Crocoite Quareni S, De Pieri R Acta Crystallographica 19 (1965) 287-289 A three-dimensional refinement of the structure of crocoite, PbCrO4 _database_code_amcsd 0009297 CELL PARAMETERS: 7.1200 7.4300 6.7900 90.000 102.420 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 350.796 Density (g/cm3): 6.119 MAX. ABS. INTENSITY / VOLUME**2: 118.2116845 RIR: 6.291 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 16.37 10.81 5.4156 -1 0 1 2 17.47 6.69 5.0769 1 1 0 4 17.93 28.02 4.9473 0 1 1 4 20.29 29.72 4.3765 -1 1 1 4 20.40 12.52 4.3538 1 0 1 2 23.69 12.71 3.7564 1 1 1 4 23.95 7.31 3.7150 0 2 0 2 25.62 57.62 3.4767 2 0 0 2 26.89 3.58 3.3155 0 0 2 2 27.22 100.00 3.2767 1 2 0 4 27.52 6.83 3.2410 0 2 1 4 28.34 11.75 3.1490 2 1 0 4 28.92 7.10 3.0871 -2 1 1 4 29.50 60.50 3.0278 0 1 2 4 29.78 28.00 3.0001 -1 1 2 4 33.08 16.29 2.7078 -2 0 2 2 33.81 1.79 2.6514 2 1 1 4 34.56 14.69 2.5957 1 1 2 4 35.28 18.64 2.5441 -2 1 2 4 35.36 2.61 2.5385 2 2 0 4 35.84 1.69 2.5057 -2 2 1 4 36.55 4.26 2.4585 -1 2 2 4 38.28 2.04 2.3512 -3 0 1 2 38.81 13.09 2.3201 0 3 1 4 39.97 13.89 2.2554 2 2 1 4 40.03 1.34 2.2523 -1 3 1 4 40.06 12.19 2.2509 -1 0 3 2 40.23 11.25 2.2416 -3 1 1 4 40.78 2.66 2.2126 3 1 0 4 41.97 3.25 2.1527 1 3 1 4 43.31 24.85 2.0891 2 1 2 4 44.07 4.85 2.0547 3 0 1 2 44.31 3.90 2.0444 -3 1 2 4 44.94 1.12 2.0172 2 3 0 4 45.33 8.85 2.0006 -2 3 1 4 45.66 3.61 1.9867 1 0 3 2 45.73 1.74 1.9842 0 3 2 4 45.82 1.60 1.9803 3 1 1 4 45.92 21.67 1.9763 -1 3 2 4 46.16 14.67 1.9665 3 2 0 4 47.89 9.19 1.8996 0 2 3 4 48.80 2.99 1.8661 2 3 1 4 49.04 6.73 1.8575 0 4 0 2 49.36 17.83 1.8464 1 3 2 4 49.38 13.51 1.8455 -3 2 2 4 49.90 2.32 1.8275 -2 3 2 4 50.30 5.58 1.8140 -2 2 3 4 50.56 3.32 1.8052 -3 0 3 2 50.88 5.44 1.7946 1 4 0 4 52.05 1.36 1.7570 -1 4 1 4 52.65 3.56 1.7383 4 0 0 2 52.95 1.98 1.7291 -4 1 1 4 53.64 2.36 1.7085 1 4 1 4 53.76 1.54 1.7052 -3 3 1 4 54.04 6.29 1.6970 -4 0 2 2 54.19 4.90 1.6926 4 1 0 4 54.20 3.26 1.6923 3 3 0 4 54.37 4.37 1.6874 3 1 2 4 55.42 3.98 1.6578 0 0 4 2 55.55 1.59 1.6544 -1 1 4 4 55.55 1.71 1.6544 -4 1 2 4 56.09 2.05 1.6396 -2 0 4 2 56.14 5.74 1.6383 2 4 0 4 56.26 1.26 1.6351 2 3 2 4 56.91 1.70 1.6180 0 1 4 4 57.09 5.52 1.6134 -3 3 2 4 57.57 4.26 1.6011 -2 1 4 4 59.62 2.96 1.5507 2 2 3 4 59.92 5.30 1.5436 -1 2 4 4 60.44 2.29 1.5317 -2 4 2 4 62.76 2.18 1.4806 -3 1 4 4 63.31 2.71 1.4689 4 2 1 4 64.26 1.67 1.4495 3 4 0 4 64.52 2.49 1.4443 -4 3 1 4 65.09 1.82 1.4330 -1 5 1 4 65.11 2.55 1.4327 -1 4 3 4 65.64 7.05 1.4223 1 2 4 4 65.78 2.07 1.4197 -4 2 3 4 65.78 5.59 1.4197 3 3 2 4 65.81 1.09 1.4192 4 0 2 2 66.48 1.37 1.4063 1 5 1 4 66.83 3.04 1.3999 -1 3 4 4 66.85 1.59 1.3996 -3 2 4 4 66.88 1.37 1.3990 -3 4 2 4 66.90 1.60 1.3985 -5 1 1 4 67.15 2.61 1.3940 4 1 2 4 67.64 3.61 1.3851 2 0 4 2 68.04 1.55 1.3779 3 4 1 4 68.66 1.87 1.3669 5 1 0 4 68.69 1.33 1.3664 2 5 0 4 69.25 1.21 1.3568 1 4 3 4 69.29 5.54 1.3560 0 5 2 4 70.52 1.42 1.3355 -1 1 5 4 70.73 3.80 1.3320 -4 1 4 4 72.37 1.19 1.3058 5 0 1 2 72.42 4.32 1.3050 -5 2 2 4 72.57 3.02 1.3027 -2 5 2 4 72.59 1.68 1.3024 5 2 0 4 73.10 1.59 1.2946 -3 4 3 4 73.41 4.51 1.2898 -3 3 4 4 74.80 1.40 1.2692 4 4 0 4 75.72 1.74 1.2561 -3 5 1 4 75.95 1.57 1.2529 -4 4 2 4 77.00 1.35 1.2383 0 6 0 2 77.12 2.15 1.2368 0 4 4 4 77.14 1.37 1.2366 1 1 5 4 77.68 1.15 1.2292 -2 4 4 4 77.83 3.93 1.2273 2 5 2 4 78.45 1.24 1.2192 1 6 0 4 78.95 2.78 1.2126 5 3 0 4 81.19 1.15 1.1847 -5 1 4 4 81.96 1.69 1.1756 -6 0 2 2 82.70 2.50 1.1669 3 2 4 4 82.73 2.02 1.1665 2 6 0 4 84.64 1.81 1.1451 6 1 0 4 85.40 1.19 1.1368 5 2 2 4 86.08 1.42 1.1295 4 5 0 4 86.47 1.39 1.1254 -2 0 6 2 87.50 1.07 1.1149 -5 4 2 4 87.94 1.89 1.1104 2 4 4 4 88.88 1.33 1.1011 -2 5 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.