Zn5(P3O10)2(H2O)17 Averbuch-Pouchot M, Durif A, Guitel J Acta Crystallographica B31 (1975) 2482-2486 Structure cristalline du tripolyphosphate de zinc heptadecahydrate: Zn5(P3O10)2(H2O)17 _cod_database_code 1007252 _database_code_amcsd 0015934 CELL PARAMETERS: 10.7660 10.3160 8.5250 111.390 115.080 70.190 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 779.167 Density (g/cm3): 2.354 MAX. ABS. INTENSITY / VOLUME**2: 10.45479416 RIR: 1.446 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.29 19.85 9.5152 1 0 0 2 9.44 39.11 9.3732 0 1 0 2 11.72 25.46 7.5536 1 1 0 2 11.87 15.22 7.4569 0 0 1 2 12.01 5.63 7.3671 -1 -1 1 2 12.32 100.00 7.1857 -1 0 1 2 13.11 11.52 6.7508 0 -1 1 2 14.64 1.35 6.0492 -1 1 0 2 17.05 15.95 5.1990 -2 -1 1 2 17.44 24.30 5.0839 1 0 1 2 17.79 37.24 4.9846 -1 -2 1 2 18.36 8.01 4.8315 -2 0 1 2 18.94 17.95 4.6866 0 2 0 2 18.98 27.01 4.6747 2 1 0 2 19.19 13.59 4.6239 1 2 0 2 19.36 19.36 4.5859 1 -1 1 2 20.37 3.25 4.3604 1 1 1 2 20.62 2.88 4.3066 -2 -2 1 2 20.89 2.08 4.2528 -1 -1 2 2 22.43 12.43 3.9635 -1 0 2 2 22.53 5.50 3.9466 -2 -1 2 2 22.73 15.23 3.9114 -2 1 0 2 22.91 7.15 3.8815 -1 2 0 2 23.28 9.17 3.8216 0 -1 2 2 23.56 1.41 3.7768 2 2 0 2 23.78 15.33 3.7412 -2 1 1 2 23.87 9.40 3.7284 0 0 2 2 24.16 2.13 3.6836 -2 -2 2 2 24.78 2.20 3.5929 -2 0 2 2 24.81 2.28 3.5884 -3 -1 1 2 24.92 7.38 3.5724 0 2 1 2 25.43 4.64 3.5031 2 0 1 2 25.95 15.02 3.4333 -1 -3 1 2 26.41 5.77 3.3754 0 -2 2 2 26.50 15.80 3.3633 -3 0 1 2 26.70 2.91 3.3393 -3 -2 1 2 27.46 7.14 3.2481 -1 1 2 2 27.52 2.75 3.2410 -3 -1 2 2 27.95 10.41 3.1919 0 -3 1 2 27.95 2.67 3.1917 0 1 2 2 28.04 6.77 3.1817 1 3 0 2 28.13 5.32 3.1717 3 0 0 2 28.19 2.25 3.1655 -3 -2 2 2 28.55 4.27 3.1265 1 0 2 2 28.75 8.04 3.1047 1 -1 2 2 29.53 1.88 3.0246 -2 2 0 2 30.09 12.95 2.9700 -3 0 2 2 30.11 5.99 2.9683 -2 1 2 2 30.38 8.96 2.9421 3 2 0 2 30.61 6.79 2.9209 2 3 0 2 31.23 11.82 2.8641 -3 1 1 2 31.28 6.29 2.8600 2 2 1 2 31.35 7.44 2.8535 -2 2 1 2 31.46 11.55 2.8440 1 1 2 2 31.56 5.85 2.8345 -3 -3 1 2 31.91 16.61 2.8043 -3 -3 2 2 31.94 1.99 2.8019 -2 -1 3 2 32.01 5.03 2.7957 1 -2 2 2 32.04 8.10 2.7937 -1 -1 3 2 32.21 1.15 2.7794 -2 -2 3 2 32.26 6.87 2.7753 0 -3 2 2 32.73 5.00 2.7363 1 -3 1 2 32.92 10.95 2.7206 -1 -2 3 2 33.58 1.94 2.6687 -4 -1 1 2 34.40 1.19 2.6068 0 2 2 2 34.45 5.16 2.6035 -4 -2 1 2 34.54 1.35 2.5968 -4 -1 2 2 34.59 1.79 2.5934 -1 2 2 2 34.86 8.16 2.5737 0 -1 3 2 35.00 13.81 2.5634 -1 -4 1 2 35.25 6.79 2.5458 -3 1 2 2 35.46 2.38 2.5314 -4 0 1 2 35.66 1.22 2.5179 3 3 0 2 35.78 3.39 2.5096 -1 3 1 2 36.04 1.89 2.4923 -2 -4 2 2 36.14 5.70 2.4856 0 0 3 2 36.25 2.27 2.4781 0 -2 3 2 36.50 1.83 2.4616 3 -1 1 2 36.81 4.64 2.4418 1 2 2 2 36.90 1.89 2.4361 4 1 0 2 37.47 1.13 2.4004 1 4 0 2 37.55 3.52 2.3952 -3 0 3 2 37.74 3.59 2.3835 -2 3 0 2 37.82 4.22 2.3788 4 0 0 2 37.89 2.49 2.3746 3 2 1 2 37.90 4.65 2.3741 -4 -3 1 2 38.40 1.07 2.3440 -3 -4 1 2 39.50 1.41 2.2814 -4 -1 3 2 40.07 3.28 2.2503 0 -3 3 2 40.28 1.06 2.2391 -4 -3 3 2 40.53 2.10 