H6 K O10.5 P2 Zn2 Tordjman I, Durif A, Averbuch-Pouchot M, Guitel J Acta Crystallographica B31 (1975) 1143-1148 Structure cristalline du monophosphate de zinc-potassium: Zn2KH(PO4)2(H2O)2.5 _cod_database_code 1007025 _database_code_amcsd 0009533 CELL PARAMETERS: 9.1090 13.5430 8.8140 102.210 113.350 95.920 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 954.277 Density (g/cm3): 2.783 MAX. ABS. INTENSITY / VOLUME**2: 6.686502836 RIR: 0.782 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.83 48.58 12.9461 0 1 0 2 10.82 36.66 8.1794 1 0 0 2 11.38 34.52 7.7770 0 0 1 2 11.53 100.00 7.6746 -1 1 0 2 11.54 2.09 7.6672 0 -1 1 2 11.86 23.73 7.4624 -1 0 1 2 13.24 23.37 6.6861 -1 -1 1 2 13.68 2.76 6.4731 0 2 0 2 13.96 14.99 6.3438 1 1 0 2 14.14 10.35 6.2649 -1 1 1 2 14.82 2.72 5.9772 0 1 1 2 15.20 36.26 5.8301 0 -2 1 2 15.59 16.23 5.6849 -1 2 0 2 17.45 12.77 5.0824 -1 -2 1 2 18.08 9.92 4.9061 1 -1 1 2 18.81 5.23 4.7176 -1 2 1 2 18.83 36.95 4.7138 1 0 1 2 19.18 8.79 4.6283 1 2 0 2 20.13 16.67 4.4117 0 2 1 2 20.42 8.37 4.3495 -2 1 1 2 20.44 8.14 4.3455 -1 -1 2 2 20.58 2.21 4.3154 0 3 0 2 20.59 14.56 4.3128 0 -3 1 2 20.65 9.40 4.3019 -1 0 2 2 21.18 7.82 4.1944 -1 3 0 2 21.73 3.12 4.0897 2 0 0 2 21.84 2.36 4.0691 1 1 1 2 22.87 1.33 3.8885 0 0 2 2 23.02 6.13 3.8636 -1 -3 1 2 23.18 11.74 3.8373 -2 2 0 2 23.20 42.74 3.8336 0 -2 2 2 23.26 2.82 3.8242 -2 2 1 2 23.61 10.41 3.7681 1 -3 1 2 23.85 5.51 3.7312 -2 0 2 2 24.15 28.83 3.6854 2 1 0 2 24.32 5.07 3.6591 -2 -1 2 2 24.59 99.93 3.6198 -1 3 1 2 24.85 21.95 3.5828 -2 -2 1 2 25.26 9.66 3.5256 1 3 0 2 25.68 26.05 3.4693 0 1 2 2 26.24 3.69 3.3961 0 3 1 2 26.67 30.20 3.3431 -2 -2 2 2 26.75 6.17 3.3326 0 -4 1 2 27.04 6.55 3.2971 -1 2 2 2 27.44 19.62 3.2501 -1 4 0 2 27.56 2.71 3.2365 0 4 0 2 27.61 8.07 3.2303 -2 3 1 2 27.64 19.78 3.2279 2 -1 1 2 28.13 5.54 3.1719 2 2 0 2 28.29 13.82 3.1542 2 -2 1 2 28.49 18.42 3.1325 -2 2 2 2 28.53 24.67 3.1286 1 -2 2 2 28.62 5.77 3.1194 1 -4 1 2 28.70 8.19 3.1103 2 0 1 2 29.24 5.15 3.0542 -1 -4 1 2 29.37 5.18 3.0411 1 0 2 2 29.64 2.87 3.0135 -2 -3 1 2 29.65 1.42 3.0133 -3 1 1 2 29.70 4.99 3.0085 -3 0 1 2 29.90 2.43 2.9886 0 2 2 2 30.47 15.83 