Ba H2 K O10 P3 Seethanen D, Durif A Acta Crystallographica B34 (1978) 1091-1093 Structure cristalline du trimetaphosphate de baryum-potassium monohydrate: Ba K P3 O9 (H2 O) _cod_database_code 1007022 _database_code_amcsd 0009635 CELL PARAMETERS: 7.3400 17.7700 7.1800 90.000 95.240 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 932.587 Density (g/cm3): 3.057 MAX. ABS. INTENSITY / VOLUME**2: 8.522581739 RIR: 0.908 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.96 36.74 8.8850 0 2 0 2 13.10 52.53 6.7598 1 1 0 4 13.35 31.99 6.6332 0 1 1 4 15.70 14.92 5.6447 1 2 0 4 15.91 100.00 5.5703 0 2 1 4 17.27 52.18 5.1333 -1 1 1 4 18.13 41.86 4.8927 1 0 1 2 18.81 1.27 4.7172 1 1 1 4 19.34 39.40 4.5907 -1 2 1 4 19.46 51.18 4.5614 0 3 1 4 19.99 9.09 4.4425 0 4 0 2 20.72 28.35 4.2859 1 2 1 4 22.37 51.96 3.9751 -1 3 1 4 23.43 49.48 3.7963 1 4 0 4 23.58 61.00 3.7734 0 4 1 4 24.36 20.76 3.6547 2 0 0 2 24.87 17.21 3.5797 2 1 0 4 24.91 3.13 3.5750 0 0 2 2 25.41 6.55 3.5048 0 1 2 4 26.05 53.77 3.4209 -1 4 1 4 26.37 41.13 3.3799 2 2 0 4 26.84 13.34 3.3221 -2 1 1 4 26.88 38.51 3.3166 0 2 2 4 27.11 16.50 3.2890 1 4 1 4 27.22 77.63 3.2767 -1 1 2 4 27.91 4.98 3.1962 1 5 0 4 28.04 9.88 3.1825 0 5 1 4 28.24 41.69 3.1606 -2 2 1 4 28.60 1.75 3.1214 -1 2 2 4 28.70 29.45 3.1103 2 3 0 4 28.87 10.14 3.0921 2 1 1 4 29.18 55.68 3.0607 0 3 2 4 29.23 65.13 3.0554 1 1 2 4 30.17 23.76 2.9623 -1 5 1 4 30.18 53.24 2.9617 0 6 0 2 30.19 44.39 2.9606 2 2 1 4 30.44 1.88 2.9368 -2 3 1 4 30.53 15.95 2.9283 1 2 2 4 30.78 6.43 2.9053 -1 3 2 4 31.10 15.02 2.8755 1 5 1 4 31.70 1.50 2.8223 2 4 0 4 32.14 10.98 2.7852 0 4 2 4 32.27 9.37 2.7743 2 3 1 4 32.59 4.83 2.7477 1 3 2 4 32.62 42.66 2.7449 1 6 0 4 32.73 13.08 2.7362 0 6 1 4 33.30 10.87 2.6908 -2 4 1 4 33.42 1.09 2.6809 -2 0 2 2 33.81 9.37 2.6509 -2 1 2 4 34.60 3.94 2.5925 -1 6 1 4 34.96 1.15 2.5666 -2 2 2 4 34.99 6.22 2.5642 2 4 1 4 35.22 3.05 2.5479 2 5 0 4 35.29 2.49 2.5431 1 4 2 4 35.62 16.46 2.5204 0 5 2 4 36.80 12.25 2.4424 -2 3 2 4 37.10 10.36 2.4235 2 1 2 4 37.25 4.66 2.4139 3 1 0 4 37.60 1.15 2.3923 0 7 1 4 37.91 13.89 2.3733 -3 0 1 2 38.10 16.56 2.3622 0 1 3 4 38.25 4.12 2.3532 2 5 1 4 38.26 1.51 2.3525 -3 1 1 4 38.31 3.32 2.3497 3 2 0 4 38.53 3.84 2.3368 1 5 2 4 38.65 3.31 2.3295 -1 0 3 2 39.00 4.21 2.3097 -1 1 3 4 39.15 1.61 2.3010 2 6 0 4 39.25 1.01 2.2954 -2 4 2 4 39.27 15.25 2.2944 -1 7 1 4 39.29 18.06 2.2930 -3 2 