H16 Na2 Ni O20 P4 Boudjada A, Durif A, Guitel J Acta Crystallographica B34 (1978) 17-20 Structure cristalline d'un monophosphate acide mixte de nickel-sodium tetrahydrate Na2 Ni H8 (P O4)4 (H2 O)4 _cod_database_code 1007019 _database_code_amcsd 0009622 CELL PARAMETERS: 11.1000 10.7100 7.2240 90.000 100.200 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 845.224 Density (g/cm3): 2.155 MAX. ABS. INTENSITY / VOLUME**2: 5.873693497 RIR: 0.887 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.57 52.12 7.6478 1 1 0 4 13.60 1.30 6.5092 -1 0 1 2 14.96 46.87 5.9234 0 1 1 4 15.93 19.21 5.5624 -1 1 1 4 16.03 39.14 5.5282 1 0 1 2 16.23 21.53 5.4623 2 0 0 2 16.55 8.47 5.3550 0 2 0 2 18.06 3.08 4.9124 1 1 1 4 18.23 60.74 4.8660 2 1 0 4 18.45 7.05 4.8084 1 2 0 4 20.43 1.93 4.3480 -2 1 1 4 20.77 5.32 4.2775 0 2 1 4 21.49 5.09 4.1354 -1 2 1 4 23.12 100.00 3.8463 1 2 1 4 23.26 11.18 3.8239 2 2 0 4 23.73 25.03 3.7493 2 1 1 4 25.04 9.58 3.5567 -2 2 1 4 25.05 45.70 3.5549 0 0 2 2 25.43 39.23 3.5025 -3 0 1 2 26.26 32.17 3.3934 1 3 0 4 26.30 11.05 3.3882 -1 1 2 4 26.42 2.39 3.3739 0 1 2 4 27.40 9.08 3.2546 -2 0 2 2 27.83 5.19 3.2060 2 2 1 4 27.97 8.07 3.1904 0 3 1 4 28.52 24.82 3.1301 -1 3 1 4 28.67 7.01 3.1140 -2 1 2 4 28.98 9.61 3.0810 1 1 2 4 29.47 2.98 3.0307 3 0 1 2 29.67 25.21 3.0112 3 2 0 4 29.90 16.59 2.9884 2 3 0 4 30.07 3.51 2.9714 -1 2 2 4 30.18 10.90 2.9617 0 2 2 4 30.50 1.29 2.9312 -3 2 1 4 30.66 6.76 2.9162 3 1 1 4 32.18 30.36 2.7812 -2 2 2 4 32.47 2.34 2.7576 1 2 2 4 32.79 2.11 2.7311 4 0 0 2 33.47 8.25 2.6775 0 4 0 2 33.48 1.44 2.6764 2 1 2 4 33.64 1.73 2.6642 2 3 1 4 33.87 2.06 2.6464 4 1 0 4 33.99 3.00 2.6376 3 2 1 4 34.06 36.34 2.6323 -4 1 1 4 34.49 6.69 2.6005 1 4 0 4 35.20 9.64 2.5493 3 3 0 4 35.55 7.06 2.5250 -1 3 2 4 35.92 3.30 2.5002 -3 3 1 4 36.58 11.47 2.4562 2 2 2 4 37.32 2.61 2.4097 1 4 1 4 37.38 3.94 2.4060 -1 0 3 2 37.39 6.16 2.4051 -2 3 2 4 37.41 3.21 2.4042 2 4 0 4 37.64 11.51 2.3898 1 3 2 4 37.82 3.44 2.3788 -4 0 2 2 38.58 1.35 2.3334 -2 4 1 