2.9336 -2 -3 2 2 30.58 1.27 2.9237 2 -3 1 2 30.59 1.37 2.9225 1 -3 2 2 30.67 7.13 2.9150 0 -4 2 2 30.91 10.49 2.8926 -3 0 2 2 31.15 4.05 2.8710 -1 -4 2 2 31.20 11.50 2.8663 -3 2 1 2 31.24 41.63 2.8632 -1 -2 3 2 31.33 43.05 2.8549 2 1 1 2 31.34 40.44 2.8540 -3 -1 1 2 31.40 4.05 2.8492 -1 0 3 2 31.59 2.37 2.8323 -3 1 2 2 31.61 1.49 2.8305 -2 -1 3 2 31.78 2.24 2.8155 1 4 0 2 31.80 4.87 2.8137 -3 -1 2 2 32.11 1.71 2.7877 -3 1 0 2 32.13 29.42 2.7857 -1 3 2 2 32.15 1.01 2.7841 1 1 2 2 32.80 3.66 2.7306 -2 -2 3 2 32.88 1.64 2.7239 -3 2 0 2 32.89 1.10 2.7231 -2 3 2 2 32.94 9.80 2.7195 -2 4 1 2 33.17 8.65 2.7008 2 3 0 2 33.31 5.28 2.6895 0 -5 1 2 33.44 13.36 2.6795 -1 -3 3 2 33.50 2.06 2.6752 0 -2 3 2 33.74 4.22 2.6567 -1 1 3 2 33.74 5.68 2.6563 -3 2 2 2 33.78 3.29 2.6536 -2 1 3 2 34.01 9.60 2.6358 1 -4 2 2 34.07 18.08 2.6313 -1 5 0 2 34.15 2.44 2.6258 -3 -2 2 2 34.17 2.48 2.6240 -3 3 1 2 34.19 2.83 2.6226 2 -4 1 2 34.38 3.51 2.6084 -3 -2 1 2 34.39 17.94 2.6078 1 -5 1 2 34.60 9.38 2.5923 0 0 3 2 35.02 3.58 2.5625 3 1 0 2 35.08 2.21 2.5582 -3 3 0 2 35.32 1.10 2.5412 -2 -4 2 2 35.38 5.38 2.5371 -2 -3 3 2 35.97 2.16 2.4969 0 -5 2 2 36.11 1.90 2.4875 -3 0 3 2 36.13 3.89 2.4859 1 2 2 2 36.26 7.57 2.4775 -3 -1 3 2 36.74 4.90 2.4461 2 -1 2 2 36.84 8.68 2.4399 -1 -5 2 2 36.90 1.03 2.4361 -1 -4 3 2 36.90 4.30 2.4360 -2 2 3 2 37.15 1.84 2.4201 -3 3 2 2 37.71 17.76 2.3857 -3 -3 2 2 37.76 2.02 2.3826 -3 -2 3 2 37.87 3.09 2.3758 2 -3 2 2 38.00 3.85 2.3676 0 -4 3 2 38.18 3.66 2.3569 2 0 2 2 38.22 1.70 2.3551 3 -1 1 2 38.26 1.06 2.3525 -3 4 1 2 38.28 1.35 2.3511 3 -2 1 2 38.40 2.24 2.3440 3 2 0 2 38.49 5.89 2.3391 -3 4 0 2 38.53 2.39 2.3368 -3 -3 1 2 38.81 8.03 2.3204 2 -5 1 2 38.90 2.45 2.3154 -2 5 1 2 38.99 3.73 2.3101 1 -2 3 2 39.45 2.01 2.2844 3 0 1 2 39.79 2.00 2.2657 -3 2 3 2 40.03 4.88 2.2525 -4 0 2 2 40.03 3.32 2.2522 2 3 1 2 40.17 1.14 2.2451 0 -6 1 2 40.47 1.98 2.2287 -3 -3 3 2 40.84 1.06 2.2095 2 1 2 2 40.85 1.01 2.2089 -4 2 1 2 40.91 2.10 2.2058 0 4 2 2 40.92 1.27 2.2053 0 2 3 2 40.98 3.02 2.2026 -1 6 0 2 41.06 1.83 2.1982 -2 3 3 2 41.17 1.87 2.1925 -2 -1 4 2 41.52 5.91 2.1747 -4 2 2 2 41.55 7.27 2.1735 -3 4 2 2 41.71 3.07 