1 4 39.51 4.92 2.2807 0 6 2 4 40.01 17.22 2.2533 1 7 1 4 40.01 1.68 2.2533 3 3 0 4 40.18 2.05 2.2445 3 0 1 2 40.49 27.54 2.2280 -2 6 1 4 40.51 10.29 2.2268 3 1 1 4 40.62 1.71 2.2213 0 8 0 2 40.75 3.17 2.2142 -1 6 2 4 40.81 13.15 2.2111 0 3 3 4 40.88 3.85 2.2073 1 0 3 2 40.97 1.43 2.2031 -3 3 1 4 41.21 5.36 2.1904 1 1 3 4 41.50 11.33 2.1761 3 2 1 4 41.66 7.10 2.1679 -1 3 3 4 41.93 2.66 2.1545 2 6 1 4 42.19 9.71 2.1422 1 2 3 4 42.19 3.31 2.1420 1 6 2 4 42.22 2.43 2.1403 -2 5 2 4 42.31 10.06 2.1363 3 4 0 4 42.54 15.01 2.1253 1 8 0 4 42.62 2.71 2.1212 0 8 1 4 43.07 1.46 2.1002 0 4 3 4 43.10 11.85 2.0989 3 3 1 4 43.22 1.64 2.0933 -3 4 1 4 43.29 21.98 2.0902 -3 1 2 4 43.40 4.84 2.0849 2 7 0 4 43.70 9.37 2.0712 -2 1 3 4 43.73 11.93 2.0698 0 7 2 4 43.77 10.80 2.0683 1 3 3 4 43.89 1.50 2.0631 -1 4 3 4 44.13 3.83 2.0521 -1 8 1 4 44.63 3.11 2.0302 -2 2 3 4 44.81 6.65 2.0226 1 8 1 4 44.88 2.96 2.0197 -1 7 2 4 44.99 49.37 2.0151 2 5 2 4 45.75 2.09 1.9833 -3 3 2 4 45.98 1.26 1.9737 -3 5 1 4 46.15 6.86 1.9670 -2 3 3 4 46.21 4.22 1.9645 1 7 2 4 46.62 10.30 1.9483 -1 5 3 4 47.31 8.70 1.9215 3 1 2 4 47.70 9.91 1.9067 2 1 3 4 47.79 6.95 1.9032 0 9 1 4 47.82 3.64 1.9021 -3 4 2 4 47.93 2.75 1.8982 2 8 0 4 47.94 7.30 1.8977 3 5 1 4 48.23 4.01 1.8867 0 8 2 4 48.37 15.92 1.8816 3 6 0 4 48.55 4.36 1.8751 1 5 3 4 49.06 6.99 1.8568 0 6 3 4 49.07 1.73 1.8566 -2 8 1 4 49.45 21.47 1.8433 -2 7 2 4 49.61 1.81 1.8375 3 3 2 4 49.80 2.50 1.8310 1 9 1 4 49.91 6.88 1.8273 4 0 0 2 49.99 1.83 1.8246 2 3 3 4 50.54 5.54 1.8059 1 8 2 4 51.03 9.95 1.7899 4 2 0 4 51.10 2.95 1.7875 0 0 4 2 51.38 2.53 1.7783 -3 1 3 4 51.42 1.29 1.7770 0 10 0 2 51.51 2.95 1.7741 -4 2 1 4 51.57 1.63 1.7724 3 4 2 4 51.79 4.11 1.7653 -1 1 4 4 51.91 4.32 1.7615 2 7 2 4 52.20 7.12 1.7524 0 2 4 4 52.68 2.06 1.7376 0 7 3 4 52.69 1.12 1.7371 2 9 0 4 53.03 1.23 1.7267 1 10 0 4 53.10 5.78 1.7247 4 1 1 4 53.38 5.62 1.7164 -1 7 3 4 53.40 2.18 1.7157 -3 6 2 4 53.56 13.47 1.7111 -3 3 3 4 53.76 1.16 1.7051 -2 6 3 4 53.97 2.03 1.6989 -1 9 2 4 54.00 1.67 1.6980 3 5 2 4 54.25 4.72 1.6909 -4 0 2 2 54.39 12.91 1.6868 -1 10 1 4 54.51 1.68 1.6833 -4 1 2 4 54.58 1.59 1.6815 3 7 1 4 54.75 7.78 1.6766 -4 4 1 4 54.93 4.28 1.6715 2 9 1 4 54.97 2.09 1.6705 1 2 4 4 54.98 3.93 1.6703 1 10 1 4 55.09 2.86 1.6669 -2 0 4 2 55.14 1.92 1.6657 1 7 3 4 55.14 2.74 1.6656 1 9 2 4 55.23 3.79 1.6632 4 3 1 4 55.36 1.31 1.6596 -2 1 4 4 55.80 5.29 