data_global _chemical_name_mineral 'Raspite' loop_ _publ_author_name 'Fujita T' 'Kawada I' 'Kato K' _journal_name_full 'Acta Crystallographica, Section B' _journal_volume 33 _journal_year 1977 _journal_page_first 162 _journal_page_last 164 _publ_section_title ; Raspite from Broken Hill ; _database_code_amcsd 0009580 _chemical_compound_source 'Broken Hill NSW, Australia' _chemical_formula_sum 'Pb W O4' _cell_length_a 13.555 _cell_length_b 4.976 _cell_length_c 5.561 _cell_angle_alpha 90 _cell_angle_beta 107.63 _cell_angle_gamma 90 _cell_volume 357.471 _exptl_crystal_density_diffrn 8.455 _symmetry_space_group_name_H-M 'P 1 21/a 1' loop_ _space_group_symop_operation_xyz 'x,y,z' '1/2+x,1/2-y,z' '1/2-x,1/2+y,-z' '-x,-y,-z' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv Pb 0.14961 0.19405 0.16670 ? W 0.07708 0.74944 0.61185 ? O1 0.01630 0.05150 0.72900 0.00861 O2 0.05950 0.43460 0.38820 0.01203 O3 0.15100 0.61480 0.90000 0.01798 O4 0.19030 0.88290 0.53860 0.01393 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Pb 0.01065 0.01410 0.01410 0.00081 0.00662 -0.00061 W 0.00499 0.00666 0.00970 0.00033 0.00291 0.00033