Nasinite Corazza E, Menchetti S, Sabelli C Acta Crystallographica B31 (1975) 2405-2410 The crystal structure of nasinite, Na2[B5O8(OH)]*2H2O Locality: synthetic _database_code_amcsd 0009544 CELL PARAMETERS: 12.0150 6.5180 11.1730 90.000 90.000 90.000 SPACE GROUP: Pna2_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 875.000 Density (g/cm3): 2.133 MAX. ABS. INTENSITY / VOLUME**2: 2.248230640 RIR: 0.343 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.75 83.57 6.0075 2 0 0 2 15.47 1.30 5.7293 1 1 0 4 15.86 68.99 5.5865 0 0 2 1 16.76 100.00 5.2912 2 0 1 2 17.39 17.00 5.0981 1 1 1 4 20.10 8.03 4.4174 2 1 0 4 21.63 1.27 4.1080 2 1 1 4 21.72 26.57 4.0910 2 0 2 2 22.23 26.26 3.9998 1 1 2 4 25.71 13.72 3.4650 2 1 2 4 26.11 10.17 3.4123 3 1 0 4 27.33 5.93 3.2635 3 1 1 4 27.58 38.62 3.2337 0 1 3 2 28.19 16.66 3.1654 2 0 3 2 28.38 2.83 3.1453 1 2 0 4 28.59 16.75 3.1226 1 1 3 4 29.50 66.74 3.0277 1 2 1 4 29.74 55.12 3.0038 4 0 0 2 30.70 7.44 2.9120 3 1 2 4 30.82 71.54 2.9008 4 0 1 2 31.22 26.66 2.8646 2 2 0 4 31.42 2.36 2.8474 2 1 3 4 31.79 44.41 2.8150 0 2 2 2 32.04 31.07 2.7933 0 0 4 1 32.67 11.34 2.7408 1 2 2 4 33.82 21.76 2.6502 4 1 1 4 35.21 6.38 2.5490 2 2 2 4 35.44 20.30 2.5328 2 0 4 2 35.51 3.20 2.5278 3 2 0 4 35.69 4.73 2.5160 3 1 3 4 35.76 30.98 2.5107 1 1 4 4 36.66 27.16 2.4513 4 1 2 4 37.42 13.42 2.4030 1 2 3 4 38.12 3.57 2.3609 2 1 4 4 38.50 3.16 2.3381 4 0 3 2 39.11 5.37 2.3030 3 2 2 4 39.69 5.13 2.2706 2 2 3 4 39.99 13.44 2.2547 5 1 0 4 40.83 15.38 2.2101 5 1 1 4 40.86 1.76 2.2087 4 2 0 4 41.01 17.24 2.2008 4 1 3 4 42.27 14.11 2.1380 1 3 0 4 42.38 12.22 2.1327 0 3 1 2 42.63 4.15 2.1209 0 2 4 2 43.08 12.08 2.0999 1 3 1 4 43.20 4.09 2.0944 2 0 5 2 43.27 10.19 2.0908 5 1 2 4 43.32 13.54 2.0886 1 2 4 4 43.47 27.87 2.0819 1 1 5 4 44.09 16.81 2.0540 4 2 2 4 44.28 6.67 2.0455 4 0 4 2 44.34 2.52 2.0432 2 3 0 4 45.11 13.11 2.0098 2 3 1 4 45.28 2.95 2.0025 6 0 0 2 45.35 11.34 1.9999 2 2 4 4 45.42 6.46 1.9968 1 3 2 4 45.49 27.00 1.9940 2 1 5 4 46.05 2.12 1.9711 6 0 1 2 46.53 1.15 1.9517 4 1 4 4 47.12 10.77 1.9288 5 1 3 4 47.38 2.60 1.9188 2 3 2 4 47.50 3.69 1.9142 6 1 0 4 47.72 2.97 1.9057 5 2 1 4 47.88 7.36 1.8998 4 2 3 4 48.23 1.24 1.8867 6 1 1 4 48.28 6.72 1.8851 6 0 2 2 48.35 9.21 1.8825 3 3 1 4 48.51 2.32 1.8767 0 3 3 2 48.58 8.62 1.8743 3 2 4 4 48.71 7.42 1.8694 3 1 5 4 49.14 2.31 1.8542 1 3 3 4 49.90 19.53 1.8277 5 2 2 4 50.07 4.95 