Borax Levy H A, Lisensky G C Acta Crystallographica B34 (1978) 3502-3510 Crystal structures of sodium sulfate decahydrate (Glauber's salt) and sodium tetraborate decahydrate (borax). Redetermination by neutron diffraction Locality: Synthetic Note: anisoU's from ICSD _database_code_amcsd 0009647 CELL PARAMETERS: 11.8850 10.6540 12.2060 90.000 106.623 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1480.966 Density (g/cm3): 1.710 MAX. ABS. INTENSITY / VOLUME**2: 2.808514726 RIR: 0.535 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.37 8.49 7.7802 1 1 0 4 12.37 22.45 7.1547 -1 1 1 4 14.86 17.51 5.9627 1 1 1 4 15.15 4.81 5.8479 0 0 2 2 15.56 44.86 5.6941 2 0 0 2 16.64 4.22 5.3270 0 2 0 2 17.10 18.94 5.1868 -1 1 2 4 18.30 87.70 4.8479 0 2 1 4 22.58 26.34 3.9381 0 2 2 4 22.64 16.42 3.9283 -2 2 1 4 22.86 1.14 3.8901 2 2 0 4 24.75 4.60 3.5976 2 0 2 2 24.90 5.02 3.5759 3 1 0 4 25.46 1.29 3.4991 -3 1 2 4 25.50 3.17 3.4925 2 2 1 4 26.29 2.05 3.3903 1 3 0 4 26.75 4.84 3.3331 -1 3 1 4 27.99 5.03 3.1879 3 1 1 4 28.02 1.93 3.1846 1 3 1 4 28.37 1.14 3.1461 0 2 3 4 29.09 8.62 3.0700 -2 2 3 4 29.97 17.22 2.9814 2 2 2 4 30.10 28.65 2.9690 -2 0 4 2 30.49 1.89 2.9323 -1 1 4 4 30.57 7.48 2.9240 0 0 4 2 31.42 26.22 2.8471 4 0 0 2 31.61 61.13 2.8303 1 3 2 4 32.69 1.16 2.7398 3 1 2 4 33.65 4.80 2.6635 0 4 0 2 33.91 1.97 2.6434 -3 3 1 4 33.97 3.33 2.6387 -3 1 4 4 34.54 3.11 2.5970 0 4 1 4 34.59 1.57 2.5934 3 3 0 4 34.82 35.68 2.5763 1 1 4 4 35.00 99.71 2.5637 -3 3 2 4 35.16 17.78 2.5525 -4 2 2 4 35.65 1.65 2.5186 2 2 3 4 36.58 13.40 2.4568 1 3 3 4 37.72 7.49 2.3849 -3 3 3 4 38.42 19.60 2.3429 2 0 4 2 38.47 2.08 2.3398 3 1 3 4 38.52 1.40 2.3370 4 2 1 4 38.61 14.61 2.3321 -2 4 2 4 38.99 1.08 2.3100 -5 1 1 4 39.04 2.63 2.3072 -5 1 2 4 40.72 6.68 2.2157 3 3 2 4 41.04 4.13 2.1993 0 4 3 4 41.05 4.47 2.1988 -4 2 4 4 41.56 1.15 2.1728 -2 4 3 4 41.80 4.20 2.1612 -3 3 4 4 42.13 8.71 2.1447 2 2 4 4 42.22 1.95 2.1407 2 4 2 4 43.19 1.10 2.0945 1 5 0 4 43.49 3.98 2.0807 -1 5 1 4 43.66 6.73 2.0733 -5 1 4 4 44.34 6.25 2.0431 1 5 1 4 44.62 3.45 2.0308 -2 0 6 2 45.03 8.43 2.0133 3 1 4 4 45.64 1.65 1.9876 3 3 3 4 45.77 1.42 1.9824 -4 4 1 4 46.09 2.38 1.9692 -5 3 1 4 46.14 2.10 1.9675 -5 3 2 4 46.59 3.28 1.9493 0 0 6 2 46.61 5.55 1.9486 2 4 3 4 46.68 1.99 1.9460 -3 1 6 4 46.84 1.89 1.9397 1 5 2 4 46.95 1.35 1.9353 -3 3 5 4 47.54 7.19 1.9125 -5 3 3 4 47.87 2.11 1.9002 -5 1 5 4 47.93 5.49 1.8980 6 0 0 2 47.94 2.93 1.8976 -2 2 6 4 48.02 4.49 1.8947 -4 4 3 4 48.46 1.58 1.8783 -4 0 6 2 49.03 1.01 1.8581 3 5 0 4 49.10 5.41 1.8553 -6 2 2 4 49.17 3.17 1.8530 1 3 5 4 49.19 7.62 1.8523 -6 0 4 2 49.34 1.49 1.8471 -3 5 2 4 49.81 1.28 1.8306 0 2 6 4 51.06 2.94 1.7887 -4 4 4 4 51.46 1.56 1.7757 0 6 0 2 51.47 2.75 1.7756 3 3 4 4 51.60 2.10 1.7714 -4 2 6 4 51.98 1.02 1.7592 2 4 4 4 52.03 2.44 1.7576 0 4 5 4 52.09 9.83 1.7557 -1 3 6 4 52.40 3.99 1.7463 4 4 2 4 52.96 4.67 1.7289 -3 3 6 4 53.79 11.42 1.7044 5 3 2 4 53.82 2.32 1.7034 3 5 2 4 53.92 2.75 1.7003 6 2 1 4 53.97 2.77 1.6991 0 6 2 4 55.45 2.05 1.6571 -2 2 7 4 57.02 1.72 1.6152 -7 1 4 4 57.03 1.82 1.6150 -2 4 6 4 58.16 1.12 1.5861 2 4 5 4 58.27 1.47 1.5834 -5 5 1 4 58.69 2.61 1.5730 0 4 6 4 59.85 1.20 1.5454 3 1 6 4 60.44 1.36 1.5318 -7 3 2 4 60.92 1.07 1.5207 -6 4 4 4 61.05 3.96 1.5177 0 6 4 4 61.46 6.29 1.5086 1 7 0 4 62.57 3.23 1.4845 -4 0 8 2 65.29 1.26 1.4291 4 0 6 2 65.58 2.66 1.4235 8 0 0 2 66.02 1.48 1.4152 6 4 2 4 66.02 3.94 1.4152 2 6 4 4 70.18 1.23 1.3410 -1 5 7 4 70.30 1.71 1.3391 -3 5 7 4 71.00 1.07 1.3275 2 0 8 2 73.94 2.39 1.2818 -6 6 4 4 75.84 1.58 1.2545 7 5 1 4 77.87 1.19 1.2267 -9 1 6 4 82.31 1.06 1.1715 4 0 8 2 82.74 1.14 1.1664 -9 3 6 4 84.88 1.22 1.1424 0 2 10 4 87.83 1.28 1.1115 7 7 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.