VOSO4(H2O)3 Theobald F, Galy J Acta Crystallographica B29 (1973) 2732-2736 Structure cristalline de VOSO4((H2O)3 Locality: synthetic Note: polymorph of bobjonesite _database_code_amcsd 0009497 CELL PARAMETERS: 7.4110 7.4390 12.2720 90.000 108.900 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 640.084 Density (g/cm3): 2.319 MAX. ABS. INTENSITY / VOLUME**2: 9.087045473 RIR: 1.276 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.63 5.27 7.0114 1 0 0 2 14.14 35.83 6.2636 0 1 1 4 15.26 45.79 5.8052 0 0 2 2 16.37 41.36 5.4154 -1 0 2 2 17.38 13.35 5.1023 1 1 0 4 19.40 100.00 4.5766 0 1 2 4 20.28 51.87 4.3782 -1 1 2 4 22.83 15.38 3.8945 1 0 2 2 23.92 18.68 3.7195 0 2 0 2 25.06 2.99 3.5532 -2 0 2 2 25.14 7.98 3.5422 0 2 1 4 25.41 38.93 3.5057 2 0 0 2 25.82 1.60 3.4503 1 1 2 4 25.95 5.88 3.4333 0 1 3 4 26.89 8.28 3.3161 -2 1 1 4 27.06 32.38 3.2954 -1 2 1 4 27.14 2.42 3.2858 1 2 0 4 27.83 13.38 3.2062 -2 1 2 4 28.14 13.25 3.1712 2 1 0 4 28.50 1.02 3.1318 0 2 2 4 29.13 24.05 3.0660 -1 2 2 4 29.24 4.68 3.0542 -1 0 4 2 29.35 7.21 3.0429 1 2 1 4 30.80 2.40 2.9026 0 0 4 2 31.34 4.13 2.8540 2 1 1 4 31.67 22.88 2.8253 -1 1 4 4 32.97 5.67 2.7165 -1 2 3 4 33.08 3.43 2.7077 -2 0 4 2 33.13 6.34 2.7040 0 1 4 4 33.41 7.88 2.6818 0 2 3 4 33.88 19.90 2.6456 2 0 2 2 34.16 8.10 2.6248 -2 2 1 4 35.27 1.49 2.5444 -2 1 4 4 36.03 8.06 2.4927 2 1 2 4 36.50 12.23 2.4618 -3 0 2 2 37.07 7.79 2.4250 0 3 1 4 37.85 7.82 2.3770 2 2 1 4 38.45 6.66 2.3412 -1 3 1 4 38.52 2.09 2.3372 -3 1 2 4 38.52 5.11 2.3371 3 0 0 2 38.54 10.49 2.3359 1 2 3 4 38.63 2.41 2.3308 -1 1 5 4 39.38 2.29 2.2883 0 2 4 4 40.16 1.03 2.2453 1 3 1 4 40.99 1.45 2.2018 -3 0 4 2 41.24 13.73 2.1891 -2 2 4 4 41.78 1.00 2.1619 2 1 3 4 43.64 2.35 2.0742 3 1 1 4 44.21 6.09 2.0485 -1 2 5 4 44.27 3.88 2.0459 -3 2 1 4 44.56 3.54 2.0335 -2 3 2 4 45.39 4.17 1.9980 -3 2 3 4 45.62 6.36 1.9884 -2 0 6 2 45.86 2.94 1.9789 3 2 0 4 46.58 2.97 1.9499 -2 3 3 4 46.64 1.25 1.9475 1 1 5 4 46.64 1.61 1.9473 2 0 4 2 46.96 3.56 1.9351 0 0 6 2 46.98 6.97 1.9341 2 3 1 4 47.06 1.87 1.9311 2 2 3 4 47.21 14.65 1.9251 -1 