Pb3(P3O9)2(H2O)3 Brunel-Lauegt M, Tordjman I, Durif A Acta Crystallographica B32 (1976) 3246-3249 Structure cristalline du trimetaphosphate de plomb trihydrate, Pb3(P3O9)2(H2O)3 _cod_database_code 1007250 _database_code_amcsd 0015932 CELL PARAMETERS: 11.9570 11.9570 12.2700 90.000 90.000 90.000 SPACE GROUP: P4_12_12 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1754.240 Density (g/cm3): 4.329 MAX. ABS. INTENSITY / VOLUME**2: 58.82411754 RIR: 4.425 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.33 9.18 8.5634 1 0 1 8 10.46 11.08 8.4549 1 1 0 4 14.82 2.84 5.9785 2 0 0 4 16.24 7.27 5.4584 1 0 2 8 16.49 30.45 5.3745 2 0 1 8 16.58 8.08 5.3473 2 1 0 8 17.86 22.97 4.9655 1 1 2 8 18.10 100.00 4.9020 2 1 1 8 21.01 6.80 4.2274 2 2 0 4 22.05 24.15 4.0310 2 1 2 8 22.24 13.30 3.9969 2 2 1 8 22.98 1.33 3.8699 1 0 3 8 24.17 39.60 3.6818 1 1 3 8 24.64 4.18 3.6135 3 1 1 8 25.59 19.06 3.4810 2 2 2 8 26.67 30.45 3.3423 3 0 2 8 26.88 28.91 3.3163 3 2 0 8 27.45 11.13 3.2487 2 1 3 8 27.71 39.85 3.2189 3 1 2 8 27.87 6.12 3.2014 3 2 1 8 29.11 20.07 3.0675 0 0 4 2 29.89 31.57 2.9892 4 0 0 4 30.08 9.90 2.9713 1 0 4 8 30.41 7.80 2.9395 2 2 3 8 30.65 10.83 2.9173 3 2 2 8 30.79 16.50 2.9043 4 0 1 8 30.83 11.86 2.9000 4 1 0 8 31.34 2.44 2.8545 3 0 3 8 32.24 19.55 2.7764 3 1 3 8 33.52 1.28 2.6737 4 2 0 8 33.68 3.30 2.6608 2 1 4 8 34.33 13.28 2.6124 4 2 1 8 34.83 17.61 2.5759 3 2 3 8 35.04 9.54 2.5610 3 3 2 8 36.18 3.18 2.4828 2 2 4 8 36.66 1.69 2.4510 4 2 2 8 36.98 2.31 2.4309 3 0 4 8 37.26 1.78 2.4134 4 0 3 8 37.61 3.33 2.3914 4 3 0 8 37.76 5.35 2.3822 3 1 4 8 38.04 6.82 2.3657 4 1 3 8 38.35 2.61 2.3472 4 3 1 8 39.11 18.45 2.3033 5 1 1 8 39.70 13.97 2.2702 2 0 5 8 40.04 10.01 2.2519 3 2 4 8 40.44 14.12 2.2303 2 1 5 8 40.49 5.31 2.2281 4 3 2 8 40.63 4.93 2.2204 5 2 0 8 41.21 1.29 2.1904 5 1 2 8 41.32 12.31 2.1849 5 2 1 8 42.21 14.35 2.1408 4 0 4 8 42.78 7.15 2.1137 4 4 0 4 42.92 7.70 2.1073 4 1 4 8 43.30 1.26 2.0897 3 0 5 8 43.44 3.96 2.0830 4 4 1 8 43.61 2.02 2.0754 3 3 4 8 43.85 3.99 2.0644 5 0 3 8 43.85 6.11 2.0644 4 3 3 8 44.54 12.72 2.0343 5 1 3 8 44.81 5.10 2.0226 5 3 1 8 44.97 1.34 2.0157 1 0 6 8 44.98 1.86 2.0155 4 2 4 8 45.38 6.84 1.9984 4 4 2 8 45.64 1.50 1.9877 1 1 6 8 46.18 4.32 1.9657 6 1 0 8 46.54 1.69 1.9514 5 2 3 8 46.71 4.66 1.9448 5 3 2 8 46.80 4.32 1.9410 6 1 1 8 46.96 1.09 1.9349 2 0 6 8 47.61 4.66 1.9101 2 1 6 8 47.96 2.75 1.8967 4 0 5 8 48.13 1.60 1.8906 6 2 0 8 48.25 1.73 1.8860 4 3 4 8 48.60 2.20 1.8733 4 1 5 8 48.64 7.38 1.8720 6 1 2 8 48.73 3.18 1.8685 6 2 1 8 48.89 3.50 1.8630 5 1 4 8 49.23 2.54 1.8507 3 3 5 8 49.37 1.31 1.8461 5 4 1 8 50.14 1.60 1.8195 3 0 6 8 50.48 10.26 1.8079 4 2 5 8 50.52 