4 38.92 1.80 2.3140 0 1 3 4 38.98 1.85 2.3104 3 3 1 4 40.54 2.38 2.2255 2 4 1 4 41.01 1.55 2.2008 -5 0 1 2 41.13 1.88 2.1947 -1 2 3 4 41.25 6.88 2.1883 1 1 3 4 41.31 5.91 2.1856 2 3 2 4 41.54 1.24 2.1740 -4 2 2 4 41.62 3.10 2.1697 -3 0 3 2 41.64 1.16 2.1692 4 3 0 4 42.07 5.58 2.1478 3 2 2 4 42.21 8.02 2.1408 5 1 0 4 42.30 6.68 2.1365 -2 2 3 4 42.50 2.63 2.1272 -3 4 1 4 43.78 1.41 2.0677 -2 4 2 4 44.00 5.08 2.0580 1 4 2 4 44.16 2.16 2.0509 0 5 1 4 44.51 4.43 2.0356 -5 2 1 4 44.80 2.48 2.0230 5 2 0 4 45.08 1.88 2.0109 -3 2 3 4 45.12 3.04 2.0095 2 1 3 4 45.19 1.30 2.0066 3 4 1 4 45.40 2.01 1.9978 4 3 1 4 45.41 1.44 1.9973 1 5 1 4 45.46 5.15 1.9952 -1 3 3 4 45.96 3.72 1.9745 0 3 3 4 46.14 1.06 1.9673 4 1 2 4 46.49 1.04 1.9532 -2 5 1 4 46.54 6.34 1.9512 -2 3 3 4 47.26 6.62 1.9232 2 4 2 4 47.58 2.60 1.9111 2 2 3 4 47.70 1.18 1.9066 -4 4 1 4 48.18 2.58 1.8886 2 5 1 4 48.78 7.52 1.8669 5 2 1 4 48.87 2.03 1.8636 5 3 0 4 49.14 1.01 1.8541 -3 3 3 4 49.46 1.29 1.8427 3 0 3 2 49.63 5.15 1.8370 -1 5 2 4 49.69 3.39 1.8347 0 5 2 4 50.20 1.81 1.8173 -6 1 1 4 50.87 6.17 1.7950 6 1 0 4 50.98 3.65 1.7915 4 4 1 4 51.03 3.88 1.7896 -1 4 3 4 51.04 1.24 1.7893 -2 5 2 4 51.17 2.15 1.7850 0 6 0 2 51.24 4.19 1.7829 1 5 2 4 51.38 2.16 1.7783 -4 4 2 4 51.41 6.57 1.7775 0 0 4 2 51.48 3.20 1.7750 2 3 3 4 51.50 2.22 1.7746 0 4 3 4 51.63 4.44 1.7702 -5 0 3 2 51.90 3.10 1.7616 1 6 0 4 52.39 1.01 1.7465 -5 1 3 4 52.41 2.57 1.7457 4 3 2 4 52.48 1.24 1.7436 -6 2 1 4 52.52 1.29 1.7425 3 2 3 4 52.98 1.57 1.7283 -6 1 2 4 53.07 6.30 1.7255 -4 3 3 4 53.13 6.00 1.7238 6 2 0 4 53.39 3.30 1.7160 1 4 3 4 53.56 1.41 1.7111 -1 2 4 4 53.86 1.24 1.7022 -3 5 2 4 53.93 1.02 1.7002 -3 1 4 4 53.93 4.02 1.7002 -5 4 1 4 53.98 6.09 1.6986 1 6 1 4 54.05 4.05 1.6967 2 6 0 4 54.14 1.24 1.6941 -2 2 4 4 54.39 1.90 1.6870 0 2 4 4 54.57 1.08 1.6818 -4 5 1 4 54.60 1.46 1.6807 -5 2 3 4 54.90 3.07 1.6725 6 1 1 4 55.85 2.12 1.6460 5 2 2 4 56.38 1.73 1.6318 4 1 3 4 56.44 2.02 1.6302 2 6 1 4 57.16 1.37 1.6114 -1 3 4 4 57.26 2.25 