2.1657 -1 -2 4 2 41.84 2.28 2.1593 -1 3 3 2 41.88 2.40 2.1572 3 1 1 2 41.89 1.64 2.1564 0 -6 2 2 41.95 5.20 2.1535 0 -5 3 2 42.00 9.36 2.1510 -2 0 4 2 42.17 5.46 2.1427 -4 -1 1 2 42.18 4.17 2.1422 3 -4 1 2 42.21 2.03 2.1409 1 -4 3 2 42.22 6.65 2.1404 -3 -4 2 2 42.85 1.66 2.1104 -4 3 1 2 42.94 2.82 2.1063 -1 0 4 2 43.13 4.12 2.0972 -2 6 0 2 43.20 6.30 2.0940 -3 5 1 2 43.33 1.46 2.0883 -3 3 3 2 43.47 4.70 2.0820 1 1 3 2 43.55 2.22 2.0782 -4 2 0 2 43.63 1.69 2.0745 -4 1 3 2 43.65 4.31 2.0735 -3 -1 4 2 43.75 3.99 2.0689 -2 -5 3 2 44.01 7.53 2.0576 -2 1 4 2 44.06 1.65 2.0551 -3 0 4 2 44.22 7.05 2.0480 -1 5 2 2 44.41 1.39 2.0398 -3 -2 4 2 44.50 7.49 2.0358 1 5 1 2 44.81 2.57 2.0224 0 -2 4 2 45.18 1.04 2.0068 2 5 0 2 45.23 3.11 2.0050 -1 -4 4 2 45.32 1.65 2.0009 -2 6 1 2 45.53 2.18 1.9924 0 3 3 2 45.57 7.10 1.9906 0 -3 4 2 45.66 10.54 1.9867 1 6 0 2 45.92 3.54 1.9762 -4 4 1 2 46.30 1.37 1.9608 3 -2 2 2 46.38 5.25 1.9579 4 1 0 2 46.55 1.37 1.9508 -1 -6 3 2 46.60 13.45 1.9490 1 4 2 2 46.72 2.11 1.9442 0 0 4 2 46.76 1.22 1.9429 2 -2 3 2 46.76 1.25 1.9426 3 -1 2 2 46.96 1.18 1.9348 3 -3 2 2 47.12 1.17 1.9289 -1 4 3 2 47.27 1.37 1.9230 2 -3 3 2 47.36 2.69 1.9197 2 -1 3 2 47.38 3.24 1.9186 -4 4 0 2 47.89 6.02 1.8993 3 4 0 2 48.00 6.21 1.8954 -2 -6 1 2 48.01 1.51 1.8950 -3 6 0 2 48.30 1.03 1.8843 0 -7 2 2 48.70 4.09 1.8698 -4 -3 1 2 48.82 1.80 1.8656 -4 0 4 2 48.86 4.57 1.8639 2 -4 3 2 49.03 2.74 1.8578 2 0 3 2 49.27 1.11 1.8494 0 7 0 2 49.60 1.27 1.8378 1 -7 2 2 49.66 2.23 1.8359 1 -6 3 2 49.90 2.71 1.8275 -1 -7 1 2 49.91 7.16 1.8273 -4 5 1 2 50.15 2.23 1.8191 2 -7 1 2 50.19 4.50 1.8177 3 -6 1 2 50.30 1.44 1.8140 0 -5 4 2 50.46 3.07 1.8088 1 -2 4 2 50.80 2.16 1.7972 1 -3 4 2 51.54 5.52 1.7731 -5 2 1 2 51.64 1.36 1.7699 -5 -1 2 2 51.64 1.06 1.7699 1 3 3 2 51.65 1.88 1.7696 2 5 1 2 51.68 4.92 1.7689 -2 5 3 2 51.68 2.68 1.7688 -5 0 3 2 51.71 4.28 1.7676 2 1 3 2 51.74 3.62 1.7669 4 -4 1 2 51.79 2.47 1.7652 -3 3 4 2 51.81 2.53 1.7645 -1 7 1 2 51.91 1.97 1.7613 -4 -3 4 2 51.92 5.68 1.7612 -5 1 3 2 52.02 1.23 1.7579 -4 2 4 2 52.06 3.14 1.7567 -4 4 3 2 52.14 2.58 1.7542 -2 7 1 2 52.22 2.46 1.7517 0 -7 3 2 52.73 1.23 1.7359 1 5 2 