Palladseite Geller S Acta Crystallographica 15 (1962) 713-721 The crystal structure of Pd17Se15 Locality: synthetic Sample: P432 refinement _database_code_amcsd 0009273 CELL PARAMETERS: 10.6060 10.6060 10.6060 90.000 90.000 90.000 SPACE GROUP: P432 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1193.040 Density (g/cm3): 8.332 MAX. ABS. INTENSITY / VOLUME**2: 109.2630519 RIR: 4.270 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 16.72 3.66 5.3030 2 0 0 6 18.71 2.10 4.7431 2 1 0 24 23.73 3.67 3.7498 2 2 0 12 25.19 2.90 3.5353 2 2 1 24 26.58 38.83 3.3539 3 1 0 24 27.90 78.85 3.1978 3 1 1 24 29.17 3.09 3.0617 2 2 2 8 30.39 16.89 2.9416 3 2 0 24 31.56 51.54 2.8346 3 2 1 24 33.81 1.02 2.6515 4 0 0 6 34.88 45.33 2.5723 4 1 0 24 34.88 17.81 2.5723 3 2 2 24 35.92 30.41 2.4999 4 1 1 24 36.94 23.61 2.4332 3 3 1 24 37.94 22.74 2.3716 4 2 0 24 38.91 22.46 2.3144 4 2 1 24 42.62 5.25 2.1212 4 3 0 24 42.62 4.96 2.1212 5 0 0 6 43.51 5.38 2.0800 5 1 0 24 43.51 6.52 2.0800 4 3 1 24 44.38 6.43 2.0411 5 1 1 24 44.38 70.73 2.0411 3 3 3 8 46.92 1.03 1.9364 5 2 1 24 48.56 100.00 1.8749 4 4 0 12 49.36 1.81 1.8463 5 2 2 24 50.15 2.07 1.8189 5 3 0 24 50.15 6.57 1.8189 4 3 3 24 51.71 36.09 1.7677 6 0 0 6 52.48 4.15 1.7436 6 1 0 24 53.24 6.39 1.7205 6 1 1 24 53.24 10.95 1.7205 5 3 2 24 54.74 5.96 1.6770 6 2 0 24 55.48 4.50 1.6564 6 2 1 24 55.48 8.09 1.6564 5 4 0 24 55.48 6.36 1.6564 4 4 3 24 56.21 16.67 1.6365 5 4 1 24 56.93 3.18 1.6174 5 3 3 24 58.37 2.98 1.5810 6 3 0 24 58.37 4.15 1.5810 5 4 2 24 60.48 2.93 1.5308 4 4 4 8 61.17 1.47 1.5151 7 0 0 6 61.86 3.15 1.4999 7 1 0 24 61.86 2.27 1.4999 5 5 0 12 62.54 1.32 1.4851 5 5 1 24 63.22 4.63 1.4708 6 4 0 24 63.90 2.25 1.4568 6 4 1 24 64.57 1.07 1.4433 7 2 1 24 66.57 1.48 1.4048 5 4 4 24 67.22 1.99 1.3926 7 3 0 24 67.88 22.41 1.3808 7 3 1 24 69.18 5.10 1.3580 6 4 3 24 69.83 3.26 1.3470 7 3 2 24 69.83 3.09 1.3470 6 5 1 24 71.11 9.73 1.3257 8 0 0 6 71.75 1.92 1.3155 7 4 0 24 72.39 7.15 1.3055 5 5 4 24 72.39 3.16 1.3055 7 4 1 24 72.39 1.23 1.3055 8 1 1 24 73.02 11.22 1.2957 7 3 3 24 73.65 10.87 1.2862 6 4 4 24 74.28 3.88 1.2768 7 4 2 24 74.28 1.60 1.2768 8 2 1 24 74.91 1.65 1.2677 6 5 3 24 76.16 8.24 1.2499 6 6 0 12 77.41 6.16 1.2329 7 4 3 24 78.02 5.02 1.2247 7 5 1 24 79.88 1.38 1.2009 7 5 2 24 81.10 4.24 1.1858 8 4 0 24 81.72 2.15 1.1784 7 4 4 24 82.33 4.61 1.1712 9 1 0 24 83.55 4.74 1.1572 8 4 2 24 84.16 2.70 1.1504 7 6 0 24 84.76 3.27 1.1437 9 2 1 24 84.76 4.58 1.1437 7 6 1 24 85.98 4.26 1.1306 6 6 4 24 86.59 1.79 1.1242 8 5 0 24 86.59 5.01 1.1242 7 6 2 24 87.19 3.85 1.1180 8 5 1 24 87.19 2.96 1.1180 9 3 0 24 89.01 1.53 1.0998 8 5 2 24 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.