Gladite
Kohatsu I, Wuensch B J
Acta Crystallographica B32 (1976) 2401-2409
The crystal structure of gladite, PbCuBi5S9, a superstructure intermediate in
the series Bi2S3-PbCuBiS3 (bismuthinite-aikinite)
_database_code_amcsd 0009571
33.531 11.486 4.003 90 90 90 Pbnm
atom     x     y   z B(1,1) B(2,2) B(3,3)  B(1,2) B(1,3) B(2,3)
Pb   .3349 .3174 .25 .00020  .0028    .02 -.00022      0      0
Cu   .2390 .2200 .25 .00012  .0005   .006  .00002      0      0
Bi1  .0565 .0209 .25 .00025  .0020   .011   .0001      0      0
Bi2  .3924 .0056 .25 .00030  .0027   .016  .00007      0      0
Bi3  .7294 .0283 .25 .00045  .0016    .01 -.00005      0      0
Bi4  .6550 .3542 .25 .00034  .0033   .019  .00018      0      0
Bi5  .9866 .3430 .25 .00019  .0025   .019  .00002      0      0
S1   .2095 .0354 .25 .00019  .0014    .01 -.00011      0      0
S2   .5415 .0552 .25 .00041  .0031    .03 -.00008      0      0
S3   .8804 .0565 .25 .00022  .0027    .02  .00007      0      0
S4   .1855 .3786 .25 .00008  .0011   .011  .00004      0      0
S5   .5172 .3760 .25 .00026  .0028   .022  .00004      0      0
S6   .8511 .3917 .25 .00046  .0035    .02 -.00016      0      0
S7   .1006 .2158 .25 .00001  .0005   .001 -.00004      0      0
S8   .4344 .2038 .25 .00039  .0034   .039 -.00006      0      0
S9   .7669 .2290 .25 .00045  .0037   .028  .00006      0      0