H10 Na2 O8 S2 Lisensky G, Levy H Acta Crystallographica B34 (1978) 1975-1977 Sodium thiosulfate pentahydrate: a redetermination by neutron diffraction _cod_database_code 1008026 _database_code_amcsd 0015973 CELL PARAMETERS: 5.9522 21.6180 7.5430 90.000 103.804 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 942.560 Density (g/cm3): 1.749 MAX. ABS. INTENSITY / VOLUME**2: 2.738488237 RIR: 0.510 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.18 2.50 10.8090 0 2 0 2 12.76 5.94 6.9377 0 1 1 4 14.61 27.23 6.0639 0 2 1 4 15.33 50.03 5.7803 1 0 0 2 15.87 26.11 5.5841 1 1 0 4 16.40 100.00 5.4045 0 4 0 2 17.26 13.77 5.1370 0 3 1 4 17.40 2.37 5.0972 1 2 0 4 17.61 17.43 5.0356 -1 1 1 4 19.00 17.36 4.6699 -1 2 1 4 19.69 28.87 4.5089 1 3 0 4 20.42 4.37 4.3489 0 4 1 4 21.13 28.57 4.2050 -1 3 1 4 22.13 2.23 4.0169 1 1 1 4 22.52 14.03 3.9477 1 4 0 4 23.26 44.03 3.8237 1 2 1 4 23.90 1.61 3.7234 0 5 1 4 24.30 37.11 3.6626 0 0 2 2 24.65 6.92 3.6111 0 1 2 4 24.71 6.54 3.6030 0 6 0 2 25.04 33.45 3.5557 1 3 1 4 25.50 11.82 3.4935 -1 0 2 2 25.73 2.26 3.4622 1 5 0 4 25.83 26.54 3.4488 -1 1 2 4 26.82 37.35 3.3242 -1 2 2 4 26.86 5.60 3.3188 -1 5 1 4 28.39 35.14 3.1436 -1 3 2 4 29.46 2.15 3.0319 0 4 2 4 30.22 59.03 2.9575 -1 6 1 4 30.47 5.11 2.9339 -1 4 2 4 30.71 36.68 2.9117 -2 1 1 4 30.94 12.25 2.8901 2 0 0 2 31.22 41.49 2.8647 2 1 0 4 31.44 28.35 2.8457 0 7 1 4 31.55 9.17 2.8355 -2 2 1 4 31.89 2.15 2.8059 1 0 2 2 32.03 62.84 2.7946 0 5 2 4 32.17 21.01 2.7825 1 1 2 4 32.88 5.77 2.7239 1 7 0 4 32.92 2.25 2.7209 -2 3 1 4 32.98 3.54 2.7159 1 2 2 4 34.30 8.55 2.6147 1 3 2 4 34.65 5.03 2.5890 -2 0 2 2 34.93 5.03 2.5685 0 6 2 4 35.21 4.31 2.5486 2 4 0 4 35.41 6.11 2.5352 0 8 1 4 35.80 13.22 2.5081 -1 6 2 4 36.07 7.09 2.4903 1 4 2 4 36.27 1.11 2.4766 2 1 1 4 36.46 11.15 2.4642 1 7 1 4 36.61 31.54 2.4545 -1 1 3 4 36.71 22.41 2.4480 1 8 0 4 36.89 1.42 2.4365 -2 3 2 4 37.01 21.68 2.4293 2 2 1 4 38.12 2.24 2.3610 0 7 2 4 38.20 8.63 2.3560 2 3 1 4 38.24 13.33 2.3537 1 5 2 4 38.52 2.05 2.3369 -1 3 3 4 39.48 1.65 2.2824 0 9 1 4 39.58 4.48 2.2772 -2 6 1 4 39.82 10.99 2.2638 2 4 1 4 40.00 7.29 2.2543 1 8 1 4 40.54 4.46 2.2252 0 4 3 4 40.68 13.34 2.2181 1 9 0 4 41.44 7.80 2.1790 -1 9 1 4 41.78 4.61 2.1618 0 10 0 2 42.13 1.81 2.1450 -1 5 3 4 42.28 2.92 2.1374 -1 8 2 4 42.52 2.10 2.1261 0 5 3 4 43.02 9.34 2.1025 -2 6 2 4 43.24 6.61 2.0925 -2 2 3 4 43.66 3.62 2.0734 0 10 1 4 43.71 1.84 2.0710 1 9 1 4 43.75 6.03 2.0690 1 1 3 4 44.46 10.01 2.0375 -1 6 3 4 44.52 9.98 2.0349 2 1 2 4 44.76 1.71 2.0248 1 10 0 4 44.84 1.70 2.0213 0 6 3 4 45.14 6.95 2.0086 0 9 2 4 45.14 1.44 2.0084 2 2 2 4 45.41 1.14 1.9971 1 3 3 4 45.47 4.13 1.9949 -1 10 1 4 45.73 1.84 1.9839 -2 4 3 4 45.85 3.30 1.9793 -1 9 2 4 46.55 2.96 1.9509 -3 2 1 4 46.83 1.20 1.9400 1 4 3 4 46.83 1.06 