Melanterite Baur W H Acta Crystallographica 17 (1964) 1167-1174 On the crystal chemistry of salt hydrates. III. The determination of the crystal structure of FeSO4*7H2O (melanterite) Locality: synthetic _database_code_amcsd 0009289 CELL PARAMETERS: 14.0720 6.5030 11.0410 90.000 105.570 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 973.287 Density (g/cm3): 1.897 MAX. ABS. INTENSITY / VOLUME**2: 8.628239120 RIR: 1.481 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.06 4.97 6.7778 2 0 0 2 15.11 2.09 5.8632 1 1 0 4 15.97 7.39 5.5481 0 1 1 4 16.19 14.71 5.4754 -1 0 2 2 16.39 3.34 5.4069 -1 1 1 4 16.67 6.68 5.3179 0 0 2 2 18.10 100.00 4.8998 1 1 1 4 18.23 55.88 4.8659 -2 0 2 2 19.50 9.41 4.5525 1 0 2 2 22.08 11.50 4.0258 2 1 1 4 23.59 61.83 3.7717 -3 1 1 4 23.88 17.68 3.7262 2 0 2 2 26.30 4.88 3.3889 4 0 0 2 27.14 4.13 3.2856 3 1 1 4 27.43 24.80 3.2515 0 2 0 2 27.85 14.44 3.2029 -1 1 3 4 28.60 6.95 3.1214 -2 1 3 4 28.68 1.67 3.1127 0 1 3 4 28.71 2.29 3.1094 0 2 1 4 28.95 1.97 3.0839 -1 2 1 4 29.17 5.77 3.0617 3 0 2 2 29.73 7.44 3.0053 4 1 0 4 30.48 5.25 2.9324 -4 1 2 4 30.49 1.42 2.9316 2 2 0 4 30.80 1.46 2.9028 -3 1 3 4 32.01 7.45 2.7957 -1 2 2 4 32.32 4.76 2.7700 3 1 2 4 32.53 7.36 2.7525 -1 0 4 2 32.61 1.18 2.7457 2 2 1 4 32.81 3.30 2.7300 -5 0 2 2 32.84 12.63 2.7272 4 1 1 4 33.71 4.84 2.6590 0 0 4 2 33.88 7.16 2.6459 1 2 2 4 33.97 5.15 2.6392 3 2 0 4 34.21 8.69 2.6207 -4 1 3 4 34.23 2.17 2.6195 -3 0 4 2 34.42 1.20 2.6054 2 1 3 4 35.01 1.87 2.5631 4 0 2 2 35.52 2.05 2.5271 -3 2 2 4 35.67 1.66 2.5172 -5 1 2 4 35.89 1.97 2.5024 5 1 0 4 36.13 6.66 2.4862 1 0 4 2 36.33 3.77 2.4725 3 2 1 4 36.68 1.07 2.4499 2 2 2 4 36.95 3.07 2.4330 -4 0 4 2 37.00 2.93 2.4298 -3 1 4 4 37.53 4.47 2.3963 0 2 3 4 37.70 1.00 2.3863 -4 2 1 4 38.36 2.38 2.3462 4 2 0 4 38.56 1.63 2.3350 -5 1 3 4 38.81 1.11 2.3206 3 1 3 4 38.90 4.08 2.3150 -6 0 2 2 38.96 3.84 2.3115 5 1 1 4 38.97 3.07 2.3110 -4 2 2 4 39.23 1.26 2.2965 -3 2 3 4 39.59 1.64 2.2763 2 0 4 2 39.90 1.19 2.2593 6 0 0 2 40.65 1.14 2.2194 -5 0 4 2 41.40 2.51 2.1809 -6 1 2 4 42.74 1.70 2.1158 -1 3 1 4 43.20 1.13 2.0942 -2 2 4 4 43.48 4.32 2.0814 1 3 1 4 43.54 3.50 2.0785 -1 1 5 4 43.99 1.20 2.0583 0 2 4 4 44.16 2.88 2.0508 -3 1 5 4 44.83 2.95 2.0218 0 1 5 4 44.98 2.68 2.0155 -1 3 2 4 45.04 5.19 2.0129 4 2 2 4 45.15 2.44 2.0081 -6 0 4 2 46.24 11.66 1.9632 -3 3 1 4 46.63 2.12 1.9480 -4 2 4 4 47.11 4.26 1.9291 1 1 5 4 47.51 3.58 1.9136 -7 1 1 4 47.78 1.07 1.9036 6 0 2 2 48.26 3.97 1.8859 -6 2 2 4 48.32 4.60 1.8837 3 3 1 4 48.76 1.51 1.8678 -1 3 3 4 48.84 5.33 1.8647 2 2 4 4 48.84 2.95 1.8646 -5 1 5 4 48.89 1.53 1.8631 4 0 4 2 49.10 2.50 1.8554 6 2 0 4 49.21 2.85 1.8516 -7 1 3 4 49.52 3.29 1.8408 5 1 3 4 49.54 1.79 1.8401 -2 0 6 2 49.97 2.42 1.8251 -3 0 6 2 50.65 1.74 1.8023 -3 3 3 4 50.75 1.61 1.7990 1 3 3 4 51.36 1.16 1.7791 -4 0 6 2 52.02 1.22 1.7578 4 3 1 4 52.16 3.28 1.7535 7 1 1 4 53.64 3.52 1.7085 -6 2 4 4 54.13 1.80 1.6945 8 0 0 2 54.23 3.43 1.6916 3 1 5 4 55.21 1.21 1.6638 7 2 0 4 56.14 1.12 1.6383 -5 3 3 4 56.45 1.38 1.6301 5 3 1 4 56.61 2.07 1.6257 0 4 0 2 56.83 2.12 1.6201 -7 1 5 4 57.55 1.83 1.6015 -2 2 6 4 59.20 1.36 1.5607 -4 2 6 4 59.38 3.86 1.5564 0 2 6 4 59.99 1.54 1.5420 -2 4 2 4 60.00 1.17 1.5418 -1 3 5 4 60.54 2.67 1.5293 -3 1 7 4 61.73 1.60 1.5026 8 2 0 4 61.78 2.45 1.5016 -9 1 3 4 63.44 1.23 1.4662 -8 2 4 4 63.46 1.84 1.4658 4 4 0 4 64.89 1.04 1.4370 5 3 3 4 65.19 1.54 1.4310 1 1 7 4 68.85 1.08 1.3636 8 2 2 4 68.92 1.10 1.3625 3 3 5 4 69.54 1.27 1.3517 -4 4 4 4 70.82 1.21 1.3304 -6 4 2 4 72.57 1.91 1.3027 4 2 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.