Meridianiite Fortes A D, Wood I G, Knight K S Physics and Chemistry of Minerals 35 (2008) 207-221 The crystal structure and thermal expansion tensor of MgSO4-11D2O (meridianiite) determined by neutron powder diffraction Note: T = 4.2 K Locality: synthetic _database_code_amcsd 0009133 CELL PARAMETERS: 6.7275 6.7814 17.3180 88.206 89.447 62.608 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 701.142 Density (g/cm3): 1.509 MAX. ABS. INTENSITY / VOLUME**2: 1.527665590 RIR: 0.330 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 5.11 14.49 17.3093 0 0 1 2 10.22 1.15 8.6546 0 0 2 2 14.72 9.45 6.0183 0 1 0 2 14.83 1.46 5.9731 1 0 0 2 15.36 25.69 5.7698 0 0 3 2 15.36 8.43 5.7693 1 1 0 2 15.44 26.09 5.7386 0 1 1 2 15.67 3.80 5.6557 -1 0 1 2 15.72 22.62 5.6371 1 0 1 2 15.74 25.68 5.6319 0 -1 1 2 16.08 34.16 5.5128 1 1 1 2 16.31 52.16 5.4346 -1 -1 1 2 17.69 22.39 5.0127 0 1 2 2 18.00 83.04 4.9283 -1 0 2 2 18.09 25.28 4.9037 1 0 2 2 18.21 95.23 4.8725 0 -1 2 2 18.28 65.61 4.8542 1 1 2 2 18.69 1.16 4.7485 -1 -1 2 2 20.52 14.73 4.3273 0 0 4 2 21.00 19.91 4.2294 0 1 3 2 21.35 13.29 4.1610 -1 0 3 2 21.47 11.64 4.1388 1 0 3 2 21.52 9.09 4.1292 1 1 3 2 21.66 3.18 4.1034 0 -1 3 2 22.05 13.77 4.0319 -1 -1 3 2 24.98 43.45 3.5649 0 1 4 2 25.39 43.38 3.5086 -1 1 0 2 25.43 2.51 3.5021 1 1 4 2 25.48 20.43 3.4955 1 0 4 2 25.72 9.05 3.4641 0 -1 4 2 25.73 8.20 3.4619 0 0 5 2 25.80 7.10 3.4527 -1 1 1 2 26.03 50.69 3.4228 -1 -1 4 2 26.33 36.24 3.3849 1 2 0 2 26.52 100.00 3.3608 2 1 0 2 26.97 5.36 3.3059 2 1 1 2 27.00 14.78 3.3028 -1 -2 1 2 28.01 2.82 3.1861 1 2 2 2 28.38 13.50 3.1444 2 1 2 2 28.60 16.30 3.1214 -2 -1 2 2 29.37 2.36 3.0408 0 1 5 2 29.52 54.10 3.0259 -1 1 3 2 29.76 28.75 3.0021 -1 0 5 2 29.78 62.81 3.0002 1 1 5 2 29.90 19.32 2.9882 1 0 5 2 29.92 4.14 2.9866 2 0 0 2 29.99 20.04 2.9799 0 2 1 2 30.08 21.26 2.9706 1 -1 3 2 30.19 17.64 2.9599 1 2 3 2 30.30 65.24 2.9497 0 -2 1 2 30.34 21.11 2.9457 -2 0 1 2 30.40 17.26 2.9404 2 0 1 2 30.43 4.45 2.9377 -1 -1 5 2 31.00 1.41 2.8849 0 0 6 2 31.00 2.29 2.8846 2 2 0 2 31.04 23.38 2.8809 -1 -2 3 2 31.17 35.91 2.8693 0 2 2 2 31.31 23.34 2.8565 2 2 1 2 31.56 1.50 2.8345 -2 -2 1 2 31.64 2.50 2.8279 -2 0 2 2 31.75 3.18 2.8185 2 0 2 2 32.52 1.39 2.7535 -1 1 4 2 