Hexahydroborite Sedlacek P, Dornberger-Schiff K Acta Crystallographica B27 (1971) 1532-1541 An OD-Disordered modification of the calcium monoborate dihydrate Ca[B(OH)4]2*2H2O Locality: synthetic Sample: MDO (1) _database_code_amcsd 0009397 CELL PARAMETERS: 16.0800 6.6900 7.9500 90.000 104.900 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 826.466 Density (g/cm3): 1.849 MAX. ABS. INTENSITY / VOLUME**2: 5.424579053 RIR: 0.955 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.39 100.00 7.7697 2 0 0 2 14.41 56.09 6.1447 1 1 0 4 17.54 2.91 5.0560 -1 1 1 4 21.70 18.74 4.0956 3 1 0 4 22.43 85.26 3.9642 -3 1 1 4 23.04 1.12 3.8603 -2 0 2 2 23.15 2.87 3.8413 0 0 2 2 26.08 25.16 3.4172 -1 1 2 4 26.65 11.69 3.3450 0 2 0 2 26.67 46.19 3.3430 3 1 1 4 28.44 20.40 3.1382 -3 1 2 4 28.44 20.46 3.1378 2 0 2 2 28.63 11.53 3.1179 1 1 2 4 29.06 9.01 3.0724 2 2 0 4 31.15 1.34 2.8715 -5 1 1 4 31.75 30.69 2.8186 5 1 0 4 32.47 1.87 2.7577 2 2 1 4 34.63 1.41 2.5899 6 0 0 2 35.38 8.27 2.5372 -4 2 1 4 35.59 48.98 2.5226 0 2 2 4 36.42 8.29 2.4666 5 1 1 4 36.52 1.99 2.4606 -6 0 2 2 36.62 5.73 2.4541 -1 1 3 4 36.90 1.78 2.4362 4 0 2 2 37.44 16.52 2.4020 -3 1 3 4 39.16 3.33 2.3006 -4 2 2 4 39.25 2.33 2.2953 4 2 1 4 39.37 17.64 2.2885 2 2 2 4 39.47 4.72 2.2828 1 1 3 4 40.88 1.27 2.2074 1 3 0 4 41.59 11.27 2.1716 -7 1 1 4 42.93 5.55 2.1069 7 1 0 4 43.05 1.00 2.1013 1 3 1 4 43.35 1.50 2.0872 -6 2 1 4 43.65 6.99 2.0736 -2 2 3 4 43.67 1.82 2.0729 -7 1 2 4 44.22 8.76 2.0482 3 3 0 4 44.23 1.23 2.0478 6 2 0 4 44.56 1.32 2.0334 0 2 3 4 45.43 8.37 1.9965 3 1 3 4 45.78 20.38 1.9821 -6 2 2 4 46.09 15.38 1.9693 4 2 2 4 46.66 4.32 1.9467 -8 0 2 2 46.71 9.64 1.9448 -1 3 2 4 46.77 12.41 1.9424 8 0 0 2 47.06 15.77 1.9309 3 3 1 4 47.08 5.03 1.9302 -4 0 4 2 47.09 1.60 1.9297 6 0 2 2 48.18 4.74 1.8889 -3 3 2 4 48.18 5.71 1.8887 -1 1 4 4 49.96 3.95 1.8257 -5 3 1 4 50.91 1.28 1.7937 -5 1 4 4 51.26 6.27 1.7823 1 1 4 4 51.43 14.42 1.7767 -6 0 4 2 51.89 1.43 1.7620 2 0 4 2 52.51 4.73 1.7426 -5 3 2 4 52.74 1.32 1.7356 3 3 2 4 54.54 3.09 1.6825 -8 2 2 4 54.55 5.79 1.6823 7 1 2 4 54.90 5.09 1.6725 0 4 0 2 54.92 1.51 1.6718 -4 2 4 4 55.09 2.07 1.6671 4 2 3 4 56.26 1.73 1.6350 2 4 0 4 56.40 2.63 1.6314 -7 1 4 4 56.94 1.44 1.6171 3 1 4 4 56.94 1.79 1.6171 -2 4 1 4 58.02 1.03 1.5896 -10 0 2 2 58.86 5.04 1.5689 4 0 4 2 59.49 5.82 1.5539 10 0 0 2 59.59 5.01 1.5514 5 3 2 4 59.84 2.60 1.5457 -3 1 5 4 60.36 1.32 1.5335 0 4 2 4 62.88 1.87 1.4780 -3 3 4 4 64.10 1.27 1.4528 -9 1 4 4 64.95 2.17 1.4357 -10 2 2 4 65.14 1.72 1.4320 -8 2 4 4 65.40 1.36 1.4270 8 2 2 4 65.89 2.26 1.4175 -6 4 1 4 68.05 1.37 1.3778 -9 3 2 4 68.56 3.69 1.3687 -11 1 3 4 71.38 1.28 1.3214 -9 3 3 4 73.14 2.20 1.2939 -3 3 5 4 73.80 1.13 1.2840 -5 1 6 4 73.85 1.47 1.2833 -1 3 5 4 74.25 1.25 1.2773 6 2 4 4 75.17 1.52 1.2640 -4 4 4 4 76.00 1.77 1.2522 -3 5 2 4 77.03 1.07 1.2379 -9 3 4 4 77.38 2.96 1.2333 10 2 2 4 77.70 2.80 1.2289 5 5 0 4 77.71 1.12 1.2288 1 1 6 4 77.85 2.72 1.2270 -2 2 6 4 78.61 1.39 1.2170 -11 3 2 4 84.71 1.94 1.1443 4 4 4 4 85.25 2.38 1.1384 10 4 0 4 86.09 1.24 1.1294 9 1 4 4 87.77 1.14 1.1121 7 5 1 4 88.32 1.10 1.1066 -1 5 4 4 88.64 1.09 1.1034 0 6 1 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.