Na3PO4(NaOH).167*12H2O Tillmanns E, Baur W H Acta Crystallographica B27 (1971) 2124-2132 On the crystal chemistry of salt hydrates. VII. The crystal structures of pseudo trisodium orthoarsenate dodecahydrate and the isomorphous phosphate and vanadate salts _database_code_amcsd 0009400 CELL PARAMETERS: 11.8900 11.8900 12.6710 90.000 90.000 120.000 SPACE GROUP: P-3c1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1551.334 Density (g/cm3): 1.766 MAX. ABS. INTENSITY / VOLUME**2: 2.254006118 RIR: 0.415 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.59 100.00 10.2970 1 0 0 6 13.98 15.17 6.3355 0 0 2 2 14.90 5.85 5.9450 1 1 0 6 16.43 51.33 5.3959 0 1 2 6 16.43 1.76 5.3959 1 0 2 6 16.47 3.20 5.3821 1 1 1 12 17.22 3.48 5.1485 2 0 0 6 20.49 82.17 4.3352 1 1 2 12 22.25 15.73 3.9956 0 2 2 6 22.25 26.50 3.9956 2 0 2 6 22.85 10.20 3.8919 2 1 0 12 23.92 7.20 3.7204 2 1 1 12 25.96 14.28 3.4323 3 0 0 6 26.89 69.87 3.3162 1 2 2 12 26.89 2.06 3.3162 2 1 2 12 28.17 4.10 3.1677 0 0 4 2 29.50 47.44 3.0277 0 1 4 6 29.50 1.02 3.0277 1 0 4 6 29.60 8.65 3.0179 0 3 2 6 30.06 25.55 2.9725 2 2 0 6 30.90 47.41 2.8939 2 2 1 12 31.25 9.16 2.8621 1 2 3 12 31.25 40.19 2.8621 2 1 3 12 31.32 59.64 2.8559 3 1 0 12 32.01 11.38 2.7956 1 1 4 12 32.13 57.37 2.7860 1 3 1 12 32.13 1.94 2.7860 3 1 1 12 33.21 72.07 2.6980 0 2 4 6 33.29 49.06 2.6910 2 2 2 12 34.45 85.26 2.6036 1 3 2 12 34.45 11.29 2.6036 3 1 2 12 34.85 23.37 2.5743 4 0 0 6 36.58 6.89 2.4568 1 2 4 12 36.58 48.31 2.4568 2 1 4 12 36.98 4.45 2.4309 2 2 3 12 37.72 3.37 2.3849 0 4 2 6 37.72 3.17 2.3849 4 0 2 6 38.03 3.02 2.3658 1 3 3 12 38.03 36.61 2.3658 3 1 3 12 38.62 8.07 2.3312 1 1 5 12 38.68 25.52 2.3279 0 3 4 6 38.68 4.92 2.3279 3 0 4 6 38.78 3.92 2.3223 2 3 1 12 40.77 1.72 2.2134 2 3 2 12 40.78 14.54 2.2125 1 4 1 12 41.67 17.80 2.1676 2 2 4 12 42.57 9.29 2.1237 1 2 5 12 42.62 1.47 2.1211 3 1 4 12 42.70 1.48 2.1177 1 4 2 12 43.91 2.22 2.0617 2 3 3 12 43.91 13.79 2.0617 3 2 3 12 43.97 1.89 2.0594 5 0 0 6 45.40 3.49 1.9978 4 0 4 6 45.59 16.30 1.9900 1 1 6 12 45.74 10.99 1.9837 1 4 3 12 45.74 13.40 1.9837 4 1 3 12 45.79 6.65 1.9817 3 3 0 6 46.36 7.96 1.9585 0 5 2 6 46.36 12.07 1.9585 5 0 2 6 47.13 7.24 1.9285 2 2 5 12 47.26 4.90 1.9234 2 4 1 