32.96 5.53 2.7173 -2 -2 2 2 33.16 1.01 2.7018 0 2 3 2 33.72 2.89 2.6581 -2 0 3 2 33.87 2.85 2.6465 2 0 3 2 33.95 7.22 2.6404 -2 -1 4 2 34.02 2.22 2.6356 0 -2 3 2 34.05 3.18 2.6327 0 1 6 2 34.13 2.33 2.6269 -1 -2 4 2 34.42 15.77 2.6052 1 1 6 2 34.43 2.61 2.6051 2 2 3 2 34.60 10.85 2.5923 1 0 6 2 35.11 11.22 2.5560 -1 -1 6 2 36.33 1.84 2.4728 0 0 7 2 36.46 3.33 2.4642 -2 0 4 2 36.55 9.09 2.4586 1 2 5 2 36.85 4.55 2.4391 1 -1 5 2 36.90 24.69 2.4362 0 -2 4 2 37.04 4.04 2.4271 2 2 4 2 37.08 3.29 2.4246 2 1 5 2 37.50 2.81 2.3984 -2 -1 5 2 37.74 3.77 2.3836 -1 -2 5 2 37.89 1.32 2.3743 -2 -2 4 2 38.96 3.43 2.3119 0 1 7 2 39.30 1.45 2.2927 1 1 7 2 39.36 4.48 2.2890 -1 0 7 2 39.37 2.37 2.2887 -2 1 0 2 39.46 3.16 2.2838 -1 2 1 2 39.52 14.76 2.2804 1 0 7 2 39.64 8.04 2.2736 -2 1 1 2 39.81 6.07 2.2643 2 -1 1 2 39.97 1.44 2.2554 2 0 5 2 40.05 5.30 2.2514 -1 1 6 2 40.38 1.04 2.2334 -1 2 2 2 40.48 1.34 2.2281 1 3 1 2 40.91 3.47 2.2060 1 -1 6 2 40.91 8.94 2.2058 1 -2 2 2 40.95 3.81 2.2041 2 -1 2 2 41.01 5.15 2.2009 2 1 6 2 41.03 1.42 2.1996 -3 -1 1 2 41.21 4.39 2.1906 -2 -2 5 2 41.29 1.75 2.1867 3 2 0 2 41.57 11.46 2.1723 -2 -3 1 2 41.72 9.54 2.1651 -3 -2 1 2 41.75 5.75 2.1637 0 0 8 2 42.03 5.51 2.1499 -1 -3 2 2 42.25 11.49 2.1389 -2 1 3 2 42.47 4.49 2.1282 3 2 2 2 42.74 5.51 2.1155 -2 -3 2 2 42.82 1.83 2.1120 -3 -2 2 2 43.79 8.95 2.0675 -3 -1 3 2 43.86 9.59 2.0642 -1 -3 3 2 44.04 18.23 2.0560 0 1 8 2 44.05 10.48 2.0558 3 2 3 2 44.46 3.37 2.0378 -1 0 8 2 44.49 10.66 2.0363 -2 1 4 2 44.54 7.42 2.0341 -2 -3 3 2 44.71 2.35 2.0269 1 2 7 2 44.95 6.94 2.0167 0 -1 8 2 45.02 2.50 2.0138 1 3 4 2 45.10 3.83 2.0102 2 -1 4 2 45.30 7.55 2.0017 1 -1 7 2 45.35 1.08 1.9997 0 3 1 2 45.56 2.41 1.9910 3 0 0 2 45.68 5.63 1.9859 0 -3 1 2 45.75 2.21 1.9830 2 3 4 2 45.85 2.77 1.9792 -3 0 1 2 45.86 14.38 1.9787 3 1 4 2 45.91 7.98 1.9768 3 0 1 2 46.06 3.61 1.9704 -3 -1 4 2 46.13 2.26 1.9679 -1 -2 7 2 46.14 3.42 1.9674 0 3 2 2 46.26 2.74 1.9623 -1 -3 4 2 46.76 3.36 1.9426 -3 0 2 2 46.79 2.28 1.9414 0 -3 2 2 46.85 18.14 1.9391 -3 -2 4 2 46.88 2.77 1.9381 3 0 2 2 46.91 4.94 1.9368 -2 -3 4 2 47.26 2.93 1.9233 0 0 9 2 47.27 15.56 1.9231 3 3 0 2 47.44 2.04 1.9164 3 3 1 2 47.53 1.76 1.9129 0 3 3 2 47.62 14.20 1.9097 -2 0 7 2 48.10 16.14 