1.9398 2 7 1 4 47.11 1.88 1.9292 -1 7 3 4 47.47 1.42 1.9154 0 7 3 4 47.54 1.92 1.9128 -2 5 3 4 47.55 3.87 1.9123 -3 3 1 4 47.58 7.07 1.9110 1 10 1 4 47.81 3.27 1.9025 -3 0 2 2 48.43 2.57 1.8797 -1 0 4 2 48.92 1.03 1.8620 -3 4 1 4 48.92 1.59 1.8617 0 10 2 4 49.20 1.40 1.8519 -1 2 4 4 49.31 5.91 1.8479 2 5 2 4 49.56 6.61 1.8394 -3 3 2 4 49.59 5.42 1.8383 -1 10 2 4 49.62 2.18 1.8374 -1 11 1 4 49.67 2.39 1.8354 -2 6 3 4 49.98 2.37 1.8247 0 1 4 4 50.37 13.89 1.8117 0 8 3 4 50.63 6.69 1.8028 -3 5 1 4 50.88 8.91 1.7945 -3 4 2 4 51.60 9.88 1.7712 1 11 1 4 51.93 1.93 1.7609 -2 9 2 4 52.05 1.85 1.7569 3 1 1 4 52.11 11.04 1.7550 -2 7 3 4 52.29 3.95 1.7494 0 12 1 4 52.60 1.33 1.7398 3 2 1 4 52.87 2.72 1.7317 0 11 2 4 53.11 4.19 1.7243 1 7 3 4 53.78 1.38 1.7045 2 7 2 4 53.78 2.85 1.7044 -3 2 3 4 53.88 1.90 1.7015 -1 12 1 4 54.41 1.23 1.6863 0 5 4 4 54.55 1.21 1.6823 -3 6 2 4 54.68 2.03 1.6785 -3 3 3 4 54.78 5.62 1.6759 3 4 1 4 54.84 1.87 1.6742 -2 8 3 4 55.02 1.05 1.6689 -3 7 1 4 55.76 4.51 1.6485 1 12 1 4 56.28 1.50 1.6347 3 7 0 4 56.29 2.46 1.6345 2 3 3 4 56.36 1.46 1.6325 0 6 4 4 56.37 5.19 1.6323 3 5 1 4 56.37 3.76 1.6323 1 1 4 4 56.57 3.70 1.6269 -1 10 3 4 56.85 2.65 1.6196 -2 5 4 4 56.89 1.21 1.6186 0 10 3 4 56.89 3.65 1.6185 1 2 4 4 57.76 1.41 1.5963 1 3 4 4 57.81 1.52 1.5949 -2 9 3 4 58.27 2.39 1.5834 3 6 1 4 58.87 1.57 1.5688 3 8 0 4 58.96 1.21 1.5666 1 4 4 4 59.01 1.19 1.5654 -2 11 2 4 59.90 1.73 1.5441 0 14 0 2 59.95 1.20 1.5431 -1 8 4 4 59.96 1.81 1.5429 3 2 2 4 60.47 1.97 1.5309 1 5 4 4 60.93 1.55 1.5204 -2 7 4 4 61.13 1.02 1.5160 0 8 4 4 61.55 3.15 1.5067 -3 7 3 4 61.58 1.10 1.5061 -3 2 4 4 62.63 1.09 1.4832 -4 1 1 4 62.84 1.01 1.4787 -2 12 2 4 63.04 8.14 1.4745 2 7 3 4 63.12 3.03 1.4728 -4 2 1 4 63.74 1.18 1.4602 2 12 1 4 63.92 1.37 1.4563 0 9 4 4 63.94 1.36 1.4560 -4 3 1 4 64.09 1.20 1.4529 -1 4 5 4 64.37 1.98 1.4472 -2 13 1 4 64.48 1.58 1.4451 4 0 0 2 64.68 1.54 1.4411 -2 2 5 4 65.00 1.17 1.4347 -3 5 4 4 65.34 2.98 1.4282 -3 10 2 4 65.35 2.93 1.4280 1 11 3 4 65.47 1.15 1.4256 2 8 3 4 66.15 2.60 1.4127 -2 9 4 4 66.67 1.48 1.4029 2 0 4 2 66.87 1.01 1.3992 -2 13 2 4 67.07 1.74 1.3955 -4 1 3 4 67.31 2.47 1.3911 -4 5 2 4 67.46 3.62 1.3884 -1 15 1 4 67.50 1.49 1.3875 0 5 5 4 68.46 1.08 1.3705 4 5 0 4 68.66 2.54 1.3669 -2 14 1 4 70.26 2.21 1.3398 0 11 4 4 70.52 1.97 1.3354 1 2 5 4 70.93 1.47 1.3287 0 16 1 4 71.13 2.07 1.3254 -3 8 4 4 73.73 1.32 1.2850 -3 9 4 4 76.74 1.15 1.2419 1 17 0 4 78.51 2.44 1.2183 -4 6 4 4 78.94 1.21 1.2128 0 10 5 4 80.03 1.27 1.1989 -3 14 2 4 80.13 1.90 1.1977 4 5 2 4 81.75 1.75 1.1780 4 6 2 4 81.85 1.01 1.1768 3 3 4 4 82.65 1.13 1.1675 -4 8 4 4 82.95 1.29 1.1640 2 17 0 4 83.05 1.01 1.1628 -3 1 6 4 84.97 1.05 1.1414 -2 17 2 4 87.30 1.24 1.1168 5 5 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.