H14 K4 Ni O25 P6 Seethanen D, Tordjman I, Averbuch-Pouchot M Acta Crystallographica B34 (1978) 2387-2390 Structure cristalline du trimetaphosphate mixte de nickelpotassium heptahydrate, Ni K4 (P3 O9)2 (H2 O)7, et donnees cristallographiques de Co K4 (P3 O9)2 (H2 O)7 _cod_database_code 1008027 _database_code_amcsd 0015974 CELL PARAMETERS: 23.0300 11.8820 8.7320 90.000 90.000 90.000 SPACE GROUP: Fm2m X-RAY WAVELENGTH: 1.541838 Cell Volume: 2389.446 Density (g/cm3): 2.226 MAX. ABS. INTENSITY / VOLUME**2: 8.755965417 RIR: 1.281 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.68 32.09 11.5150 2 0 0 2 13.16 11.17 6.7292 1 1 1 4 14.91 14.30 5.9410 0 2 0 1 16.79 26.69 5.2797 2 2 0 2 17.09 100.00 5.1871 3 1 1 4 21.49 32.37 4.1345 4 2 0 2 21.77 1.01 4.0824 2 0 2 4 23.08 26.91 3.8537 5 1 1 4 23.17 3.76 3.8383 6 0 0 2 24.99 43.79 3.5635 1 3 1 4 25.32 8.30 3.5181 0 2 2 2 25.61 10.69 3.4789 4 0 2 4 26.49 83.18 3.3646 2 2 2 4 27.32 14.72 3.2646 3 3 1 4 27.67 5.32 3.2240 6 2 0 2 29.76 46.78 3.0020 4 2 2 4 30.08 12.09 2.9705 0 4 0 1 31.02 1.68 2.8827 6 0 2 4 31.07 47.62 2.8788 8 0 0 2 31.09 2.32 2.8763 2 4 0 2 31.50 3.28 2.8398 5 3 1 4 31.89 8.33 2.8060 1 1 3 4 33.79 16.86 2.6529 3 1 3 4 33.96 5.38 2.6399 4 4 0 2 34.58 11.66 2.5935 6 2 2 4 34.62 7.15 2.5906 8 2 0 2 37.44 13.08 2.4019 2 4 2 4 38.31 2.92 2.3492 6 4 0 2 38.58 6.02 2.3334 1 3 3 4 39.11 1.54 2.3030 10 0 0 2 39.91 11.49 2.2590 4 4 2 4 40.20 5.56 2.2431 3 3 3 4 40.49 2.83 2.2279 8 2 2 4 41.08 2.00 2.1971 3 5 1 4 41.36 11.80 2.1830 0 0 4 2 42.08 1.98 2.1473 10 2 0 2 42.14 5.47 2.1442 7 1 3 4 43.29 5.04 2.0901 5 3 3 4 43.36 12.64 2.0870 9 3 1 4 43.76 12.47 2.0687 6 4 2 4 43.79 4.01 2.0673 8 4 0 2 44.12 2.98 2.0527 5 5 1 4 44.20 4.75 2.0491 0 2 4 2 44.38 1.30 2.0412 4 0 4 4 44.48 3.42 2.0370 10 0 2 4 45.19 4.88 2.0067 11 1 1 4 47.07 1.36 1.9304 4 2 4 4 47.17 17.35 1.9269 10 2 2 4 47.94 7.79 1.8976 6 0 4 4 48.39 2.19 1.8812 7 5 1 4 48.62 4.92 1.8727 4 6 0 2 49.69 8.68 1.8349 1 5 3 4 49.94 2.66 1.8262 12 2 0 2 50.49 3.81 1.8076 6 2 4 4 51.27 5.38 1.7818 2 6 2 4 51.98 1.71 1.7591 0 4 4 2 52.62 6.73 1.7394 8 0 4 4 52.63 1.34 1.7389 2 4 4 4 52.96 5.21 1.7290 9 3 3 4 53.33 2.99 1.7179 13 1 1 4 54.43 4.18 1.6857 3 1 5 4 54.46 3.73 1.6848 12 2 2 4 54.54 1.33 1.6825 11 1 3 4 54.55 4.53 1.6823 4 4 4 4 54.63 1.38 1.6799 10 4 2 4 55.01 2.11 1.6694 8 2 4 4 55.28 2.88 1.6619 1 7 1 4 56.37 3.16 1.6323 6 6 2 4 56.39 1.92 1.6316 8 6 0 2 56.92 2.08 1.6178 5 1 5 4 57.14 2.32 1.6120 12 4 0 2 57.36 5.50 1.6064 7 5 3 4 57.64 1.57 1.5991 6 4 4 4 57.84 2.08 1.5941 1 3 5 4 58.95 4.66 1.5669 5 7 1 4 59.15 3.99 1.5619 11 3 3 4 59.82 2.02 1.5461 11 5 1 4 61.80 2.09 1.5012 13 1 3 4 61.81 2.37 1.5010 8 4 4 4 62.12 2.87 1.4943 9 5 3 4 62.31 1.57 1.4902 14 2 2 4 63.11 1.30 1.4730 2 8 0 2 63.97 3.04 1.4553 0 0 6 2 64.67 2.04 1.4414 12 0 4 4 64.77 1.66 1.4394 16 0 0 2 64.83 5.26 1.4382 4 8 0 2 65.69 3.52 1.4213 4 6 4 4 65.77 3.12 1.4199 10 6 2 4 66.10 1.84 1.4136 13 3 3 4 66.66 5.00 1.4030 2 2 6 4 67.02 1.23 1.3963 9 7 1 4 67.79 1.74 1.3824 11 5 3 4 68.67 3.00 1.3667 14 4 2 4 69.33 2.37 1.3554 9 3 5 4 69.69 3.08 1.3492 15 1 3 4 70.69 2.22 1.3326 11 1 5 4 71.83 1.27 1.3143 12 6 2 4 72.82 1.99 1.2988 8 0 6 4 72.95 3.64 1.2968 12 4 4 4 73.76 1.44 1.2846 15 3 3 4 74.44 2.68 1.2745 4 4 6 4 74.87 1.33 1.2682 17 3 1 4 75.20 1.71 1.2635 8 8 2 4 76.29 1.58 1.2482 10 8 0 2 77.79 1.75 1.2278 18 0 2 4 78.73 1.32 1.2155 1 7 5 4 78.74 1.69 1.2154 14 6 2 4 79.57 2.40 1.2047 10 2 6 4 79.83 1.22 1.2015 14 4 4 4 79.86 1.52 1.2010 11 7 3 4 79.87 1.20 1.2010 4 8 4 4 80.75 1.02 1.1900 8 4 6 4 80.90 1.51 1.1882 1 3 7 4 81.66 2.13 1.1791 15 5 3 4 81.77 2.24 1.1778 16 2 4 4 81.85 1.19 1.1768 5 7 5 4 82.04 2.13 1.1746 12 8 0 2 82.61 1.05 1.1679 11 5 5 4 82.72 1.07 1.1667 2 6 6 4 84.51 1.36 1.1465 0 10 2 2 85.02 1.24 1.1409 2 10 2 4 86.08 1.38 1.1295 8 8 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.