2 52.88 1.98 1.7314 1 0 4 2 53.00 1.55 1.7277 -1 5 3 2 53.02 1.53 1.7273 -3 -5 4 2 53.36 1.36 1.7168 -3 -6 2 2 53.43 3.12 1.7148 4 3 0 2 53.66 7.54 1.7081 -5 -1 1 2 53.69 2.02 1.7071 -1 -1 5 2 53.75 1.36 1.7054 -1 -3 5 2 53.85 1.36 1.7025 -3 0 5 2 53.97 2.89 1.6991 -2 -6 4 2 54.26 1.63 1.6905 -5 -2 3 2 54.39 4.31 1.6868 1 -8 1 2 54.42 5.55 1.6860 -3 -3 5 2 54.50 1.25 1.6836 4 -5 1 2 54.54 2.49 1.6825 1 -5 4 2 54.64 1.42 1.6796 0 -8 1 2 54.68 2.37 1.6787 -4 6 1 2 54.93 4.26 1.6715 -4 -4 4 2 55.07 1.12 1.6676 -2 -7 3 2 55.35 1.76 1.6600 3 -7 1 2 55.54 1.69 1.6546 -5 4 2 2 55.65 1.16 1.6515 -3 1 5 2 55.79 2.36 1.6477 -5 3 0 2 55.94 1.48 1.6438 -4 -5 2 2 55.98 4.01 1.6425 1 -8 2 2 56.16 1.20 1.6377 -3 4 4 2 56.23 1.39 1.6359 5 0 0 2 56.25 1.89 1.6354 3 -3 3 2 56.33 1.29 1.6334 -5 -2 1 2 56.42 1.06 1.6308 -5 1 4 2 56.43 1.56 1.6306 4 2 1 2 56.58 3.70 1.6267 -3 -4 5 2 56.61 2.32 1.6258 2 -8 1 2 56.97 5.25 1.6164 3 -1 3 2 57.71 1.52 1.5975 0 -1 5 2 57.74 1.61 1.5966 -1 -5 5 2 57.80 1.52 1.5951 1 -6 4 2 57.87 3.33 1.5935 -2 6 3 2 58.06 2.32 1.5888 -5 2 4 2 58.10 4.86 1.5876 2 -2 4 2 58.17 1.32 1.5859 4 4 0 2 58.27 2.28 1.5833 0 -8 3 2 58.28 1.86 1.5831 0 -4 5 2 58.41 1.15 1.5800 -4 -3 5 2 58.53 2.35 1.5771 4 -4 2 2 58.67 1.67 1.5736 3 3 2 2 58.74 3.28 1.5718 -1 -8 3 2 58.85 2.53 1.5692 -3 7 2 2 59.29 1.54 1.5585 2 -7 3 2 59.32 3.81 1.5578 -2 8 1 2 59.42 1.55 1.5554 0 0 5 2 59.52 2.63 1.5531 -5 -3 4 2 59.53 5.89 1.5529 3 -7 2 2 60.10 1.82 1.5395 -3 8 0 2 60.64 1.92 1.5271 -2 -8 2 2 60.68 1.84 1.5262 -4 2 5 2 61.07 1.49 1.5173 -1 -6 5 2 61.11 2.67 1.5165 -5 -4 2 2 61.14 1.86 1.5158 -2 -6 5 2 61.26 3.76 1.5132 -3 5 4 2 61.27 4.93 1.5129 5 2 0 2 61.40 3.11 1.5099 5 -1 1 2 61.55 3.30 1.5068 -4 -6 2 2 61.55 3.27 1.5067 -2 -8 3 2 62.03 5.15 1.4961 0 1 5 2 62.06 4.25 1.4955 -5 -1 5 2 62.31 3.96 1.4902 -2 3 5 2 62.48 1.00 1.4864 5 -4 1 2 62.55 2.15 1.4849 4 -7 1 2 62.75 3.59 1.4807 -4 7 2 2 62.90 1.23 1.4775 -3 -7 4 2 63.15 2.80 1.4723 -6 1 1 2 63.41 1.05 1.4670 -1 5 4 2 63.43 1.75 1.4665 1 3 4 2 63.60 1.10 1.4630 -5 6 2 2 63.65 1.11 1.4619 -3 -2 6 2 63.87 2.56 1.4573 -4 3 5 2 63.90 2.25 1.4569 -3 -1 6 2 64.25 1.83 1.4498 -6 3 