Boussingaultite Montgomery H, Lingafelter E C Acta Crystallographica 17 (1964) 1478-1479 The crystal structure of Tutton's salts. II. Magnesium ammonium sulfate hexahydrate and nickel ammonium sulfate hexahydrate Locality: synthetic _database_code_amcsd 0020241 CELL PARAMETERS: 9.3830 12.6690 6.2200 90.000 107.050 90.000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 Cell Volume: 706.895 Density (g/cm3): 1.694 MAX. ABS. INTENSITY / VOLUME**2: 3.258555921 RIR: 0.626 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.09 3.90 7.3211 1 1 0 4 13.98 7.97 6.3345 0 2 0 2 14.90 8.51 5.9466 0 0 1 2 16.47 86.94 5.3831 0 1 1 4 17.14 38.47 5.1745 1 2 0 4 19.79 14.88 4.4853 2 0 0 2 20.48 8.85 4.3355 0 2 1 4 20.76 48.52 4.2783 -1 2 1 4 21.01 53.59 4.2281 2 1 0 4 21.02 82.95 4.2258 -2 0 1 2 21.39 44.63 4.1548 1 1 1 4 22.18 9.26 4.0087 -2 1 1 4 23.28 100.00 3.8208 1 3 0 4 24.32 1.21 3.6606 2 2 0 4 24.64 19.05 3.6127 1 2 1 4 25.88 18.60 3.4431 0 3 1 4 26.10 13.25 3.4142 -1 3 1 4 28.17 40.27 3.1672 0 4 0 2 28.22 27.68 3.1627 2 0 1 2 29.04 3.50 3.0747 2 3 0 4 29.10 28.34 3.0686 2 1 1 4 29.32 4.21 3.0461 1 3 1 4 29.60 50.78 3.0181 -1 1 2 4 29.91 5.52 2.9871 -2 3 1 4 30.05 3.63 2.9733 0 0 2 2 30.09 14.78 2.9700 -3 1 1 4 30.72 3.75 2.9102 3 1 0 4 30.83 17.26 2.9007 -2 0 2 2 30.89 3.92 2.8947 0 1 2 4 31.62 17.55 2.8296 2 2 1 4 31.64 2.25 2.8275 -2 1 2 4 32.02 3.16 2.7955 0 4 1 4 32.08 39.66 2.7899 -1 2 2 4 32.20 3.72 2.7799 -1 4 1 4 32.54 18.08 2.7518 -3 2 1 4 33.13 1.31 2.7041 3 2 0 4 33.29 1.83 2.6916 0 2 2 4 34.67 2.05 2.5872 2 4 0 4 34.91 9.51 2.5702 1 4 1 4 35.42 2.59 2.5344 -2 4 1 4 35.46 14.88 2.5315 2 3 1 4 35.88 1.39 2.5029 -1 3 2 4 36.29 33.25 2.4753 -3 3 1 4 36.98 3.13 2.4312 0 3 2 4 37.62 2.24 2.3910 -2 3 2 4 38.63 2.23 2.3310 0 5 1 4 40.13 1.33 2.2472 3 2 1 4 40.21 3.18 2.2427 4 0 0 2 40.30 16.00 2.2380 2 4 1 4 40.67 2.87 2.2182 -1 4 2 4 40.86 2.30 2.2083 4 1 0 4 40.91 1.28 2.2061 2 5 0 4 41.05 1.46 2.1989 -3 4 1 4 41.18 3.27 2.1923 -4 2 1 4 41.53 10.93 2.1743 3 4 0 4 41.56 5.65 2.1731 -2 5 1 4 41.66 12.03 2.1678 0 4 2 4 41.69 1.38 2.1666 2 1 2 4 42.25 5.43 2.1391 -2 4 2 4 42.77 15.37 2.1141 4 2 0 4 43.31 2.04 2.0889 3 3 1 4 44.30 2.74 2.0446 -4 3 1 4 44.81 5.36 2.0224 -2 1 3 4 45.24 1.62 2.0043 -4 2 2 4 45.59 2.10 1.9898 0 6 1 4 45.73 1.44 1.9842 -1 6 1 4 45.77 5.59 1.9822 0 0 3 2 45.81 1.50 1.9807 4 3 0 4 45.89 4.21 1.9775 2 5 1 4 46.23 3.12 1.9637 -1 5 2 4 46.56 2.07 1.9504 2 3 2 4 46.57 4.87 1.9503 -3 5 1 4 47.01 6.51 1.9331 