2.2256 1 0 3 2 40.53 2.88 2.2256 -2 -4 3 2 41.01 6.59 2.2008 3 -2 1 2 41.65 1.22 2.1684 1 -2 3 2 41.96 1.49 2.1533 -4 -4 2 2 42.11 3.28 2.1458 -4 1 2 2 42.19 1.82 2.1418 -3 2 2 2 42.22 2.23 2.1405 -5 -2 2 2 42.67 2.65 2.1190 3 4 0 2 43.05 3.88 2.1011 -2 -1 4 2 43.38 2.18 2.0861 0 4 1 2 43.40 3.34 2.0849 -4 -4 1 2 43.49 2.45 2.0811 1 4 1 2 43.85 1.08 2.0647 1 3 2 2 44.24 1.55 2.0473 -2 -3 4 2 44.42 3.38 2.0393 -3 -3 4 2 44.46 3.35 2.0377 3 1 2 2 44.58 2.47 2.0325 2 -3 2 2 44.60 1.39 2.0315 -1 -5 1 2 44.94 1.20 2.0170 -5 0 1 2 45.36 1.95 1.9993 -3 -5 2 2 45.73 1.88 1.9838 2 4 1 2 45.78 1.13 1.9822 4 2 1 2 45.88 1.61 1.9778 -4 2 1 2 46.03 2.66 1.9717 -3 3 1 2 46.07 2.02 1.9701 -5 -1 3 2 46.43 3.02 1.9557 -4 2 0 2 47.33 1.14 1.9206 1 5 0 2 47.47 4.49 1.9152 5 2 0 2 47.52 1.32 1.9135 2 -4 1 2 47.59 8.10 1.9108 0 -2 4 2 47.79 1.39 1.9030 5 0 0 2 47.80 4.75 1.9030 -5 -4 2 2 48.19 1.22 1.8884 4 4 0 2 48.35 1.01 1.8826 1 2 3 2 48.57 1.21 1.8745 2 -2 3 2 48.85 2.34 1.8642 0 0 4 2 48.86 1.81 1.8639 2 1 3 2 48.98 1.54 1.8598 -5 1 1 2 49.40 6.20 1.8447 -2 4 1 2 49.49 1.94 1.8418 -4 -4 4 2 49.76 4.34 1.8324 -4 -5 3 2 50.44 6.48 1.8092 -2 1 4 2 50.83 4.74 1.7964 -4 0 4 2 50.89 1.34 1.7942 1 -5 1 2 51.42 2.67 1.7770 2 -4 2 2 52.39 1.12 1.7464 -1 3 3 2 52.76 3.70 1.7351 -6 -1 1 2 52.76 2.05 1.7350 3 3 2 2 53.01 3.76 1.7276 0 -5 3 2 53.07 1.04 1.7255 1 5 1 2 53.08 2.31 1.7253 -5 -4 4 2 53.21 1.28 1.7215 1 0 4 2 53.39 2.05 1.7161 -4 3 1 2 53.40 3.52 1.7159 0 5 1 2 54.21 1.07 1.6921 -2 -6 1 2 54.36 1.51 1.6878 -3 -3 5 2 54.37 4.06 1.6874 -5 1 3 2 54.91 1.31 1.6722 -6 0 1 2 55.37 2.37 1.6592 4 5 0 2 55.41 2.57 1.6583 -3 -1 5 2 55.55 1.54 1.6543 -2 -6 3 2 55.55 1.34 1.6543 -3 -6 1 2 55.70 2.00 1.6503 3 1 3 2 55.99 1.35 1.6424 -5 -5 1 2 56.00 2.24 1.6420 5 -1 1 2 56.07 2.76 1.6402 -1 -5 4 2 56.24 2.12 1.6356 -1 -2 5 2 56.52 1.23 1.6283 -4 3 2 2 56.64 2.35 1.6252 -6 -3 4 2 56.72 1.12 1.6231 6 1 0 2 57.01 1.19 1.6154 0 -6 1 2 57.75 1.04 1.5963 -6 -4 1 2 57.85 1.13 1.5939 5 3 1 2 58.06 1.33 1.5886 2 -4 3 2 58.42 1.01 1.5797 2 -1 4 2 58.83 1.13 1.5697 -6 1 1 2 60.35 1.77 1.5338 -5 -6 2 2 60.70 1.30 1.5258 -3 -5 5 2 60.95 1.24 1.5200 -7 -3 2 2 60.97 1.75 1.5196 -4 0 5 2 61.05 1.23 1.5179 -4 -5 5 2 61.52 2.31 1.5074 -7 -1 2 2 61.55 3.02 1.5067 2 1 4 2 62.30 1.96 1.4904 -1 6 0 2 62.63 2.16 1.4833 4 0 3 2 62.82 2.19 1.4792 4 5 1 2 63.88 1.04 1.4573 5 2 2 2 64.23 1.03 1.4501 -2 3 4 2 64.34 1.64 1.4479 2 6 1 2 64.96 1.15 1.4355 -6 -6 3 2 65.08 1.02 1.4333 -1 -5 5 2 65.11 1.04 1.4326 -4 -7 3 2 66.15 1.53 1.4126 -4 1 5 2 68.59 1.17 1.3681 2 -6 2 2 68.61 1.90 1.3679 1 7 0 2 68.71 1.21 1.3661 -5 3 3 2 69.64 1.02 1.3502 0 -5 5 2 70.26 1.58 1.3397 -5 1 5 2 71.19 1.02 1.3245 -1 -6 5 2 73.22 1.19 1.2927 1 -6 4 2 73.26 1.21 1.2921 2 -6 3 2 73.32 1.88 1.2912 -8 -2 1 2 74.08 1.18 1.2798 -5 -7 5 2 74.75 1.06 1.2701 -2 -8 3 2 75.52 1.24 1.2589 6 6 0 2 76.77 1.02 1.2416 -7 -3 6 2 76.89 1.18 1.2399 3 3 4 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.