1.8217 1 2 5 4 50.39 8.58 1.8108 6 1 2 4 50.51 4.98 1.8071 3 3 2 4 50.93 1.04 1.7929 4 0 5 2 50.98 1.36 1.7913 2 3 3 4 51.37 1.64 1.7787 2 0 6 2 51.61 3.96 1.7710 1 1 6 4 51.84 3.24 1.7637 6 0 3 2 52.13 2.92 1.7544 5 1 4 4 52.63 5.45 1.7390 4 3 1 4 52.84 8.33 1.7325 4 2 4 4 53.38 3.41 1.7164 5 2 3 4 53.39 5.02 1.7159 2 1 6 4 53.72 2.15 1.7062 6 2 0 4 53.85 6.55 1.7025 6 1 3 4 53.96 4.49 1.6994 3 3 3 4 54.01 3.62 1.6978 1 3 4 4 54.40 2.46 1.6866 6 2 1 4 54.66 2.18 1.6790 4 3 2 4 54.83 3.00 1.6742 3 2 5 4 56.01 4.07 1.6418 7 1 1 4 56.28 4.04 1.6346 3 1 6 4 56.39 1.34 1.6318 6 2 2 4 56.95 4.46 1.6168 0 2 6 2 57.52 1.44 1.6024 1 2 6 4 57.68 2.59 1.5981 1 4 1 4 57.80 1.73 1.5951 5 3 1 4 57.96 3.51 1.5911 7 1 2 4 58.12 1.05 1.5871 5 1 5 4 58.30 2.78 1.5827 4 0 6 2 58.45 3.10 1.5790 6 1 4 4 58.55 3.28 1.5765 3 3 4 4 58.71 1.09 1.5727 2 4 0 4 59.33 2.60 1.5577 0 3 5 2 59.72 1.11 1.5485 5 3 2 4 61.13 1.45 1.5161 7 1 3 4 61.23 2.98 1.5138 2 4 2 4 61.80 1.47 1.5012 2 1 7 4 62.05 1.06 1.4958 3 4 1 4 62.35 1.58 1.4893 4 3 4 4 63.57 3.80 1.4635 8 1 0 4 63.89 2.53 1.4571 3 4 2 4 63.94 1.27 1.4560 6 2 4 4 64.18 1.57 1.4511 8 1 1 4 64.30 1.98 1.4488 2 4 3 4 64.45 1.89 1.4458 3 1 7 4 64.95 1.45 1.4358 5 1 6 4 65.56 1.71 1.4238 6 3 2 4 65.59 1.41 1.4234 1 2 7 4 65.99 1.42 1.4157 8 1 2 4 66.49 1.41 1.4063 7 2 3 4 66.94 1.26 1.3979 1 4 4 4 68.05 1.36 1.3777 4 1 7 4 68.46 2.38 1.3704 2 4 4 4 68.85 3.59 1.3637 6 0 6 2 69.24 1.32 1.3569 1 1 8 4 69.67 1.51 1.3496 3 2 7 4 70.56 1.96 1.3348 6 1 6 4 70.59 1.25 1.3342 7 2 4 4 70.70 1.27 1.3325 7 1 5 4 72.04 1.12 1.3110 5 4 2 4 72.24 1.21 1.3078 9 1 0 4 74.44 1.26 1.2745 4 4 4 4 74.51 1.24 1.2734 9 1 2 4 74.99 3.16 1.2666 7 3 3 4 75.00 1.60 1.2664 4 0 8 2 75.04 1.95 1.2658 2 5 1 4 75.77 1.12 1.2554 2 2 8 4 76.73 1.11 1.2421 2 5 2 4 77.33 1.25 1.2340 9 1 3 4 77.42 1.62 1.2328 6 4 2 4 77.59 1.13 1.2304 0 5 3 2 77.93 1.90 1.2259 6 1 7 4 78.08 2.47 1.2240 1 5 3 4 78.38 2.32 1.2200 1 4 6 4 78.90 2.44 1.2133 1 1 9 4 79.14 1.93 1.2102 3 5 2 4 79.45 1.29 1.2062 9 2 2 4 79.83 4.76 1.2015 2 4 6 4 80.34 1.02 1.1951 2 1 9 4 80.83 1.27 1.1890 4 5 1 4 81.44 1.03 1.1818 7 4 0 4 83.64 1.96 1.1562 7 4 2 4 83.65 1.52 1.1560 10 1 2 4 85.23 1.29 1.1386 4 5 3 4 85.89 1.80 1.1316 9 3 1 4 86.29 1.04 1.1273 3 3 8 4 87.55 1.21 1.1143 3 2 9 4 88.61 1.03 1.1037 10 0 4 2 89.63 1.50 1.0938 8 0 7 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.