3 5 0 4 47.12 4.46 1.9285 0 5 2 4 47.49 1.13 1.9147 3 4 1 4 47.57 10.09 1.9116 -3 1 3 4 47.66 1.18 1.9083 -2 5 2 4 47.78 2.37 1.9035 1 6 1 4 48.18 4.14 1.8888 -2 6 1 4 48.41 2.57 1.8804 -4 4 1 4 49.06 2.62 1.8569 -1 3 3 4 49.08 2.15 1.8563 -5 1 1 4 49.45 9.52 1.8432 -2 3 3 4 49.60 2.03 1.8380 4 2 1 4 49.82 5.49 1.8303 4 4 0 4 50.50 2.84 1.8073 1 1 3 4 50.53 3.67 1.8063 2 4 2 4 50.89 6.27 1.7944 0 3 3 4 51.25 2.44 1.7824 -3 5 2 4 51.35 1.60 1.7794 3 2 2 4 51.44 7.38 1.7764 5 1 0 4 52.13 1.83 1.7546 1 2 3 4 52.33 3.11 1.7483 4 3 1 4 52.39 4.67 1.7465 -1 6 2 4 52.47 6.66 1.7438 3 5 1 4 53.21 1.25 1.7216 0 6 2 4 53.25 5.18 1.7202 -2 4 3 4 53.33 1.74 1.7178 -4 5 1 4 53.69 2.59 1.7071 -2 6 2 4 53.96 1.96 1.6992 -4 2 3 4 54.02 1.07 1.6976 3 3 2 4 54.65 1.70 1.6793 4 5 0 4 54.77 1.92 1.6760 1 3 3 4 54.85 2.00 1.6737 1 7 1 4 55.21 2.29 1.6637 -2 7 1 4 55.32 1.21 1.6608 2 5 2 4 55.66 3.37 1.6513 5 3 0 4 55.92 2.08 1.6442 -5 3 2 4 55.99 1.29 1.6423 4 4 1 4 56.54 2.89 1.6276 -4 3 3 4 56.73 1.13 1.6227 -4 5 2 4 57.61 1.12 1.6001 3 4 2 4 58.95 3.64 1.5667 -4 6 1 4 59.07 1.55 1.5639 -1 7 2 4 59.18 2.13 1.5612 0 5 3 4 59.35 1.06 1.5571 -3 7 1 4 59.49 1.64 1.5538 -2 0 4 2 59.82 1.18 1.5460 0 7 2 4 59.86 1.96 1.5452 5 2 1 4 59.98 1.62 1.5422 -2 1 4 4 60.04 2.77 1.5410 -4 4 3 4 60.19 1.14 1.5373 4 6 0 4 60.49 1.22 1.5306 4 5 1 4 62.15 2.34 1.4935 -4 6 2 4 62.50 4.12 1.4861 1 7 2 4 62.74 1.27 1.4809 4 3 2 4 62.84 3.85 1.4788 -3 2 4 4 63.78 1.69 1.4592 -5 5 2 4 63.93 1.09 1.4563 3 1 3 4 63.98 1.87 1.4551 6 2 0 4 64.34 2.62 1.4479 -1 3 4 4 64.45 4.61 1.4458 3 7 1 4 64.92 2.22 1.4365 -6 3 2 4 67.19 3.14 1.3932 3 6 2 4 67.86 3.56 1.3812 1 6 3 4 68.20 1.42 1.3750 -6 2 3 4 68.23 1.42 1.3745 -4 7 2 4 68.60 2.52 1.3680 -1 9 1 4 69.13 1.82 1.3588 6 0 1 2 69.43 1.20 1.3537 -4 6 3 4 69.58 2.50 1.3511 6 1 1 4 69.71 2.29 1.3490 -5 1 4 4 70.15 1.20 1.3415 4 5 2 4 70.93 2.01 1.3287 -7 1 1 4 71.19 2.20 1.3246 -2 5 4 4 71.67 1.23 1.3168 -1 5 4 4 72.04 2.76 1.3109 -4 8 1 4 73.94 2.17 1.2819 1 4 4 4 74.41 1.93 1.2750 7 1 0 4 74.46 1.09 1.2742 5 7 0 4 75.72 1.11 1.2561 7 2 0 4 76.95 1.46 1.2391 0 10 1 4 77.06 1.29 1.2376 -6 6 2 4 77.54 1.28 1.2311 -6 5 3 4 79.59 1.07 1.2044 -1 2 5 4 81.12 1.44 1.1856 2 9 2 4 82.79 1.17 1.1659 -6 4 4 4 83.02 1.01 1.1632 7 2 1 4 83.49 1.47 1.1579 2 5 4 4 84.11 2.24 1.1509 5 2 3 4 84.98 1.03 1.1413 -5 2 5 4 85.06 1.05 1.1404 2 8 3 4 87.09 1.48 1.1190 4 8 2 4 89.05 1.00 1.0994 -6 -8 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.