1.8918 1 -2 5 2 48.49 3.13 1.8773 0 -3 3 2 48.87 2.68 1.8638 -3 -1 5 2 48.91 4.43 1.8624 3 2 5 2 49.00 2.98 1.8590 -1 1 8 2 49.18 1.37 1.8526 -1 -3 5 2 49.28 9.40 1.8492 1 2 8 2 49.30 3.47 1.8483 0 1 9 2 49.61 11.99 1.8376 3 3 3 2 49.67 1.13 1.8355 -3 -2 5 2 49.73 5.30 1.8336 -1 0 9 2 49.79 1.21 1.8314 -2 -3 5 2 49.88 3.71 1.8283 2 1 8 2 49.89 1.03 1.8278 1 0 9 2 49.98 1.65 1.8248 1 -1 8 2 50.24 2.10 1.8161 0 -1 9 2 50.56 1.01 1.8051 3 0 4 2 50.74 1.02 1.7994 0 -3 4 2 50.78 2.53 1.7979 -1 -2 8 2 50.84 4.01 1.7959 1 3 6 2 51.48 7.07 1.7750 1 -2 6 2 51.53 4.11 1.7734 2 3 6 2 51.54 1.51 1.7731 3 3 4 2 51.85 2.27 1.7633 3 1 6 2 52.07 3.54 1.7563 3 2 6 2 52.14 4.72 1.7543 -2 2 0 2 52.24 2.43 1.7510 2 2 8 2 52.55 1.81 1.7415 -1 -3 6 2 52.90 3.88 1.7309 0 0 10 2 53.05 1.18 1.7264 -2 2 2 2 53.88 1.69 1.7015 -1 1 9 2 54.19 2.33 1.6925 2 4 0 2 54.34 7.48 1.6882 -2 2 3 2 54.42 1.43 1.6860 1 3 7 2 54.62 4.25 1.6804 4 2 0 2 54.65 1.44 1.6794 -2 -4 1 2 54.73 5.02 1.6771 2 1 9 2 54.82 1.61 1.6745 -3 1 0 2 54.92 1.61 1.6719 1 -1 9 2 54.96 1.12 1.6708 2 4 2 2 54.98 2.52 1.6702 1 -3 1 2 55.02 1.52 1.6689 1 1 10 2 55.35 5.30 1.6599 -1 3 2 2 55.50 2.19 1.6558 3 1 7 2 55.66 2.74 1.6514 -2 -4 2 2 55.70 1.48 1.6503 0 -1 10 2 55.96 1.25 1.6432 1 -3 2 2 56.17 8.38 1.6375 -1 -4 1 2 56.23 1.12 1.6359 4 1 0 2 56.32 1.40 1.6335 -1 -3 7 2 56.45 1.23 1.6302 1 4 2 2 56.80 1.76 1.6209 -2 0 9 2 57.06 4.08 1.6142 2 -2 4 2 57.19 1.73 1.6106 -2 -4 3 2 57.47 2.17 1.6036 1 -3 3 2 57.81 2.22 1.5949 -1 2 8 2 57.88 1.25 1.5930 2 4 4 2 58.06 2.87 1.5887 3 4 2 2 58.22 4.14 1.5847 -2 1 8 2 58.29 1.09 1.5828 -3 -3 6 2 58.40 2.04 1.5801 4 3 2 2 58.73 1.00 1.5722 4 2 4 2 58.83 4.30 1.5698 -4 -3 2 2 58.88 1.70 1.5685 -3 1 4 2 59.01 2.78 1.5653 -1 1 10 2 59.20 3.16 1.5609 1 2 10 2 59.23 1.15 1.5601 3 4 3 2 59.45 1.93 1.5549 -3 0 7 2 59.48 4.21 1.5540 1 -3 4 2 59.86 1.14 1.5451 -3 -1 8 2 60.09 2.64 1.5397 1 -1 10 2 60.25 1.80 1.5360 -4 -3 3 2 60.45 2.05 1.5314 4 1 4 2 60.56 2.23 1.5290 -4 -1 4 2 60.71 1.92 1.5256 -1 -4 4 2 60.86 1.30 1.5221 -1 -2 10 2 61.27 5.47 1.5130 -2 2 6 2 61.86 1.31 1.4998 3 -1 5 2 62.18 2.91 1.4930 -1 2 9 2 62.45 1.79 1.4871 4 0 1 2 62.79 1.24 1.4800 2 4 6 2 63.03 2.15 1.4748 0 -4 2 2 63.32 1.18 1.4687 2 3 9 2 