68 3.3264 2 1 0 4 27.17 2.93 3.2817 0 6 0 2 27.95 7.26 3.1925 2 2 0 4 29.06 4.25 3.0728 -1 4 2 4 29.06 4.09 3.0723 0 4 2 4 29.78 27.29 3.0003 -2 1 2 4 29.79 27.07 2.9990 1 1 2 4 30.28 19.69 2.9514 1 6 0 4 30.82 36.69 2.9010 -2 2 2 4 30.84 36.66 2.8998 1 2 2 4 32.50 11.97 2.7553 -2 3 2 4 32.51 11.96 2.7543 1 3 2 4 33.07 1.15 2.7090 2 2 1 4 34.54 7.21 2.5965 1 7 0 4 39.38 11.10 2.2880 -1 7 2 4 39.38 11.09 2.2878 0 7 2 4 41.80 1.66 2.1608 2 7 0 4 42.34 5.52 2.1345 -3 3 2 4 42.36 5.52 2.1337 2 3 2 4 42.47 9.16 2.1283 3 3 0 4 43.37 15.22 2.0865 -1 8 2 4 43.37 15.01 2.0863 0 8 2 4 44.06 24.94 2.0555 -1 0 4 2 44.14 12.00 2.0518 -3 4 2 4 44.16 12.07 2.0511 2 4 2 4 44.26 14.50 2.0463 3 4 0 4 45.62 1.66 1.9886 2 8 0 4 46.10 11.20 1.9691 0 10 0 2 46.37 8.93 1.9583 -3 5 2 4 46.38 8.60 1.9577 2 5 2 4 46.48 3.23 1.9536 3 5 0 4 47.56 6.46 1.9119 -2 8 2 4 47.57 6.50 1.9115 1 8 2 4 48.98 3.45 1.8598 -3 6 2 4 48.99 3.51 1.8592 2 6 2 4 49.09 2.70 1.8557 3 6 0 4 49.66 6.11 1.8358 2 9 0 4 49.94 2.01 1.8262 -2 4 4 4 49.95 1.88 1.8258 0 4 4 4 51.49 3.51 1.7749 -2 9 2 4 51.50 3.57 1.7746 1 9 2 4 51.94 2.08 1.7605 -3 7 2 4 51.95 2.00 1.7600 2 7 2 4 51.97 13.02 1.7594 -2 5 4 4 51.99 13.10 1.7590 0 5 4 4 52.05 2.72 1.7570 3 7 0 4 52.09 2.44 1.7559 -3 0 4 2 52.11 2.45 1.7551 1 0 4 2 52.31 2.94 1.7489 -3 1 4 4 52.33 2.86 1.7482 1 1 4 4 52.40 4.58 1.7462 -4 0 2 2 52.42 4.50 1.7456 3 0 2 2 52.62 1.19 1.7394 -4 1 2 4 52.64 1.19 1.7388 3 1 2 4 52.92 1.72 1.7302 1 11 0 4 52.97 1.20 1.7286 -3 2 4 4 52.99 1.18 1.7279 1 2 4 4 53.91 7.52 1.7007 2 10 0 4 54.39 2.78 1.6869 -2 6 4 4 54.40 2.74 1.6866 0 6 4 4 54.58 2.05 1.6813 4 1 0 4 55.23 6.51 1.6632 4 2 0 4 56.29 1.91 1.6343 4 3 0 4 57.15 1.44 1.6117 -2 7 4 4 57.16 1.37 1.6115 0 7 4 4 62.84 2.42 1.4789 -4 3 4 4 62.87 2.34 1.4782 2 3 4 4 62.99 2.34 1.4757 2 12 0 4 64.21 3.76 1.4505 -4 4 4 4 64.24 3.64 1.4499 2 4 4 4 64.56 2.61 1.4435 -2 12 2 4 64.57 2.61 1.4434 1 12 2 4 65.66 6.53 1.4219 -1 10 4 4 65.98 1.03 1.4158 2 5 4 4 66.11 3.69 1.4135 -1 13 2 4 66.11 3.72 1.4134 0 13 2 4 67.27 3.00 1.3918 4 8 0 4 68.52 1.84 1.3694 -3 9 4 4 68.54 1.80 1.3690 1 9 4 4 68.78 1.21 1.3648 -4 9 2 4 68.80 1.23 1.3645 3 9 2 4 70.55 1.46 1.3349 -2 3 6 4 70.56 1.53 1.3348 -1 3 6 4 71.04 4.92 1.3269 -5 5 2 4 71.06 4.83 1.3265 4 5 2 4 71.33 1.76 1.3223 5 3 0 4 72.07 2.63 1.3105 -3 10 4 4 72.09 2.64 1.3102 1 10 4 4 72.22 1.31 1.3082 -3 1 6 4 72.24 1.29 1.3078 0 1 6 4 72.32 3.10 1.3065 -4 10 2 4 72.34 3.03 1.3062 3 10 2 4 72.77 2.09 1.2996 -3 2 6 4 72.79 2.09 1.2992 0 2 6 4 73.19 2.37 1.2932 -5 2 4 4 73.22 2.25 1.2927 3 2 4 4 73.49 2.84 1.2886 1 15 0 4 75.70 1.38 1.2565 3 13 0 4 77.86 1.04 1.2269 -2 7 6 4 77.87 1.03 1.2268 -1 7 6 4 80.29 1.05 1.1958 -4 12 2 4 80.30 1.01 1.1956 3 12 2 4 80.54 1.65 1.1926 -2 8 6 4 80.55 1.57 1.1925 -1 8 6 4 81.07 1.27 1.1862 -4 4 6 4 81.11 1.30 1.1857 1 4 6 4 81.28 1.17 1.1836 5 8 0 4 81.91 2.27 1.1761 -6 0 2 2 81.94 2.23 1.1758 5 0 2 2 82.67 1.20 1.1672 -4 5 6 4 82.70 1.07 1.1669 1 5 6 4 83.95 1.38 1.1526 -5 8 4 4 83.99 1.33 1.1522 3 8 4 4 89.84 1.48 1.0918 -2 15 4 4 89.84 1.51 1.0917 0 15 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.