1.6088 -4 1 4 4 57.49 1.94 1.6030 4 4 2 4 57.56 1.05 1.6012 4 5 1 4 57.61 1.81 1.5999 -1 5 3 4 57.80 1.15 1.5952 0 6 2 4 58.04 1.53 1.5891 0 5 3 4 58.35 1.16 1.5814 3 5 2 4 58.87 2.45 1.5688 -6 1 3 4 59.02 1.50 1.5651 -2 6 2 4 59.20 1.17 1.5608 1 6 2 4 59.36 1.85 1.5570 -4 2 4 4 59.61 2.38 1.5510 -3 3 4 4 59.80 1.35 1.5466 1 5 3 4 60.16 1.47 1.5381 3 6 1 4 60.52 1.55 1.5299 6 3 1 4 60.53 1.58 1.5296 5 5 0 4 60.99 1.22 1.5192 -7 2 1 4 61.04 2.84 1.5180 3 4 3 4 61.09 4.28 1.5169 -7 1 2 4 61.16 1.72 1.5153 6 0 2 2 61.78 1.62 1.5016 -5 1 4 4 61.84 1.19 1.5004 6 1 2 4 61.99 1.49 1.4971 -1 4 4 4 62.12 1.64 1.4942 4 6 0 4 62.34 2.06 1.4894 -1 7 1 4 62.69 1.66 1.4819 3 1 4 4 62.74 1.65 1.4809 0 4 4 4 62.75 1.42 1.4807 -4 3 4 4 63.81 2.93 1.4586 5 5 1 4 63.91 3.02 1.4565 -2 7 1 4 64.09 1.04 1.4530 5 4 2 4 64.27 3.84 1.4493 -6 3 3 4 64.33 1.46 1.4481 -7 3 1 4 64.76 1.30 1.4394 1 4 4 4 65.06 1.56 1.4336 -1 6 3 4 66.18 2.57 1.4120 -3 0 5 2 66.31 1.82 1.4096 0 1 5 4 66.54 1.46 1.4054 4 4 3 4 67.05 1.53 1.3958 -5 3 4 4 67.36 1.57 1.3902 -6 1 4 4 67.97 1.33 1.3792 1 0 5 2 68.01 2.94 1.3785 -3 6 3 4 68.16 1.40 1.3758 -8 1 1 4 69.07 1.82 1.3599 7 3 1 4 69.28 1.99 1.3563 -6 2 4 4 69.46 1.23 1.3531 -4 1 5 4 70.35 1.40 1.3382 4 2 4 4 70.51 2.18 1.3356 1 2 5 4 70.63 2.95 1.3336 7 1 2 4 71.27 1.56 1.3232 8 2 0 4 71.55 2.66 1.3188 6 4 2 4 72.02 2.68 1.3113 -1 8 1 4 72.73 1.11 1.3003 2 8 0 4 73.33 1.46 1.2911 -1 7 3 4 74.43 1.87 1.2746 6 6 0 4 75.17 1.24 1.2640 5 1 4 4 75.59 2.37 1.2579 7 3 2 4 77.98 1.46 1.2253 2 7 3 4 78.26 1.09 1.2215 -5 7 2 4 79.46 1.20 1.2061 9 1 0 4 79.80 1.08 1.2018 -9 2 1 4 81.66 2.01 1.1791 7 2 3 4 81.68 1.00 1.1789 -3 5 5 4 82.11 1.57 1.1738 -2 2 6 4 82.72 1.28 1.1667 -4 8 2 4 83.46 1.26 1.1582 -4 1 6 4 84.06 2.11 1.1515 8 5 0 4 84.22 1.16 1.1496 1 1 6 4 84.48 1.49 1.1468 -8 5 2 4 84.76 1.76 1.1438 -5 8 1 4 85.93 1.10 1.1311 3 9 0 4 88.93 1.01 1.1006 -7 7 1 4 89.59 2.07 1.0942 2 2 6 4 89.90 1.60 1.0912 -9 1 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.