data_global _chemical_name_mineral 'Disulfodadsonite' loop_ _publ_author_name 'Orlandi P' 'Biagioni C' 'Moelo Y' 'Bonaccorsi E' _journal_name_full 'European Journal of Mineralogy' _journal_volume 25 _journal_year 2013 _journal_page_first 1005 _journal_page_last 1016 _publ_section_title ; Lead-antimony sulfosalts from Tuscany (Italy). XIV. Disulfodadsonite, Pb11Sb13S30(S2)0.5, a new mineral from the Ceragiola marble quarry, Apuan Alps: occurrence and crystal structure ; _database_code_amcsd 0020026 _chemical_compound_source 'Ceragiola marble quarry, Apuan Alps, Tuscany, Italy' _chemical_formula_sum 'Pb5.38 Sb6.62 S15.5' _cell_length_a 4.1192 _cell_length_b 17.4167 _cell_length_c 19.1664 _cell_angle_alpha 96.127 _cell_angle_beta 90.015 _cell_angle_gamma 91.229 _cell_volume 1366.879 _exptl_crystal_density_diffrn 5.874 _symmetry_space_group_name_H-M 'P -1' loop_ _space_group_symop_operation_xyz 'x,y,z' '-x,-y,-z' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_U_iso_or_equiv Pb1 0.46940 0.17450 0.28460 1.00000 0.01990 Pb2 0.46780 0.75630 0.10340 1.00000 0.01880 Pb3 0.45530 0.26870 0.49620 1.00000 0.01860 Pb4 0.50010 0.11170 0.06820 1.00000 0.02610 Pb5 0.46450 0.65170 0.27940 1.00000 0.02190 Sb1 0.88980 0.54010 0.09210 0.71000 0.02400 Pb1 0.88980 0.54010 0.09210 0.29000 0.02400 Sb2a 0.95300 0.97300 0.21010 0.72000 0.03600 Sb2b 0.97700 0.95500 0.13520 0.28000 0.03600 Sb3 0.31730 0.47960 0.42080 1.00000 0.02000 Sb4 0.83950 0.40770 0.25050 0.91000 0.02600 Pb4 0.83950 0.40770 0.25050 0.09000 0.02600 Sb5 0.06520 0.85480 0.35580 1.00000 0.03700 Sb6 0.90350 0.67190 0.92110 1.00000 0.02700 Sb7 0.05300 0.05800 0.41800 0.10000 0.02700 Sb8 0.90500 0.06100 0.42900 0.90000 0.02700 S -0.00400 -0.01000 0.01910 0.50000 0.02700 S1 0.96500 0.39840 0.48420 1.00000 0.01900 S2 0.00800 0.72490 0.38890 1.00000 0.01600 S3 0.97900 0.78980 0.00240 1.00000 0.01300 S4 0.97200 0.19320 0.39660 1.00000 0.01600 S5 0.96900 0.66650 0.17370 1.00000 0.01300 S6 0.48300 0.61240 0.01600 1.00000 0.02200 S7 0.50400 0.81690 0.26790 1.00000 0.02500 S8 0.98400 0.10430 0.18490 1.00000 0.02000 S9a 0.50000 0.94330 0.12120 0.67000 0.06100 S9b 0.29000 0.93100 0.10100 0.33000 0.06100 S10 0.46100 0.49190 0.17890 1.00000 0.02100 S11 0.51000 0.27040 0.14640 1.00000 0.02000 S12 0.51600 0.89070 0.47050 1.00000 0.02700 S13 0.47900 0.02780 0.32820 1.00000 0.01800 S14 0.93800 0.52780 0.33230 1.00000 0.01300 S15 0.41500 0.35810 0.33020 1.00000 0.01600 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Pb1 0.02000 0.02700 0.01400 0.00200 -0.00300 0.00400 Pb2 0.02000 0.02400 0.01300 0.00300 0.00000 0.00500 Pb3 0.01700 0.02400 0.01500 0.00100 0.00000 0.00000 Pb4 0.02300 0.03400 0.02200 0.00300 -0.00300 0.00900 Pb5 0.01800 0.03700 0.01200 0.00700 0.00200 0.00800 Sb1 0.02800 0.02800 0.01600 -0.00500 -0.00200 0.01100 Pb1 0.02800 0.02800 0.01600 -0.00500 -0.00200 0.01100 Sb2a 0.06200 0.01900 0.02700 0.00500 -0.00800 0.00900 Sb2b 0.06200 0.01900 0.02700 0.00500 -0.00800 0.00900 Sb3 0.01700 0.02900 0.01500 -0.00400 -0.00500 0.01000 Sb4 0.03500 0.02500 0.01800 -0.00100 0.00600 0.00000 Pb4 0.03500 0.02500 0.01800 -0.00100 0.00600 0.00000 Sb5 0.05900 0.01600 0.03900 0.01100 0.02200 0.01000 Sb6 0.04400 0.02200 0.01400 0.01300 -0.01400 -0.00200 Sb7 0.03800 0.01900 0.02700 0.01000 -0.00100 0.00700 Sb8 0.03800 0.01900 0.02700 0.01000 -0.00100 0.00700 S 0.04000 0.01400 0.03000 0.00400 -0.01700 0.00400 S1 0.03200 0.01100 0.01500 -0.00100 0.01500 0.00200 S2 0.01900 0.01600 0.01400 0.00600 0.00300 -0.00200 S3 0.01300 0.02000 0.00700 0.00300 -0.00300 0.00600 S4 0.01900 0.01700 0.01200 0.00100 0.00300 0.00500 S5 0.00500 0.02600 0.00900 0.00800 0.00400 0.00600 S6 0.02300 0.01900 0.02200 -0.00200 0.00600 -0.00300 S7 0.04700 0.01400 0.01400 -0.00200 0.00800 -0.00100 S8 0.01100 0.03900 0.01100 0.00100 -0.00700 0.01500 S9a 0.14000 0.01400 0.02300 -0.00900 -0.04400 0.00500 S9b 0.14000 0.01400 0.02300 -0.00900 -0.04400 0.00500 S10 0.02500 0.02700 0.00900 -0.00300 0.00100 0.00000 S11 0.03900 0.01000 0.01200 0.00300 -0.01300 0.00300 S12 0.04100 0.02000 0.02000 0.00200 0.00700 0.00400 S13 0.02200 0.01700 0.01400 0.00000 -0.00900 0.00500 S14 0.01900 0.01400 0.00700 0.00000 -0.00600 0.00700 S15 0.02600 0.01400 0.00800 0.00000 0.01000 0.00200