H8 Mo N2 S4 Belougne P, Chezeau N, Lapasset J Acta Crystallographica B32 (1976) 3087-3088 Nouvel affinement de la structure cristalline du thiomolybdate d'ammonium _cod_database_code 1004019 _database_code_amcsd 0009578 CELL PARAMETERS: 9.5700 6.9900 12.2000 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 816.110 Density (g/cm3): 2.052 MAX. ABS. INTENSITY / VOLUME**2: 29.23320456 RIR: 4.638 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.52 10.04 6.1000 0 0 2 2 14.61 10.20 6.0650 0 1 1 4 17.24 41.60 5.1439 1 0 2 4 17.31 100.00 5.1229 1 1 1 8 18.54 23.36 4.7850 2 0 0 2 19.93 1.37 4.4546 2 0 1 4 21.45 2.11 4.1430 1 1 2 8 23.63 8.38 3.7649 2 0 2 4 23.68 1.37 3.7566 2 1 1 8 25.34 19.04 3.5151 0 1 3 4 25.49 13.57 3.4950 0 2 0 2 28.15 5.16 3.1702 1 2 1 8 28.93 11.43 3.0862 3 0 1 4 29.28 16.02 3.0500 0 0 4 2 29.45 8.52 3.0325 0 2 2 4 30.77 2.18 2.9060 1 0 4 4 31.58 3.98 2.8329 2 1 3 8 31.69 19.17 2.8233 3 1 1 8 31.70 4.49 2.8223 2 2 0 4 32.56 10.58 2.7497 2 2 1 8 34.88 1.08 2.5719 2 0 4 4 35.03 7.41 2.5614 2 2 2 8 35.13 4.60 2.5544 1 2 3 8 35.77 5.50 2.5099 3 0 3 4 37.59 2.19 2.3925 4 0 0 2 38.84 3.38 2.3186 2 2 3 8 39.10 2.92 2.3037 0 1 5 4 40.27 7.59 2.2397 1 1 5 8 40.36 8.25 2.2345 1 2 4 8 40.50 2.64 2.2273 4 0 2 4 40.53 10.37 2.2259 1 3 1 8 40.53 1.20 2.2256 4 1 1 8 40.94 3.66 2.2045 3 0 4 4 41.07 2.01 2.1979 3 2 2 8 43.61 3.90 2.0757 2 1 5 8 44.56 1.19 2.0333 0 0 6 2 44.83 3.64 2.0217 0 3 3 4 45.88 4.98 1.9778 4 1 3 8 45.97 10.81 1.9742 4 2 0 4 46.88 1.28 1.9381 3 0 5 4 48.46 1.44 1.8783 4 2 2 8 48.66 2.29 1.8714 2 0 6 4 48.76 2.49 1.8676 3 1 5 8 48.84 2.74 1.8646 3 2 4 8 48.91 1.19 1.8623 2 3 3 8 48.98 4.84 1.8596 3 3 1 8 49.37 2.50 1.8458 2 2 5 8 49.97 6.64 1.8253 5 1 1 8 52.03 5.41 1.7575 0 2 6 4 52.36 5.86 1.7475 0 4 0 2 52.97 3.70 1.7286 1 2 6 8 53.44 1.21 1.7146 3 0 6 4 55.15 3.59 1.6653 1 1 7 8 55.36 2.71 1.6596 1 3 5 8 55.36 1.75 1.6595 4 1 5 8 55.44 3.52 1.6573 4 2 4 8 55.54 2.90 1.6546 1 4 2 8 55.72 4.55 1.6498 2 2 6 8 56.02 1.90 1.6415 2 4 0 4 56.79 2.07 1.6212 5 0 4 4 56.89 8.26 1.6186 5 2 2 8 58.03 1.49 1.5894 2 3 5 8 58.20 1.06 1.5851 2 4 2 8 59.68 2.42 1.5494 4 0 6 4 59.90 1.99 1.5442 4 3 3 8 60.92 1.76 1.5207 3 4 1 8 61.12 2.62 1.5163 0 4 4 4 62.12 2.07 1.4941 3 1 7 8 62.32 1.07 1.4900 3 3 5 8 63.16 2.73 1.4722 5 1 5 8 63.35 2.79 1.4682 5 3 1 8 64.19 1.64 1.4510 6 2 0 4 65.03 1.31 1.4341 3 4 3 8 65.95 1.02 1.4164 4 2 6 8 67.87 1.63 1.3810 1 3 7 8 68.23 1.70 1.3745 1 5 1 8 68.52 1.26 1.3694 3 4 4 8 70.14 1.35 1.3417 2 2 8 8 74.16 1.16 1.2786 3 3 7 8 74.26 1.03 1.2772 2 4 6 8 74.51 1.16 1.2734 3 5 1 8 74.94 1.17 1.2673 5 1 7 8 75.11 1.48 1.2648 5 3 5 8 80.88 1.27 1.1885 5 4 4 8 83.36 1.63 1.1593 4 4 6 8 84.77 1.23 1.1436 1 2 10 8 86.60 1.11 1.1241 5 5 1 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.