Giacovazzoite Mereiter K, Vollenkle H Acta Crystallographica B34 (1978) 378-384 Die Kristallstruktur von beta-pentakalium-[mu3-oxo-hexa-mu-sulfato- triquatriesen(III)]-Heptahydrat - eine monokline Modifikation des Masschen Salzes Locality: synthetic _database_code_amcsd 0019784 9.491 18.474 18.109 90 92.38 90 P2_1/c atom x y z Uiso U(1,1) U(2,2) U(3,3) U(1,2) U(1,3) U(2,3) K1 .54292 .15530 .24569 .0285 .0360 .0244 -.0051 .0002 .0003 K2 .63730 .22467 .03809 .0394 .0307 .0434 -.0011 -.0044 .0022 K3 .27069 .10196 .04945 .0368 .0319 .0356 -.0026 -.0014 -.0058 K4 .12321 .20390 .27225 .0363 .0321 .0708 .0119 -.0155 -.0026 K5 .32772 .11218 .44202 .0513 .0339 .0310 .0033 .0082 .0067 Fe1 .31502 .41637 .25680 .0123 .0138 .0108 .0008 -.0003 -.0009 Fe2 .63302 .40832 .34178 .0125 .0147 .0116 .0005 -.0008 -.0004 Fe3 .59817 .39747 .15754 .0136 .0164 .0111 .0014 -.0001 -.0003 S1 .38938 .52069 .39218 .0177 .0146 .0135 .0004 -.0002 -.0032 S2 .39733 .29594 .38248 .0176 .0142 .0164 -.0014 .0004 .0035 S3 .77980 .52338 .24094 .0162 .0145 .0192 -.0015 .0002 -.0009 S4 .81386 .29505 .24462 .0131 .0166 .0183 .0013 -.0001 .0006 S5 .36347 .51355 .10713 .0194 .0170 .0149 .0028 -.0026 .0014 S6 .31755 .29533 .12788 .0183 .0154 .0160 .0007 -.0025 -.0037 O1 .3285 .5085 .3160 .0272 .0160 .0136 .0040 -.0066 -.0031 O2 .5077 .4688 .4052 .0187 .0292 .0145 .0052 .0000 -.0055 O3 .2825 .5064 .4456 .0216 .0290 .0178 -.0003 .0043 -.0029 O4 .4414 .5941 .3977 .0354 .0166 .0278 -.0045 -.0046 -.0024 O5 .3059 .3545 .3486 .0208 .0189 .0147 .0025 .0023 .0043 O6 .5477 .3170 .3754 .0187 .0248 .0369 .0014 .0004 .0163 O7 .3698 .2900 .4601 .0335 .0481 .0163 .0062 .0038 .0094 O8 .3737 .2282 .3436 .0398 .0173 .0385 .0023 -.0085 -.0063 O9 .7305 .5007 .3149 .0340 .0242 .0178 -.0122 .0066 -.0026 O10 .7646 .4613 .1893 .0189 .0208 .0199 -.0015 .0030 -.0026 O11 .9297 .5423 .2490 .0197 .0280 .0297 -.0033 -.0020 -.0012 O12 .6989 .5852 .2148 .0242 .022 .0371 .0019 .0010 .0017 O13 .7914 .3482 .3047 .0176 .0271 .0163 .0053 -.0029 -.0028 O14 .6980 .3045 .1866 .0212 .0171 .0242 .0041 -.0079 -.0030 O15 .9500 .3100 .2138 .0167 .0297 .0327 -.0001 .0029 -.0046 O16 .8067 .2217 .2720 .0359 .0206 .0348 .0033 -.0030 .0007 O17 .5076 .4815 .1064 .0228 .0375 .0281 .0084 .0088 .0129 O18 .2849 .4779 .1659 .0229 .0405 .0196 .0045 -.0001 .0106 O19 .2903 .5008 .0365 .0383 .0332 .0146 -.0035 -.0056 -.0014 O20 .3795 .5897 .1220 .0474 .0221 .0441 .0040 -.0144 -.0040 O21 .4503 .3320 .1080 .0188 .0529 .0244 -.0084 .0026 -.0178 O22 .2719 .3266 .1990 .0274 .0237 .0194 -.0060 .0028 -.0107 O23 .2119 .3101 .0696 .0222 .0436 .0226 .0039 -.0109 -.0053 O24 .3430 .2191 .1387 .0767 .0207 .0291 .0097 -.0073 -.0073 O25 .5153 .4089 .2513 .0132 .0194 .0113 .0030 .0000 -.0006 O26 .1000 .4241 .2677 .0110 .0243 .0344 .0005 -.0023 .0012 O27 .7591 .4042 .4382 .0253 .0410 .0153 .0082 -.0033 -.0081 O28 .7053 .3854 .0605 .0278 .0266 .0158 .0043 .0049 .0039 O29 .0033 .0688 .0992 .0573 .1369 .0725 -.0167 -.0219 .0473 O30 .9186 .2125 .0773 .0948 .0931 .1040 .0137 -.0194 -.0393 O31 .9814 .4050 .0607 .0330 .0362 .0711 .0063 .0049 .0043 O32 .9607 .5567 .0865 .0777 .0809 .0532 -.0048 .0212 .0128 O33 .9283 .7310 .0725 .0451 .0730 .0560 .0118 -.0019 -.0129 O34 .9627 .8835 .0670 .0278 .0552 .0463 -.0032 .0069 .0010 O35 .7819 .2085 .4299 .0443 .0437 .0351 -.0214 -.0066 .0133 H1 .051 .458 .259 .0507 H2 .059 .387 .249 .0507 H3 .741 .436 .473 .0507 H4 .855 .400 .431 .0507 H5 .708 .422 .040 .0507 H6 .818 .376 .061 .0507 H7 -.08 .042 .081 .076 H8 .024 .050 .151 .076 H9 .923 .242 .120 .076 H10 .948 .163 .089 .076 H11 .057 .373 .083 .076 H12 -.001 .440 .073 .076 H13 .002 .579 .135 .076 H14 .990 .588 .055 .076 H15 .895 .735 .021 .076 H16 .022 .717 .071 .076 H17 .918 .902 .099 .076 H18 .947 .831 .072 .076 H19 .787 .229 .388 .076 H20 .749 .171 .422 .001