2.81 1.8067 6 2 2 8 50.76 5.16 1.7988 3 1 6 8 51.13 2.22 1.7864 5 4 2 8 51.25 4.82 1.7824 6 3 0 8 51.59 1.02 1.7717 6 1 3 8 52.58 3.06 1.7407 3 2 6 8 52.58 7.13 1.7405 4 4 4 8 52.78 1.03 1.7343 1 0 7 8 53.38 3.31 1.7164 1 1 7 8 53.39 2.46 1.7161 6 2 3 8 53.50 1.73 1.7127 5 0 5 8 53.50 3.11 1.7127 4 3 5 8 53.54 2.69 1.7117 6 3 2 8 53.77 3.51 1.7048 5 3 4 8 53.98 4.55 1.6987 5 4 3 8 54.80 1.76 1.6751 5 5 1 8 54.94 1.98 1.6713 4 1 6 8 55.52 3.91 1.6551 6 1 4 8 55.84 5.24 1.6465 5 2 5 8 55.87 7.27 1.6456 7 0 2 8 55.96 1.12 1.6432 6 4 1 8 55.99 2.10 1.6424 7 2 0 8 56.30 1.74 1.6340 6 3 3 8 56.45 1.96 1.6302 7 1 2 8 57.24 2.03 1.6094 6 2 4 8 57.55 2.08 1.6015 4 4 5 8 57.99 3.71 1.5903 3 1 7 8 58.67 3.46 1.5736 5 3 5 8 58.82 1.87 1.5700 7 3 0 8 59.12 2.90 1.5627 5 5 3 8 59.34 1.41 1.5573 7 3 1 8 59.66 2.77 1.5497 3 2 7 8 59.78 1.42 1.5470 6 0 5 8 60.03 1.33 1.5412 5 1 6 8 60.03 3.84 1.5412 6 3 4 8 60.33 3.83 1.5342 6 1 5 8 60.77 2.29 1.5241 7 2 3 8 60.90 2.22 1.5213 1 0 8 8 60.99 3.50 1.5192 6 5 1 8 61.44 1.12 1.5091 1 1 8 8 61.85 2.10 1.5001 4 1 7 8 62.39 2.48 1.4885 3 3 7 8 62.53 1.57 1.4854 6 5 2 8 63.15 1.71 1.4724 7 4 1 8 63.15 1.71 1.4724 8 1 1 8 64.34 1.21 1.4480 5 3 6 8 64.34 2.73 1.4479 7 2 4 8 64.66 4.26 1.4416 7 4 2 8 64.74 2.22 1.4400 8 2 1 8 65.70 1.79 1.4213 3 1 8 8 66.09 3.19 1.4137 5 0 7 8 66.33 2.41 1.4091 6 6 0 4 66.61 1.96 1.4040 5 1 7 8 66.95 1.49 1.3976 7 3 4 8 67.14 1.13 1.3943 7 4 3 8 67.24 1.42 1.3924 7 1 5 8 67.47 1.13 1.3882 6 2 6 8 67.86 1.24 1.3811 7 5 1 8 67.98 2.84 1.3790 5 4 6 8 68.27 1.15 1.3739 6 4 5 8 68.30 1.12 1.3734 6 6 2 8 68.68 2.49 1.3667 8 2 3 8 68.78 1.50 1.3649 7 2 5 8 69.31 1.13 1.3558 4 1 8 8 70.90 1.94 1.3292 2 0 9 8 71.44 1.17 1.3204 9 1 0 8 71.92 1.88 1.3128 9 1 1 8 72.21 1.42 1.3083 6 1 7 8 72.34 2.50 1.3062 8 4 2 8 72.54 1.98 1.3032 7 1 6 8 72.81 2.23 1.2989 6 5 5 8 72.94 1.15 1.2969 9 2 0 8 73.83 2.43 1.2836 5 1 8 8 74.20 1.35 1.2780 5 4 7 8 74.80 2.32 1.2693 8 1 5 8 75.31 1.02 1.2619 5 2 8 8 75.39 2.00 1.2607 8 5 1 8 76.17 1.21 1.2498 6 3 7 8 76.49 1.27 1.2453 7 3 6 8 77.76 1.51 1.2282 5 3 8 8 78.80 1.62 1.2145 4 2 9 8 78.93 1.60 1.2128 9 1 4 8 79.20 2.11 1.2094 7 5 5 8 79.32 1.57 1.2078 7 7 0 4 79.58 1.12 1.2046 6 4 7 8 80.07 2.19 1.1985 7 2 7 8 80.39 1.24 1.1945 7 6 4 8 80.68 1.33 1.1910 9 4 2 8 81.22 1.62 1.1844 4 3 9 8 81.72 2.48 1.1784 2 2 10 8 82.79 1.03 1.1658 9 3 4 8 82.96 1.12 1.1639 9 4 3 8 83.06 1.37 1.1628 9 1 5 8 84.04 3.16 1.1516 10 2 2 8 84.40 1.46 1.1477 8 6 3 8 85.00 1.09 1.1411 9 5 2 8 85.54 1.07 1.1353 5 3 9 8 86.03 1.17 1.1300 4 1 10 8 86.88 1.77 1.1212 9 3 5 8 88.05 1.15 1.1093 10 1 4 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.