Hyalophane De Pieri R, Quareni S, Hall K M Acta Crystallographica B33 (1977) 3073-3076 Refinement of the structures of low and high hyalophanes Sample: High hyalophane _database_code_amcsd 0009609 CELL PARAMETERS: 8.5560 13.0450 7.1890 90.000 115.630 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 723.436 Density (g/cm3): 2.877 MAX. ABS. INTENSITY / VOLUME**2: 9.546457816 RIR: 1.080 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.58 4.58 6.5225 0 2 0 2 13.66 2.34 6.4816 0 0 1 2 19.31 12.78 4.5976 0 2 1 4 21.10 15.36 4.2101 -2 0 1 2 23.06 11.13 3.8571 2 0 0 2 23.49 55.24 3.7880 1 3 0 4 24.57 19.81 3.6228 -1 3 1 4 25.18 24.84 3.5373 -2 2 1 4 25.71 62.57 3.4650 -1 1 2 4 26.85 100.00 3.3200 2 2 0 4 27.23 47.48 3.2752 -2 0 2 2 27.35 7.88 3.2613 0 4 0 2 27.52 49.67 3.2408 0 0 2 2 29.74 58.00 3.0042 1 3 1 4 30.54 1.96 2.9270 -2 2 2 4 30.69 26.93 2.9133 0 4 1 4 30.81 6.18 2.9023 0 2 2 4 32.31 32.26 2.7703 -1 3 2 4 34.57 20.14 2.5949 -3 1 2 4 34.64 4.22 2.5895 2 2 1 4 34.80 40.48 2.5782 -2 4 1 4 35.04 16.25 2.5608 1 1 2 4 35.59 11.01 2.5228 3 1 0 4 37.09 10.68 2.4238 -1 5 1 4 37.74 8.43 2.3835 -3 3 1 4 38.73 9.19 2.3250 -1 1 3 4 39.86 5.65 2.2615 -3 3 2 4 40.28 3.38 2.2388 1 3 2 4 40.45 2.30 2.2297 -2 2 3 4 40.77 2.01 2.2133 3 3 0 4 40.84 9.44 2.2096 1 5 1 4 41.54 22.29 2.1742 0 6 0 2 42.36 9.71 2.1337 2 4 1 4 42.75 5.49 2.1154 -4 0 1 2 42.83 2.21 2.1114 -1 5 2 4 42.97 6.03 2.1051 -4 0 2 2 43.56 2.41 2.0778 2 0 2 2 43.60 2.81 2.0761 -1 3 3 4 43.68 6.44 2.0725 3 1 1 4 43.92 6.76 2.0613 0 6 1 4 45.05 1.14 2.0122 -4 2 1 4 45.27 14.10 2.0033 -4 2 2 4 45.83 10.65 1.9797 2 2 2 4 46.54 5.91 1.9513 -3 3 3 4 47.04 2.74 1.9318 -2 6 1 4 47.12 9.94 1.9285 4 0 0 2 47.23 2.46 1.9243 -3 5 1 4 47.73 4.40 1.9053 -4 0 3 2 48.14 4.68 1.8904 3 3 1 4 48.95 6.74 1.8608 1 1 3 4 49.02 2.55 1.8584 -3 5 2 4 49.38 4.08 1.8458 1 5 2 4 49.79 3.79 1.8314 3 5 0 4 50.38 4.56 1.8114 -2 6 2 4 50.55 5.97 1.8055 0 6 2 4 50.68 9.70 1.8011 0 4 3 4 50.81 20.90 1.7971 -2 0 4 2 51.49 8.85 1.7747 -4 4 1 4 52.20 1.69 1.7523 2 4 2 4 54.12 1.98 1.6947 -5 1 2 4 54.78 1.73 1.6757 3 1 2 4 54.83 7.63 1.6745 -3 5 3 4 55.55 4.38 1.6544 -1 7 2 4 56.25 8.32 1.6355 3 5 1 4 56.43 3.45 1.6306 0 8 0 2 56.53 1.58 1.6279 -3 3 4 4 58.07 6.27 1.5883 -4 2 4 4 58.71 7.52 1.5726 0 2 4 4 59.06 2.92 1.5641 2 2 3 4 60.40 2.98 1.5325 0 6 3 4 60.55 8.63 1.5291 -5 3 3 4 60.72 1.14 1.5253 1 5 3 4 60.78 1.10 1.5240 -3 7 2 4 61.09 1.36 1.5170 1 7 2 4 61.12 8.23 1.5162 -4 6 1 4 61.77 18.90 1.5019 2 8 0 4 63.11 4.08 1.4732 -5 1 4 4 63.59 3.21 1.4632 -1 7 3 4 64.02 2.89 1.4544 1 1 4 4 64.04 3.67 1.4540 5 3 0 4 64.51 9.04 1.4445 2 4 3 4 64.60 2.74 1.4427 4 6 0 4 65.10 1.35 1.4329 -4 6 3 4 65.51 6.51 1.4249 -6 0 2 2 65.53 1.43 1.4245 1 9 0 4 66.25 5.96 1.4107 4 0 2 2 67.17 1.30 1.3936 3 7 1 4 67.64 4.41 1.3852 -2 6 4 4 67.67 3.51 1.3845 -5 5 3 4 69.12 2.83 1.3591 -4 2 5 4 69.63 3.23 1.3503 -6 2 1 4 69.99 6.11 1.3443 -1 9 2 4 70.01 1.04 1.3439 -2 8 3 4 71.23 1.77 1.3239 -6 0 4 2 71.78 4.69 1.3150 -1 3 5 4 72.14 2.76 1.3094 -2 4 5 4 72.14 2.59 1.3093 5 3 1 4 72.37 2.68 1.3058 2 0 4 2 72.45 1.82 1.3045 0 10 0 2 73.11 1.49 1.2944 2 6 3 4 73.46 9.66 1.2891 -4 8 2 4 73.68 1.36 1.2857 6 0 0 2 73.88 8.73 1.2828 2 8 2 4 74.18 3.48 1.2784 -4 4 5 4 74.65 1.36 1.2715 0 2 5 4 74.65 1.85 1.2714 -3 9 2 4 74.68 3.29 1.2711 -6 4 1 4 75.35 1.11 1.2614 6 2 0 4 75.71 2.36 1.2562 -3 5 5 4 75.84 1.93 1.2544 -5 3 5 4 76.03 1.14 1.2518 3 7 2 4 78.76 1.48 1.2151 5 5 1 4 79.01 1.52 1.2119 -2 10 2 4 79.01 1.26 1.2118 -6 0 5 2 79.58 1.51 1.2046 0 4 5 4 80.26 1.15 1.1961 6 4 0 4 80.39 1.79 1.1945 -2 6 5 4 80.61 1.50 1.1917 -6 6 2 4 80.63 1.07 1.1916 1 1 5 4 81.30 1.04 1.1834 4 6 2 4 81.31 1.06 1.1833 4 2 3 4 82.10 1.15 1.1739 -7 1 4 4 82.20 1.06 1.1727 -7 -3 3 4 83.28 1.14 1.1602 -5 7 4 4 83.70 3.96 1.1555 -4 8 4 4 84.24 4.29 1.1494 0 8 4 4 86.15 3.66 1.1288 4 4 3 4 87.05 1.13 1.1194 2 6 4 4 89.00 1.31 1.0999 6 4 1 4 89.18 2.11 1.0981 7 1 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.