12 48.00 10.60 1.8955 3 1 5 12 48.04 15.01 1.8937 3 2 4 12 48.11 30.37 1.8913 3 3 2 12 49.08 12.93 1.8562 1 2 6 12 49.75 1.60 1.8327 4 1 4 12 49.83 9.91 1.8300 1 5 1 12 50.76 7.93 1.7986 0 3 6 6 51.47 3.99 1.7753 1 5 2 12 51.47 2.86 1.7753 5 1 2 12 51.72 3.80 1.7674 4 2 3 12 52.87 18.63 1.7317 1 1 7 12 53.39 19.21 1.7162 6 0 0 6 54.00 3.08 1.6980 1 3 6 12 54.00 15.29 1.6980 3 1 6 12 54.14 4.99 1.6941 1 5 3 12 54.14 1.55 1.6941 5 1 3 12 54.18 10.57 1.6928 4 3 0 12 54.63 13.50 1.6800 3 3 4 12 54.70 5.19 1.6779 3 4 1 12 54.70 5.91 1.6779 4 3 1 12 55.41 12.02 1.6581 4 2 4 12 55.75 6.76 1.6488 5 2 0 12 56.25 1.91 1.6354 4 3 2 12 56.26 2.46 1.6351 2 5 1 12 56.35 1.20 1.6327 4 0 6 6 57.72 1.44 1.5971 5 1 4 12 57.78 1.08 1.5957 2 5 2 12 57.78 4.31 1.5957 5 2 2 12 58.64 1.70 1.5744 3 2 6 12 58.76 2.59 1.5713 3 4 3 12 59.00 3.92 1.5655 0 1 8 6 59.30 3.53 1.5584 1 6 1 12 59.93 3.14 1.5434 4 2 5 12 60.13 2.14 1.5389 4 1 6 12 60.77 5.30 1.5242 6 1 2 12 61.23 6.31 1.5139 0 2 8 6 61.23 1.45 1.5139 2 0 8 6 61.45 1.62 1.5090 0 6 4 6 62.13 3.59 1.4939 1 5 5 12 62.49 1.02 1.4863 4 4 0 6 63.17 1.15 1.4719 6 1 3 12 63.21 2.10 1.4710 7 0 0 6 63.40 2.46 1.4670 1 2 8 12 63.69 2.78 1.4612 3 5 1 12 64.83 1.37 1.4381 0 3 8 6 65.10 1.02 1.4329 5 3 2 12 65.35 1.26 1.4279 6 2 0 12 66.72 2.39 1.4020 4 4 3 12 67.20 3.45 1.3930 2 6 2 12 67.30 1.47 1.3913 5 1 6 12 67.41 1.24 1.3892 5 3 3 12 67.81 3.16 1.3821 5 2 5 12 69.49 1.56 1.3527 2 6 3 12 69.71 1.42 1.3490 4 0 8 6 70.45 3.85 1.3365 3 3 7 12 70.60 4.24 1.3342 3 5 4 12 70.60 3.44 1.3342 7 0 4 6 70.65 3.69 1.3333 1 7 2 12 71.13 1.20 1.3254 2 4 7 12 71.13 1.18 1.3254 4 2 7 12 71.75 1.85 1.3155 2 3 8 12 71.75 3.04 1.3155 3 2 8 12 72.92 1.07 1.2973 6 3 0 12 73.35 1.48 1.2907 4 5 2 12 74.60 2.19 1.2722 5 3 5 12 75.35 2.34 1.2614 8 0 2 6 75.59 1.65 1.2580 7 2 0 12 75.96 1.14 1.2527 7 1 4 12 77.74 5.34 1.2284 2 4 8 12 79.39 1.83 1.2070 5 3 6 12 79.90 1.99 1.2005 3 6 4 12 80.51 1.47 1.1930 1 4 9 12 81.34 1.04 1.1829 2 6 6 12 82.96 1.07 1.1639 6 0 8 6 83.60 1.29 1.1566 4 3 8 12 84.40 1.90 1.1477 3 3 9 12 84.58 1.00 1.1457 1 7 6 12 84.72 3.74 1.1441 9 0 0 6 85.39 1.49 1.1368 4 0 10 6 87.47 1.03 1.1151 6 1 8 12 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.