3 2 64.31 1.96 1.4485 -3 -3 6 2 64.51 1.11 1.4444 -5 -3 5 2 64.86 1.09 1.4376 0 -9 3 2 64.94 1.33 1.4360 -1 3 5 2 65.07 1.89 1.4335 -3 7 3 2 65.11 1.39 1.4326 -1 -9 1 2 65.18 2.80 1.4313 1 -5 5 2 65.20 1.79 1.4309 -1 -7 5 2 65.33 1.12 1.4283 4 4 1 2 65.40 1.99 1.4270 -6 -2 2 2 65.49 1.45 1.4253 -1 8 2 2 65.56 2.43 1.4239 -2 -7 5 2 66.23 1.83 1.4110 1 8 1 2 66.41 1.62 1.4077 2 8 0 2 66.46 1.68 1.4069 -6 -2 4 2 66.47 1.81 1.4065 -5 -5 4 2 66.51 2.73 1.4058 -1 -1 6 2 66.68 2.89 1.4026 1 -8 4 2 66.79 3.09 1.4007 4 -2 3 2 67.26 1.97 1.3921 2 2 4 2 67.26 1.36 1.3920 2 -7 4 2 67.29 1.72 1.3914 -2 -5 6 2 67.49 1.60 1.3877 3 -9 1 2 67.62 3.19 1.3855 -6 3 0 2 67.99 1.02 1.3789 -5 3 5 2 68.03 2.91 1.3781 -4 -6 5 2 68.53 1.28 1.3693 -2 -9 3 2 68.71 2.00 1.3661 0 8 2 2 68.95 1.93 1.3620 -6 4 0 2 69.13 2.65 1.3589 1 6 3 2 69.43 1.60 1.3537 -6 0 5 2 69.69 1.16 1.3493 0 9 1 2 69.76 2.26 1.3482 -1 4 5 2 69.97 1.98 1.3445 0 -2 6 2 70.21 1.63 1.3406 0 7 3 2 70.83 1.55 1.3303 4 5 1 2 70.88 1.49 1.3295 -4 -7 1 2 70.97 1.28 1.3281 -6 4 4 2 71.25 1.37 1.3235 5 -5 2 2 71.30 1.29 1.3227 -5 -6 2 2 71.31 1.21 1.3225 4 -6 3 2 71.55 1.31 1.3187 5 0 2 2 71.60 1.48 1.3179 2 -8 4 2 71.71 1.01 1.3162 -6 2 5 2 71.87 1.49 1.3136 -6 6 1 2 71.96 1.35 1.3122 0 -10 3 2 71.96 2.01 1.3122 -4 9 0 2 72.18 1.20 1.3088 1 -9 4 2 72.60 1.22 1.3022 -4 5 5 2 72.77 2.92 1.2996 -7 1 3 2 73.09 2.54 1.2946 0 10 0 2 73.13 1.05 1.2940 -7 0 3 2 73.41 2.77 1.2898 3 1 4 2 73.71 1.80 1.2853 -1 8 3 2 73.73 1.27 1.2850 -5 -4 6 2 74.32 1.23 1.2763 2 9 0 2 74.42 1.49 1.2748 3 -10 1 2 74.71 1.29 1.2706 -4 -8 4 2 75.34 1.32 1.2615 -6 -5 3 2 75.36 1.60 1.2612 -3 -9 4 2 75.77 1.12 1.2554 -3 -3 7 2 76.26 1.68 1.2486 -6 -4 1 2 76.28 1.52 1.2483 4 7 0 2 76.51 1.25 1.2452 -2 -9 5 2 77.31 1.71 1.2342 -6 4 5 2 77.89 1.38 1.2265 4 -4 4 2 77.92 1.10 1.2261 -6 7 0 2 78.67 1.35 1.2163 6 -6 1 2 79.57 1.14 1.2047 -6 2 6 2 80.28 2.19 1.1958 -4 1 7 2 80.82 1.13 1.1892 -1 -5 7 2 84.43 1.03 1.1474 -2 -11 2 2 85.02 1.31 1.1409 3 -7 5 2 85.40 1.41 1.1368 6 -6 2 2 85.45 1.53 1.1363 -6 -2 7 2 87.06 1.15 1.1193 7 -3 1 2 87.32 1.09 1.1166 1 5 5 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.