O14 P5 Sm Tranqui D, Bagieu M, Durif A Acta Crystallographica B30 (1974) 1751-1755 Structure cristalline de l'ultraphosphate de Samarium Sm P5 O14 _cod_database_code 1007239 _database_code_amcsd 0015921 CELL PARAMETERS: 8.7500 12.9900 8.9440 90.000 90.000 90.450 SPACE GROUP: P2_1/b X-RAY WAVELENGTH: 1.541838 Cell Volume: 1016.566 Density (g/cm3): 3.457 MAX. ABS. INTENSITY / VOLUME**2: 23.88622535 RIR: 2.250 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.11 11.68 8.7497 1 0 0 2 12.01 20.13 7.3666 0 1 1 4 13.63 17.90 6.4948 0 2 0 2 14.16 18.03 6.2545 1 0 1 4 16.94 2.59 5.2348 -1 2 0 2 17.07 2.50 5.1956 1 2 0 2 19.65 33.87 4.5179 -1 2 1 4 19.76 29.19 4.4926 1 2 1 4 20.30 38.05 4.3749 2 0 0 2 22.33 2.85 3.9820 1 0 2 4 22.82 7.09 3.8972 0 3 1 4 23.34 24.76 3.8110 1 -1 2 4 23.39 28.18 3.8034 1 1 2 4 23.61 1.10 3.7689 2 -1 1 4 23.70 1.95 3.7542 2 1 1 4 24.16 100.00 3.6833 0 2 2 4 24.44 26.27 3.6417 -2 2 0 2 24.62 36.11 3.6153 2 2 0 2 26.21 2.69 3.4002 -1 2 2 4 26.29 2.61 3.3894 1 2 2 4 27.47 7.87 3.2474 0 4 0 2 28.54 18.32 3.1273 2 0 2 4 29.26 3.90 3.0523 -1 4 0 2 29.34 1.10 3.0443 2 -1 2 4 29.41 3.59 3.0367 1 4 0 2 30.61 39.23 2.9203 -2 3 1 4 30.65 1.53 2.9166 3 0 0 2 30.77 10.42 2.9058 0 1 3 4 30.83 35.41 2.8999 2 3 1 4 30.96 3.45 2.8887 -1 4 1 4 31.10 4.77 2.8755 1 4 1 4 31.69 7.21 2.8239 2 -2 2 4 31.71 3.57 2.8220 1 0 3 4 31.83 4.32 2.8115 2 2 2 4 32.28 3.39 2.7729 3 0 1 4 32.98 2.50 2.7159 3 -1 1 4 33.08 3.05 2.7076 3 1 1 4 33.58 3.63 2.6685 -3 2 0 2 33.79 3.04 2.6528 3 2 0 2 34.12 12.33 2.6277 0 4 2 4 34.26 4.11 2.6174 -2 4 0 2 34.53 2.00 2.5978 2 4 0 2 35.09 5.69 2.5571 3 -2 1 4 35.29 4.35 2.5433 3 2 1 4 36.00 3.26 2.4948 0 5 1 4 36.60 7.06 2.4555 0 3 3 4 36.79 2.09 2.4429 3 0 2 4 37.11 8.99 2.4225 2 -1 3 4 37.17 10.95 2.4186 2 1 3 4 39.32 1.25 2.2915 3 -2 2 4 39.91 4.94 2.2589 -2 4 2 4 40.14 8.55 2.2463 2 4 2 4 41.27 7.78 2.1874 4 0 0 2 41.43 4.47 2.1794 -1 5 2 4 41.45 1.79 2.1784 -3 4 0 2 41.57 3.94 2.1723 1 5 2 4 41.72 9.70 2.1649 0 6 0 2 41.79 1.42 2.1615 3 4 0 2 41.82 1.09 2.1602 2 5 1 4 42.12 2.11 2.1454 -2 3 3 4 42.28 9.82 2.1375 1 -1 4 4 42.29 1.83 2.1372 2 3 3 4 42.31 8.28 2.1362 1 1 4 4 42.36 2.72 2.1337 3 -3 2 4 42.38 5.17 2.1328 -1 4 3 4 42.49 3.50 2.1274 1 4 3 4 42.55 2.15 2.1248 4 0 1 4 42.61 5.00 2.1217 3 3 2 4 42.72 10.42 2.1165 -3 4 1 4 43.05 10.03 2.1010 3 4 1 4 43.12 1.05 2.0977 1 6 0 2 43.40 1.46 2.0848 3 0 3 4 43.55 2.21 2.0780 -4 2 0 2 43.77 2.93 2.0681 4 2 0 2 43.95 2.27 2.0603 3 -1 3 4 44.03 2.49 2.0567 3 1 3 4 44.19 4.05 2.0494 -1 6 1 4 44.35 3.96 2.0423 1 6 1 4 44.78 1.36 2.0241 4 -2 1 4 44.99 1.76 2.0149 4 2 1 4 45.25 1.48 2.0039 -2 5 2 4 45.52 1.17 1.9928 2 5 2 4 45.78 1.71 1.9818 3 2 3 4 46.36 2.87 1.9586 0 5 3 4 46.36 2.35 1.9584 -3 4 2 4 46.67 2.19 1.9464 -2 6 0 2 46.67 2.18 1.9461 3 4 2 4 46.86 10.40 1.9389 -1 3 4 4 46.93 10.98 1.9359 1 3 4 4 46.97 3.07 1.9343 2 6 0 2 