Barbosalite Redhammer G J, Tippelt G, Roth G, Lottermoser W, Amthauer G Physics and Chemistry of Minerals 27 (2000) 419-429 Structure and Mossbauer spectroscopy of barbosalite Fe2+Fe3+2(PO4)2(OH)2 between 80 K and 300 K Sample: T = 110 K _database_code_amcsd 0008413 CELL PARAMETERS: 7.3065 7.5026 7.4105 90.000 118.490 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 357.033 Density (g/cm3): 3.641 MAX. ABS. INTENSITY / VOLUME**2: 21.79615187 RIR: 1.949 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.01 12.06 6.3229 -1 0 1 2 18.04 11.96 4.9184 0 1 1 4 18.35 41.86 4.8349 -1 1 1 4 23.65 3.42 3.7627 1 0 1 2 23.72 4.27 3.7513 0 2 0 2 26.50 100.00 3.3634 1 1 1 4 26.85 53.28 3.3206 -1 1 2 4 27.15 10.22 3.2841 -2 1 1 4 27.39 10.35 3.2565 0 0 2 2 27.44 28.69 3.2507 0 2 1 4 27.65 11.93 3.2262 -1 2 1 4 27.78 2.85 3.2108 2 0 0 2 28.23 28.13 3.1614 -2 0 2 2 30.28 1.60 2.9519 2 1 0 4 30.69 1.09 2.9133 -2 1 2 4 33.74 9.35 2.6566 1 2 1 4 34.26 13.76 2.6170 -2 2 1 4 36.54 4.88 2.4592 0 2 2 4 36.84 1.75 2.4399 -1 0 3 2 36.85 6.88 2.4393 2 2 0 4 37.19 5.70 2.4174 -2 2 2 4 37.45 4.84 2.4015 -3 0 1 2 38.56 8.84 2.3347 0 3 1 4 38.62 7.36 2.3315 2 1 1 4 38.64 2.96 2.3304 1 3 0 4 38.72 12.57 2.3256 -1 3 1 4 38.81 4.63 2.3203 -1 1 3 4 39.28 6.26 2.2937 -2 1 3 4 39.40 10.39 2.2872 -3 1 1 4 39.64 2.45 2.2736 -3 1 2 4 42.91 4.60 2.1076 -3 0 3 2 43.39 1.14 2.0855 0 1 3 4 43.45 11.15 2.0828 1 3 1 4 43.67 8.58 2.0725 -1 3 2 4 43.91 1.29 2.0619 1 2 2 4 43.99 4.06 2.0584 3 1 0 4 44.11 6.10 2.0530 2 2 1 4 44.29 1.75 2.0453 -1 2 3 4 44.66 13.86 2.0291 -3 1 3 4 44.71 2.91 2.0271 -2 2 3 4 48.38 4.23 1.8813 2 0 2 2 48.44 2.86 1.8790 0 2 3 4 48.54 8.72 1.8757 0 4 0 2 49.94 7.95 1.8263 -4 0 2 2 49.98 1.27 1.8248 2 1 2 4 50.71 1.61 1.8004 1 4 0 4 50.86 3.52 1.7953 3 0 1 2 51.50 1.54 1.7745 -4 1 2 4 51.94 6.17 1.7606 1 1 3 4 52.40 1.64 1.7462 -1 1 4 4 53.05 1.31 1.7263 -3 3 2 4 53.78 1.12 1.7045 -4 1 3 4 54.57 16.15 1.6817 2 2 2 4 55.33 18.48 1.6603 -2 2 4 4 56.10 2.34 1.6395 0 3 3 4 56.41 3.13 1.6310 1 2 3 4 56.52 3.45 1.6283 0 0 4 2 56.60 6.15 1.6262 3 3 0 4 56.63 19.60 1.6253 0 4 2 4 56.85 4.62 1.6196 2 4 0 4 57.16 9.75 1.6116 -3 3 3 4 57.40 8.58 1.6054 4 0 0 2 57.67 1.16 1.5984 -4 2 1 4 58.16 2.18 1.5861 -4 2 3 4 58.38 8.81 1.5807 -4 0 4 2 58.82 1.70 1.5699 4 1 0 4 62.87 2.75 1.4782 -3 4 1 4 63.03 1.07 1.4749 -4 3 2 4 63.34 1.03 1.4684 2 1 3 4 63.41 6.19 1.4669 1 3 3 4 63.46 1.03 1.4658 -3 0 5 2 63.59 2.37 1.4631 3 1 2 4 63.75 1.67 1.4600 -1 5 1 4 63.82 1.32 1.4585 -1 3 4 4 63.82 1.51 1.4584 3 3 1 4 64.58 1.55 1.4431 -4 3 1 4 64.81 4.68 1.4386 -3 1 5 4 65.04 1.39 1.4340 -4 3 3 4 65.62 1.65 1.4227 -5 1 3 4 66.76 1.60 1.4011 -3 4 3 4 67.16 2.98 1.3938 1 5 1 4 67.33 1.41 1.3907 2 2 3 4 67.35 1.63 1.3904 -1 1 5 4 67.48 2.23 1.3880 -2 5 1 4 68.23 1.27 1.3745 -2 2 5 4 68.54 1.58 1.3691 -5 1 1 4 69.55 1.89 1.3517 -5 2 3 4 71.46 1.48 1.3201 4 2 1 4 71.61 2.19 1.3177 -2 4 4 4 72.20 13.54 1.3085 -4 4 2 4 72.39 2.53 1.3054 -5 2 1 4 74.07 1.85 1.2800 2 5 1 4 74.50 1.41 1.2737 -2 5 3 4 75.12 1.06 1.2646 -3 3 5 4 77.10 1.54 1.2371 3 1 3 4 77.52 2.60 1.2314 -1 3 5 4 77.72 1.18 1.2287 3 5 0 4 78.20 1.95 1.2224 -3 5 3 4 78.64 2.60 1.2166 -5 3 1 4 80.08 1.04 1.1983 -5 2 5 4 82.24 5.09 1.1722 2 2 4 4 83.70 1.16 1.1555 1 5 3 4 84.07 1.73 1.1514 -1 5 4 4 84.57 1.47 1.1459 5 1 1 4 87.99 1.23 1.1098 -2 6 3 4 88.20 1.89 1.1078 5 2 1 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.