63.69 1.04 1.4612 3 0 8 2 64.48 5.32 1.4452 -4 -2 6 2 64.60 1.41 1.4428 -3 -4 5 2 65.01 2.08 1.4347 0 4 4 2 65.01 1.21 1.4345 -4 -4 1 2 65.19 3.31 1.4311 2 1 11 2 65.41 1.24 1.4268 -2 -3 9 2 65.53 3.98 1.4244 4 1 6 2 66.08 1.29 1.4139 -4 0 4 2 66.30 1.08 1.4098 0 3 9 2 66.33 1.04 1.4093 4 0 4 2 66.62 2.04 1.4039 -1 0 12 2 66.80 1.76 1.4004 1 0 12 2 67.19 2.89 1.3932 0 -1 12 2 67.21 1.06 1.3929 1 4 7 2 67.40 1.28 1.3895 -4 -3 6 2 67.51 2.31 1.3875 2 -3 1 2 67.95 1.32 1.3796 3 0 9 2 67.95 1.00 1.3796 2 3 10 2 68.04 1.38 1.3780 -3 2 2 2 68.39 1.41 1.3718 2 -3 2 2 68.60 1.09 1.3680 3 2 10 2 68.78 1.00 1.3649 0 -4 5 2 68.89 1.41 1.3629 -2 3 3 2 68.90 2.65 1.3628 -4 -1 7 2 69.31 1.40 1.3557 4 3 7 2 70.12 1.02 1.3421 5 2 0 2 70.42 1.30 1.3371 3 5 1 2 70.45 3.88 1.3366 -2 3 4 2 70.59 1.91 1.3342 4 2 8 2 70.79 3.75 1.3310 -3 -5 1 2 70.84 3.97 1.3302 -2 -5 2 2 71.41 1.19 1.3210 -1 4 1 2 71.70 1.18 1.3163 0 2 12 2 71.95 2.07 1.3124 -1 -2 12 2 72.02 1.31 1.3112 1 -3 8 2 72.42 2.12 1.3050 -5 -2 3 2 72.58 1.24 1.3026 4 4 6 2 73.69 1.28 1.2856 0 -2 12 2 73.86 1.62 1.2831 1 -2 11 2 73.87 1.42 1.2829 2 -2 9 2 74.00 1.03 1.2809 1 -4 3 2 74.13 1.79 1.2791 -5 -2 4 2 74.31 1.16 1.2764 -5 -1 2 2 74.33 2.00 1.2761 -4 -3 8 2 74.59 2.75 1.2723 4 2 9 2 75.00 2.26 1.2663 -5 -3 4 2 75.39 2.45 1.2608 3 5 5 2 75.49 1.21 1.2593 -5 -1 3 2 75.49 1.12 1.2593 5 4 0 2 75.90 2.56 1.2535 -1 1 13 2 76.34 2.42 1.2475 5 3 5 2 76.39 1.46 1.2468 -2 -5 5 2 76.54 1.04 1.2446 -4 -1 9 2 76.58 1.23 1.2442 2 -3 6 2 77.70 1.80 1.2290 -2 1 12 2 78.20 1.51 1.2224 2 3 12 2 78.36 1.01 1.2203 5 2 6 2 78.42 2.06 1.2195 2 -2 10 2 78.79 1.97 1.2147 -1 4 6 2 78.88 2.03 1.2135 4 4 8 2 79.00 1.42 1.2120 -1 0 14 2 79.01 1.59 1.2118 2 -1 12 2 79.14 1.70 1.2102 -2 -5 6 2 79.43 2.16 1.2065 -3 -1 12 2 79.65 1.39 1.2037 -4 -5 4 2 79.89 2.21 1.2007 1 5 6 2 80.01 1.18 1.1992 -4 -2 10 2 80.18 1.76 1.1971 0 5 2 2 80.38 1.43 1.1946 5 0 0 2 80.61 1.81 1.1918 -2 -4 10 2 80.71 1.19 1.1905 1 -3 10 2 81.17 1.14 1.1850 -2 3 8 2 82.87 1.25 1.1650 -1 3 11 2 83.91 2.32 1.1531 -5 0 4 2 84.11 1.34 1.1509 -3 3 3 2 84.43 1.56 1.1473 5 5 2 2 84.93 1.50 1.1419 -2 4 2 2 84.95 1.24 1.1416 3 -3 3 2 85.16 1.42 1.1394 3 -1 11 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.