47.52 1.32 1.9133 4 -3 1 4 48.30 3.91 1.8845 4 -2 2 4 48.35 1.76 1.8826 3 -3 3 4 48.50 3.34 1.8771 4 2 2 4 48.57 1.39 1.8743 3 3 3 4 50.38 1.29 1.8114 -2 3 4 4 50.97 10.72 1.7916 -2 5 3 4 51.16 2.45 1.7856 -3 5 2 4 51.18 1.51 1.7847 -2 6 2 4 51.21 10.28 1.7837 2 5 3 4 51.47 1.01 1.7754 2 6 2 4 51.52 1.39 1.7739 3 5 2 4 51.58 2.49 1.7721 0 1 5 4 51.98 3.82 1.7593 3 -1 4 4 52.05 3.45 1.7571 3 1 4 4 52.19 3.92 1.7526 1 0 5 4 52.44 1.83 1.7449 -3 6 0 2 52.86 1.68 1.7319 3 6 0 2 53.26 1.06 1.7198 -1 6 3 4 53.35 1.62 1.7174 5 0 1 4 53.41 1.46 1.7156 1 6 3 4 53.50 1.14 1.7126 -3 6 1 4 53.92 1.22 1.7003 3 6 1 4 54.17 2.00 1.6930 -5 2 0 2 54.40 2.11 1.6864 4 -4 2 4 54.41 1.60 1.6864 5 2 0 2 54.48 1.32 1.6843 -1 7 2 4 54.64 1.57 1.6797 1 7 2 4 54.77 2.58 1.6759 4 4 2 4 55.22 1.22 1.6635 5 -2 1 4 55.26 1.11 1.6622 1 5 4 4 55.59 1.13 1.6533 0 3 5 4 55.67 1.12 1.6509 -4 5 1 4 55.90 3.39 1.6447 3 -3 4 4 55.96 2.44 1.6431 2 -1 5 4 56.01 2.26 1.6418 2 1 5 4 56.11 2.95 1.6392 3 3 4 4 56.13 2.71 1.6386 4 5 1 4 56.19 2.50 1.6370 4 -3 3 4 56.46 2.21 1.6297 4 3 3 4 56.47 1.53 1.6296 5 0 2 4 56.69 3.04 1.6237 0 8 0 2 57.01 1.38 1.6155 5 1 2 4 58.27 1.38 1.5834 5 -2 2 4 58.49 1.39 1.5779 5 2 2 4 58.59 4.57 1.5754 0 7 3 4 58.66 1.71 1.5738 -1 8 1 4 58.84 1.94 1.5695 1 8 1 4 59.08 1.43 1.5636 4 0 4 4 59.43 1.10 1.5554 0 6 4 4 59.73 3.18 1.5481 -2 3 5 4 59.84 2.42 1.5456 -5 4 0 2 59.87 3.42 1.5450 2 3 5 4 59.87 2.81 1.5448 -4 6 0 2 60.27 2.75 1.5355 5 4 0 2 60.39 2.30 1.5327 4 6 0 2 60.68 3.57 1.5262 0 8 2 4 60.68 1.71 1.5262 -2 8 0 2 61.03 1.70 1.5184 2 8 0 2 61.58 2.51 1.5060 -3 6 3 4 61.84 1.44 1.5003 5 -1 3 4 61.95 1.50 1.4979 5 1 3 4 61.97 2.20 1.4975 3 6 3 4 62.53 1.84 1.4854 -2 7 3 4 62.83 2.00 1.4791 2 7 3 4 63.10 4.03 1.4733 0 5 5 4 63.64 1.10 1.4621 3 5 4 4 63.73 1.73 1.4604 1 -1 6 4 63.75 2.14 1.4600 1 1 6 4 66.25 1.46 1.4107 -1 7 4 4 66.40 1.09 1.4080 1 7 4 4 66.52 1.13 1.4057 -3 8 1 4 67.01 1.05 1.3966 3 8 1 4 68.05 1.65 1.3777 4 -1 5 4 68.88 1.12 1.3632 -1 6 5 4 68.91 1.06 1.3626 6 3 1 4 69.00 1.45 1.3611 1 6 5 4 70.06 1.03 1.3430 -4 5 4 4 70.46 1.00 1.3364 4 5 4 4 71.41 1.41 1.3209 3 -1 6 4 71.47 2.12 1.3200 3 1 6 4 71.75 1.65 1.3155 5 -3 4 4 72.05 1.36 1.3108 5 3 4 4 72.32 1.33 1.3066 -5 6 2 4 72.81 1.24 1.2990 0 10 0 2 72.91 1.60 1.2974 5 6 2 4 74.45 1.18 1.2744 4 7 3 4 75.73 1.51 1.2560 -4 8 2 4 76.34 1.32 1.2474 0 10 2 4 76.79 1.38 1.2413 -1 2 7 4 76.83 1.26 1.2407 1 2 7 4 77.08 1.58 1.2373 -2 7 5 4 77.35 1.90 1.2336 2 7 5 4 77.49 1.07 1.2318 4 0 6 4 77.96 1.93 1.2255 0 3 7 4 79.77 2.30 1.2022 -1 9 4 4 79.79 1.27 1.2020 -2 10 2 4 79.94 2.30 1.2001 1 9 4 4 80.17 1.36 1.1972 2 10 2 4 81.70 2.24 1.1786 -1 4 7 4 81.78 2.53 1.1777 1 4 7 4 83.97 1.15 1.1524 3 -2 7 4 86.77 1.60 1.1223 -3 9 4 4 87.28 1.82 1.1171 3 9 4 4 88.16 1.40 1.1082 6 -5 4 4 88.72 1.00 1.1026 6 5 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.