1.6476 -1 4 4 4 56.02 4.69 1.6415 3 8 0 4 56.14 1.74 1.6384 -2 2 4 4 56.42 4.62 1.6309 3 0 3 2 56.61 2.30 1.6259 -4 3 2 4 56.64 1.97 1.6249 0 8 3 4 56.68 1.35 1.6241 3 1 3 4 56.77 3.08 1.6218 -3 8 1 4 56.82 2.35 1.6203 -3 7 2 4 57.23 3.53 1.6098 2 6 3 4 57.45 1.59 1.6041 3 2 3 4 57.68 1.77 1.5981 2 10 0 4 57.74 3.25 1.5967 -3 5 3 4 58.07 5.38 1.5884 1 4 4 4 58.40 3.32 1.5803 -4 4 2 4 58.46 1.59 1.5788 3 8 1 4 58.58 3.78 1.5757 0 11 1 4 58.69 1.16 1.5731 -2 10 1 4 58.72 2.14 1.5724 3 3 3 4 58.99 1.47 1.5657 1 8 3 4 59.20 2.73 1.5607 -2 4 4 4 59.80 1.12 1.5465 2 10 1 4 59.82 1.26 1.5461 4 2 2 4 59.87 2.27 1.5449 2 1 4 4 59.88 2.29 1.5448 -4 6 1 4 60.23 7.05 1.5365 2 9 2 4 60.50 1.07 1.5304 0 6 4 4 60.61 1.93 1.5278 -3 8 2 4 60.61 2.35 1.5277 2 2 4 4 60.65 6.76 1.5269 -4 5 2 4 60.87 3.13 1.5219 -1 6 4 4 60.93 3.60 1.5205 0 9 3 4 61.06 1.75 1.5176 4 3 2 4 61.26 2.45 1.5132 -4 1 3 4 61.44 8.44 1.5092 -2 5 4 4 61.57 1.11 1.5062 -1 9 3 4 61.72 1.97 1.5030 -3 1 4 4 61.84 3.18 1.5002 2 3 4 4 62.05 1.70 1.4957 4 6 1 4 62.68 1.71 1.4823 3 5 3 4 62.90 1.34 1.4775 2 11 0 4 63.02 4.08 1.4749 1 6 4 4 63.21 3.09 1.4711 -4 3 3 4 63.34 1.45 1.4684 -4 6 2 4 63.54 2.19 1.4642 2 4 4 4 63.67 1.13 1.4615 0 7 4 4 64.05 1.84 1.4538 -1 11 2 4 64.16 1.01 1.4516 2 8 3 4 64.61 1.21 1.4425 5 2 0 4 64.74 2.79 1.4400 -3 9 2 4 64.77 1.57 1.4394 -5 2 1 4 64.91 1.69 1.4365 2 11 1 4 64.93 2.11 1.4361 4 5 2 4 65.05 4.23 1.4338 -2 9 3 4 65.10 3.54 1.4328 1 11 2 4 65.18 1.36 1.4312 4 7 1 4 65.38 2.19 1.4274 -1 12 1 4 65.48 1.16 1.4254 0 1 5 4 65.63 2.32 1.4225 -3 10 1 4 65.90 1.72 1.4173 1 12 1 4 66.23 4.49 1.4112 4 8 0 4 66.28 2.48 1.4101 -1 2 5 4 66.43 1.25 1.4073 -4 7 2 4 66.64 1.80 1.4034 -4 8 1 4 67.13 4.23 1.3943 -5 1 2 4 67.19 2.35 1.3932 3 10 1 4 67.23 3.64 1.3926 0 8 4 4 67.44 4.23 1.3886 5 4 0 4 67.52 1.34 1.3872 4 6 2 4 67.58 2.25 1.3862 -1 8 4 4 67.60 2.66 1.3858 -5 4 1 4 67.69 1.31 1.3842 1 10 3 4 67.86 1.55 1.3812 3 9 2 4 67.93 2.15 1.3798 1 0 5 2 68.35 5.45 1.3724 2 12 0 4 68.60 1.76 1.3681 0 12 2 4 68.86 2.73 1.3635 1 2 5 4 68.99 2.70 1.3612 0 4 5 4 69.08 1.20 1.3597 -1 4 5 4 69.13 1.50 1.3588 -2 2 5 4 69.45 1.85 1.3534 4 3 3 4 69.57 1.49 1.3514 -4 6 3 4 69.62 1.66 1.3504 1 8 4 4 69.76 3.23 1.3481 2 11 2 4 70.00 2.71 1.3441 -3 6 4 4 70.03 1.03 1.3436 1 13 0 4 70.22 2.11 1.3405 -4 0 4 2 70.28 1.57 1.3394 2 12 1 4 70.41 4.45 1.3372 0 11 3 4 70.46 1.82 1.3363 1 12 2 