Hyalophane De Pieri R, Quareni S, Hall K M Acta Crystallographica B33 (1977) 3073-3076 Refinement of the structures of low and high hyalophanes Sample: Low hyalophane _database_code_amcsd 0009608 CELL PARAMETERS: 8.5570 13.0400 7.2000 90.000 115.690 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 723.986 Density (g/cm3): 2.875 MAX. ABS. INTENSITY / VOLUME**2: 9.509683715 RIR: 1.077 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.58 4.57 6.5200 0 2 0 2 13.65 2.44 6.4883 0 0 1 2 19.30 13.29 4.5991 0 2 1 4 21.09 15.61 4.2120 -2 0 1 2 22.45 1.08 3.9596 1 1 1 4 23.07 11.32 3.8556 2 0 0 2 23.49 53.75 3.7865 1 3 0 4 24.57 19.40 3.6233 -1 3 1 4 25.17 24.80 3.5380 -2 2 1 4 25.67 62.88 3.4699 -1 1 2 4 26.86 100.00 3.3187 2 2 0 4 27.19 47.16 3.2796 -2 0 2 2 27.36 7.99 3.2600 0 4 0 2 27.49 50.29 3.2441 0 0 2 2 29.74 58.58 3.0038 1 3 1 4 30.51 2.08 2.9299 -2 2 2 4 30.69 27.20 2.9130 0 4 1 4 30.78 6.02 2.9045 0 2 2 4 32.29 31.95 2.7724 -1 3 2 4 34.54 19.71 2.5969 -3 1 2 4 34.65 4.46 2.5889 2 2 1 4 34.80 40.88 2.5780 -2 4 1 4 35.03 15.86 2.5618 1 1 2 4 35.60 10.95 2.5219 3 1 0 4 37.10 10.96 2.4235 -1 5 1 4 37.75 8.74 2.3833 -3 3 1 4 38.68 9.43 2.3281 -1 1 3 4 39.84 6.07 2.2626 -3 3 2 4 40.27 3.45 2.2393 1 3 2 4 40.40 2.24 2.2327 -2 2 3 4 40.78 1.80 2.2125 3 3 0 4 40.85 9.57 2.2090 1 5 1 4 41.55 22.48 2.1733 0 6 0 2 42.37 9.59 2.1331 2 4 1 4 42.75 5.42 2.1152 -4 0 1 2 42.82 2.28 2.1119 -1 5 2 4 42.95 5.90 2.1060 -4 0 2 2 43.55 2.92 2.0782 -1 3 3 4 43.56 2.39 2.0779 2 0 2 2 43.69 6.49 2.0718 3 1 1 4 43.94 6.75 2.0608 0 6 1 4 44.12 1.05 2.0528 0 2 3 4 45.06 1.23 2.0119 -4 2 1 4 45.25 14.17 2.0041 -4 2 2 4 45.83 10.35 1.9798 2 2 2 4 46.49 5.61 1.9532 -3 3 3 4 47.05 2.60 1.9314 -2 6 1 4 47.14 10.23 1.9278 4 0 0 2 47.24 2.32 1.9240 -3 5 1 4 47.68 4.63 1.9072 -4 0 3 2 48.15 4.77 1.8897 3 3 1 4 48.92 7.03 1.8619 1 1 3 4 49.01 2.73 1.8588 -3 5 2 4 49.37 4.06 1.8458 1 5 2 4 49.81 3.63 1.8307 3 5 0 4 50.37 4.50 1.8117 -2 6 2 4 50.55 5.90 1.8056 0 6 2 4 50.65 9.85 1.8022 0 4 3 4 50.72 21.01 1.7998 -2 0 4 2 51.50 8.87 1.7744 -4 4 1 4 52.20 1.84 1.7522 2 4 2 4 54.10 1.84 1.6950 -5 1 2 4 54.79 7.69 1.6755 -3 5 3 4 54.79 1.67 1.6755 3 1 2 4 55.55 4.47 1.6544 -1 7 2 4 56.27 8.43 1.6349 3 5 1 4 56.45 3.46 1.6300 0 8 0 2 56.45 1.47 1.6299 -3 3 4 4 57.99 6.53 1.5903 -4 2 4 4 58.65 7.44 1.5741 0 2 4 4 59.04 2.96 1.5645 2 2 3 4 60.38 2.93 1.5330 0 6 3 4 60.52 8.54 1.5299 -5 3 3 4 60.70 1.11 1.5257 1 5 3 4 60.78 1.08 1.5240 -3 7 2 4 61.10 1.29 1.5168 1 7 2 4 61.14 8.17 1.5158 -4 6 1 4 61.79 19.14 1.5013 2 8 0 4 63.03 4.14 1.4747 -5 1 4 4 63.57 3.32 1.4637 -1 7 3 4 63.97 2.83 1.4554 1 1 4 4 64.07 3.64 1.4535 5 3 0 4 64.50 8.99 1.4447 2 4 3 4 64.63 2.94 1.4422 4 6 0 4 65.07 1.35 1.4335 -4 6 3 4 65.51 6.72 1.4249 -6 0 2 2 65.56 1.43 1.4240 1 9 0 4 66.27 5.98 1.4104 4 0 2 2 67.20 1.30 1.3931 3 7 1 4 67.58 4.45 1.3862 -2 6 4 4 67.64 3.45 1.3850 -5 5 3 4 69.01 2.82 1.3610 -4 2 5 4 69.65 3.22 1.3500 -6 2 1 4 69.99 1.02 1.3442 -2 8 3 4 70.00 5.97 1.3441 -1 9 2 4 71.16 1.83 1.3250 -6 0 4 2 71.69 4.81 1.3165 -1 3 5 4 72.04 2.86 1.3109 -2 4 5 4 72.17 2.58 1.3088 5 3 1 4 72.33 2.64 1.3064 2 0 4 2 72.48 1.80 1.3040 0 10 0 2 73.10 1.51 1.2945 2 6 3 4 73.46 9.79 1.2890 -4 8 2 4 73.72 1.38 1.2852 6 0 0 2 73.90 8.72 1.2825 2 8 2 4 74.07 3.69 1.2799 -4 4 5 4 74.56 1.36 1.2727 0 2 5 4 74.66 1.83 1.2713 -3 9 2 4 74.70 3.19 1.2707 -6 4 1 4 75.38 1.19 1.2609 6 2 0 4 75.62 2.41 1.2576 -3 5 5 4 75.73 1.98 1.2559 -5 3 5 4 76.05 1.13 1.2515 3 7 2 4 78.80 1.39 1.2146 5 5 1 4 78.91 1.19 1.2132 -6 0 5 2 79.02 1.53 1.2117 -2 10 2 4 79.50 1.48 1.2057 0 4 5 4 80.30 1.28 1.1956 6 4 0 4 80.30 1.81 1.1956 -2 6 5 4 80.55 1.11 1.1925 1 1 5 4 80.62 1.49 1.1916 -6 6 2 4 81.32 1.05 1.1832 4 2 3 4 81.33 1.04 1.1831 4 6 2 4 82.04 1.17 1.1746 -7 1 4 4 82.18 1.07 1.1729 -7 -3 3 4 83.23 1.17 1.1608 -5 7 4 4 83.65 4.08 1.1560 -4 8 4 4 84.21 4.25 1.1498 0 8 4 4 86.16 3.56 1.1287 4 4 3 4 87.03 1.19 1.1197 2 6 4 4 89.04 1.29 1.0995 6 4 1 4 89.23 2.00 1.0977 7 1 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.