3 4 4 47.32 6.82 1.9209 -2 1 6 4 48.02 3.96 1.8947 -3 2 4 4 48.02 8.31 1.8947 3 1 2 4 48.31 5.11 1.8838 2 1 4 4 48.62 1.28 1.8727 0 1 6 4 48.76 1.27 1.8678 3 2 1 4 50.56 1.48 1.8051 -3 0 6 2 51.01 1.97 1.7905 -1 2 6 4 51.43 1.49 1.7766 -4 0 4 2 51.53 2.33 1.7737 1 2 5 4 51.61 1.06 1.7711 0 4 2 4 51.99 4.32 1.7589 -1 4 2 4 52.13 1.76 1.7545 1 4 1 4 52.16 2.23 1.7535 -2 2 6 4 52.18 1.72 1.7529 4 0 0 2 53.01 1.53 1.7273 1 0 6 2 53.09 2.09 1.7251 2 2 4 4 53.73 5.26 1.7061 4 1 0 4 53.91 1.41 1.7008 3 3 0 4 54.40 1.15 1.6866 -2 1 7 4 54.47 1.22 1.6846 -1 4 3 4 54.54 1.12 1.6826 1 1 6 4 54.69 3.29 1.6782 1 4 2 4 54.76 2.04 1.6763 0 4 3 4 55.27 1.92 1.6621 -2 4 1 4 55.42 7.84 1.6580 -4 2 2 4 55.79 2.03 1.6477 -2 4 2 4 55.84 1.62 1.6464 -3 3 4 4 55.97 2.03 1.6429 2 4 0 4 56.20 1.06 1.6366 -4 2 1 4 56.68 1.56 1.6240 -3 2 6 4 56.97 1.16 1.6163 4 1 1 4 57.86 1.50 1.5936 3 2 3 4 58.37 1.24 1.5809 1 4 3 4 58.40 1.23 1.5803 -1 2 7 4 58.48 1.63 1.5781 -4 0 6 2 58.96 1.91 1.5666 1 2 6 4 58.99 3.04 1.5659 0 4 4 4 59.02 2.18 1.5651 1 3 5 4 59.60 2.58 1.5512 -2 3 6 4 59.85 3.28 1.5452 4 0 2 2 60.19 1.42 1.5373 3 3 2 4 60.38 1.36 1.5330 -2 4 4 4 60.45 1.27 1.5315 2 3 4 4 60.64 2.73 1.5271 -2 0 8 2 60.71 1.28 1.5255 0 3 6 4 63.66 1.40 1.4617 -5 0 4 2 63.97 3.01 1.4554 1 5 0 4 64.16 1.30 1.4516 0 4 5 4 64.17 1.65 1.4513 0 0 8 2 64.32 1.45 1.4484 -5 1 2 4 64.53 1.14 1.4442 -4 3 4 4 66.94 1.68 1.3978 1 2 7 4 68.00 2.33 1.3786 0 3 7 4 68.90 1.01 1.3628 -4 2 7 4 69.04 1.97 1.3604 -5 2 4 4 69.42 1.57 1.3538 -4 0 8 2 69.63 3.49 1.3503 -5 2 1 4 69.90 1.01 1.3458 -2 5 3 4 69.95 2.40 1.3449 2 4 4 4 70.73 1.63 1.3320 -4 1 8 4 71.95 2.12 1.3124 -4 4 2 4 71.96 1.11 1.3121 5 2 0 4 74.13 1.76 1.2790 -2 2 9 4 74.37 1.02 1.2756 4 4 0 4 74.84 1.09 1.2687 -5 3 2 4 75.53 1.02 1.2588 1 2 8 4 78.28 1.15 1.2214 -1 6 1 4 78.47 1.30 1.2188 0 2 9 4 79.19 1.07 1.2096 2 0 8 2 79.38 2.08 1.2071 1 6 1 4 81.17 1.24 1.1850 -4 2 9 4 81.18 1.16 1.1849 3 5 2 4 81.22 1.62 1.1844 -6 0 6 2 82.61 1.26 1.1680 2 4 6 4 84.45 1.50 1.1471 0 1 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.