4 70.53 5.52 1.3353 4 7 2 4 70.65 1.10 1.3333 -2 8 4 4 71.05 1.54 1.3267 4 4 3 4 71.15 1.08 1.3251 0 9 4 4 71.26 2.13 1.3234 2 7 4 4 71.48 1.32 1.3199 3 4 4 4 71.88 1.60 1.3135 -2 4 5 4 72.04 1.72 1.3109 5 6 0 4 72.20 1.46 1.3084 5 5 1 4 72.21 5.38 1.3082 5 1 2 4 72.59 1.83 1.3024 4 9 1 4 73.48 1.03 1.2888 2 1 5 4 73.55 1.64 1.2877 0 6 5 4 73.69 2.89 1.2856 -3 0 5 2 73.84 1.95 1.2833 -4 4 4 4 73.91 1.13 1.2824 -2 5 5 4 73.93 1.50 1.2821 4 8 2 4 73.97 1.23 1.2815 -3 11 2 4 74.15 2.42 1.2788 2 2 5 4 74.26 1.69 1.2771 -2 11 3 4 74.49 1.64 1.2737 -2 9 4 4 74.59 2.79 1.2723 -3 2 5 4 74.64 1.54 1.2716 2 8 4 4 74.75 1.36 1.2699 -5 3 3 4 74.80 2.79 1.2693 0 14 0 2 74.93 1.10 1.2673 -2 13 1 4 75.11 2.94 1.2647 -1 13 2 4 75.12 1.37 1.2647 -5 6 2 4 75.56 1.25 1.2584 4 6 3 4 75.70 1.39 1.2563 -3 12 1 4 75.92 1.16 1.2533 2 13 1 4 75.97 2.82 1.2526 3 6 4 4 76.10 3.00 1.2508 1 13 2 4 76.31 1.07 1.2479 -3 8 4 4 76.36 2.01 1.2471 -2 6 5 4 76.82 1.62 1.2408 2 4 5 4 76.92 1.75 1.2395 3 11 2 4 77.57 2.23 1.2308 5 7 1 4 78.00 2.59 1.2249 -4 10 2 4 78.14 4.56 1.2232 4 0 4 2 78.30 2.61 1.2210 -5 5 3 4 78.44 1.03 1.2192 -5 8 1 4 78.52 1.85 1.2182 6 0 0 2 78.55 2.37 1.2178 -2 13 2 4 78.71 2.64 1.2158 -2 10 4 4 78.74 1.53 1.2154 6 1 0 4 79.65 1.37 1.2038 -4 9 3 4 79.76 1.32 1.2024 0 8 5 4 80.02 1.61 1.1990 2 14 0 4 80.62 1.55 1.1917 0 0 6 2 80.89 1.08 1.1883 -2 14 1 4 81.14 4.71 1.1854 -4 7 4 4 81.22 1.56 1.1844 2 6 5 4 81.29 1.05 1.1835 -5 8 2 4 81.31 1.01 1.1833 -5 1 4 4 81.45 2.67 1.1816 4 11 1 4 81.64 1.59 1.1793 4 4 4 4 81.65 1.01 1.1793 -3 6 5 4 81.90 2.94 1.1762 -6 2 2 4 82.05 1.39 1.1745 5 3 3 4 82.13 1.41 1.1736 3 8 4 4 82.19 1.05 1.1728 6 2 1 4 82.57 2.29 1.1684 2 10 4 4 82.58 2.30 1.1683 0 3 6 4 83.29 1.54 1.1601 -2 11 4 4 83.55 1.04 1.1572 -5 7 3 4 83.57 1.13 1.1570 1 1 6 4 83.76 2.42 1.1549 -2 2 6 4 83.97 2.07 1.1524 6 5 0 4 84.15 4.22 1.1505 4 12 0 4 84.52 1.53 1.1464 -3 13 2 4 84.57 1.23 1.1458 -5 4 4 4 84.81 1.05 1.1432 -2 13 3 4 85.07 3.96 1.1403 0 12 4 4 85.09 1.56 1.1401 -4 4 5 4 85.41 1.94 1.1367 4 9 3 4 86.05 1.31 1.1298 0 5 6 4 86.26 1.68 1.1276 -6 6 1 4 86.28 2.91 1.1274 -5 10 1 4 86.46 1.61 1.1256 -6 5 2 4 86.56 1.24 1.1245 0 15 2 4 87.38 2.16 1.1160 3 13 2 4 87.66 2.36 1.1132 -1 10 5 4 88.24 1.15 1.1074 -6 3 3 4 88.30 1.75 1.1068 -2 5 6 4 88.33 1.82 1.1065 -4 11 3 4 89.19 1.11 1.0980 1 16 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.