data_global _amcsd_formula_title 'B Cl4 K O12 S4' loop_ _publ_author_name 'Mairesse G' 'Drache M' _journal_name_full 'Acta Crystallographica, Section B' _journal_volume 34 _journal_year 1978 _journal_page_first 1771 _journal_page_last 1776 _publ_section_title ; The crystal structure of potassium tetrachlorosulfatoborate, K (B (SO3 Cl)4) _cod_database_code 1004039 ; _database_code_amcsd 0009643 _chemical_formula_sum 'K B S4 Cl4 O12' _cell_length_a 10.513 _cell_length_b 10.838 _cell_length_c 10.965 _cell_angle_alpha 99.21 _cell_angle_beta 135.48 _cell_angle_gamma 97.15 _cell_volume 811.699 _exptl_crystal_density_diffrn 2.095 _symmetry_space_group_name_H-M 'P 1' loop_ _space_group_symop_operation_xyz 'x,y,z' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z K1 0.79910 -0.07100 0.39570 B1 0.00000 0.00000 0.00000 S1 -0.12240 0.20840 -0.06330 Cl1 -0.21870 0.25180 -0.27870 O1 -0.01870 0.11720 -0.05540 O2 0.01660 0.32730 0.09380 O3 -0.27870 0.13970 -0.10590 S2 0.34130 0.05930 0.12910 Cl2 0.26990 0.11400 -0.07380 O4 0.14730 -0.03600 0.02880 O5 0.45920 -0.01680 0.17380 O6 0.40920 0.17570 0.26760 S3 -0.28000 -0.20090 -0.33230 Cl3 -0.14790 -0.33380 -0.27340 O7 -0.17970 -0.11580 -0.14150 O8 -0.47320 -0.27220 -0.44190 O9 -0.23850 -0.12470 -0.39970 S4 0.06020 -0.05630 0.26220 Cl4 0.28520 0.06050 0.52120 O10 0.04800 0.03600 0.16570 O11 0.09910 -0.16760 0.22530 O12 -0.09550 -0.07950 0.23190 K2 0.13190 0.59500 0.22860 B2 0.26170 0.52440 0.76110 Cl5 -0.20830 0.27210 0.23180 O13 0.12580 0.40670 0.58930 O14 -0.04900 0.19700 0.52780 O15 -0.15570 0.38380 0.51670 S5 -0.06890 0.31550 0.49000 S6 0.54430 0.46490 0.83220 Cl6 0.41760 0.40980 0.57390 O16 0.44550 0.56030 0.82680 O17 0.73840 0.54010 0.95320 O18 0.49540 0.34790 0.85350 S7 0.18290 0.72480 0.63040 Cl7 0.44790 0.85780 0.82220 O19 0.19800 0.64010 0.73680 O20 0.06220 0.79670 0.59310 O21 0.14820 0.64990 0.48740 S8 0.37860 0.58040 0.08050 Cl8 0.48710 0.46340 0.22310 O22 0.27460 0.48820 0.89230 O23 0.53000 0.69180 0.15630 O24 0.24730 0.60430 0.07400