Sarabauite Nakai I, Nagashima K, Koto K, Morimoto N Acta Crystallographica B34 (1978) 3569-3572 Crystal structure of oxide-chalcogenide. I.The crystal stucture of sarabauite CaSb10O10S6 Locality: Sarabau mine, Sarawak, Malaysia _database_code_amcsd 0009650 CELL PARAMETERS: 25.3700 5.6540 16.8700 90.000 117.580 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2144.885 Density (g/cm3): 4.985 MAX. ABS. INTENSITY / VOLUME**2: 44.08930977 RIR: 2.880 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.86 26.64 11.2435 2 0 0 2 10.76 8.63 8.2242 -2 0 2 2 11.84 3.23 7.4765 0 0 2 2 14.69 2.30 6.0302 -4 0 2 2 16.16 1.35 5.4833 1 1 0 4 17.85 4.78 4.9699 1 1 1 4 19.67 1.24 4.5139 3 1 0 4 19.94 39.31 4.4523 -3 1 2 4 21.03 21.49 4.2244 -6 0 2 2 21.15 28.11 4.2012 1 1 2 4 21.29 1.35 4.1725 -2 0 4 2 21.61 2.51 4.1121 -4 0 4 2 22.59 8.63 3.9361 -3 1 3 4 22.71 31.13 3.9148 -1 1 3 4 23.72 3.18 3.7510 -5 1 2 4 23.74 3.21 3.7478 6 0 0 2 23.78 1.39 3.7418 -5 1 1 4 23.80 2.92 3.7382 0 0 4 2 23.80 1.70 3.7382 4 0 2 2 25.47 3.43 3.4970 1 1 3 4 25.74 69.73 3.4608 3 1 2 4 26.38 10.05 3.3788 -3 1 4 4 27.31 1.05 3.2651 -1 1 4 4 27.81 100.00 3.2074 -5 1 4 4 28.07 33.77 3.1788 5 1 1 4 28.28 29.19 3.1561 -8 0 2 2 28.44 3.19 3.1388 2 0 4 2 29.28 5.32 3.0497 -7 1 2 4 29.71 3.68 3.0069 -7 1 3 4 30.09 3.52 2.9699 -7 1 1 4 30.42 1.76 2.9382 1 1 4 4 31.32 6.01 2.8556 -7 1 4 4 31.46 7.66 2.8434 -5 1 5 4 31.65 13.49 2.8270 0 2 0 2 31.78 36.83 2.8155 5 1 2 4 31.84 20.44 2.8110 -4 0 6 2 31.84 11.93 2.8109 8 0 0 2 32.04 12.35 2.7931 7 1 0 4 32.23 6.53 2.7778 0 2 1 4 32.44 1.28 2.7597 -1 1 5 4 32.53 15.61 2.7524 -2 2 1 4 32.66 2.88 2.7417 2 2 0 4 32.67 1.04 2.7414 -6 0 6 2 33.02 29.35 2.7129 -2 0 6 2 33.90 2.32 2.6443 0 2 2 4 33.97 6.31 2.6388 -7 1 5 4 34.42 12.64 2.6059 4 0 4 2 34.77 37.72 2.5801 -4 2 1 4 34.97 2.15 2.5655 7 1 1 4 35.18 2.47 2.5508 3 1 4 4 35.38 1.75 2.5368 -8 0 6 2 35.54 1.60 2.5256 4 2 0 4 35.61 1.19 2.5209 -9 1 3 4 35.82 5.51 2.5066 -10 0 4 2 35.98 2.68 2.4960 -3 1 6 4 35.99 2.03 2.4956 -10 0 2 2 36.04 7.76 2.4922 0 0 6 2 36.19 3.00 2.4824 5 1 3 4 37.46 4.89 2.4006 -7 1 6 4 37.93 1.04 2.3719 -1 1 6 4 38.11 9.67 2.3613 -9 1 5 4 38.31 1.01 2.3494 -6 2 2 4 38.46 1.22 2.3404 -2 2 4 4 38.65 1.72 2.3296 -4 2 4 4 38.69 3.88 2.3273 7 1 2 4 39.43 13.46 2.2854 9 1 0 4 39.95 1.07 2.2569 6 2 0 4 40.10 2.36 2.2487 10 0 0 2 41.26 2.36 2.1882 6 0 4 2 41.62 2.54 2.1698 -7 1 7 4 42.49 5.57 2.1274 -11 1 4 4 42.81 1.08 2.1122 -12 0 4 2 42.92 1.96 2.1070 -6 0 8 2 42.95 10.33 2.1058 -8 2 2 4 44.04 2.61 2.0560 -8 0 8 2 44.04 3.02 2.0560 -12 0 2 2 44.08 22.15 2.0544 0 2 5 4 44.84 2.39 2.0213 -11 1 1 4 45.33 2.96 2.0007 -11 1 6 4 45.51 2.33 1.9933 8 2 0 4 45.99 2.74 1.9733 -5 1 8 4 46.18 1.13 1.9659 4 0 6 2 46.26 1.89 1.9625 3 1 6 4 46.39 7.30 1.9574 -2 2 6 4 46.64 11.78 1.9474 -10 0 8 2 47.28 2.12 1.9225 11 1 0 4 47.30 7.12 1.9219 10 0 2 2 47.39 1.38 1.9185 1 1 7 4 47.45 1.43 1.9161 2 2 5 4 47.94 1.87 1.8977 -11 1 7 4 47.98 1.77 1.8959 8 2 1 4 48.20 5.61 1.8881 -8 2 6 4 48.20 14.54 1.8881 -10 2 3 4 48.67 1.23 1.8709 -10 2 2 4 48.71 5.86 1.8695 0 2 6 4 48.71 6.10 1.8694 6 2 3 4 48.72 3.29 1.8691 8 0 4 2 49.40 1.45 1.8447 -13 1 4 4 49.73 6.14 1.8335 -1 1 8 4 49.85 1.14 1.8294 -4 2 7 4 49.94 11.27 1.8263 -6 2 7 4 49.94 1.56 1.8263 -10 2 1 4 50.02 1.37 1.8236 -3 3 2 4 50.39 1.81 1.8109 -14 0 4 2 50.57 5.86 1.8051 1 3 2 4 50.99 6.80 1.7911 -13 1 6 4 50.99 1.65 1.7909 -13 1 2 4 51.16 3.45 1.7856 -2 2 7 4 51.23 1.58 1.7833 -11 1 8 4 51.26 2.59 1.7823 -3 3 3 4 51.32 8.10 1.7803 -1 3 3 4 51.42 2.07 1.7772 -8 2 7 4 51.47 1.33 1.7753 -14 0 6 2 51.59 2.09 1.7715 -10 2 6 4 51.63 2.81 1.7704 -5 1 9 4 51.96 1.43 1.7599 10 2 0 4 52.03 1.17 1.7578 4 2 5 4 52.09 4.26 1.7559 5 1 6 4 52.23 3.35 1.7513 3 1 7 4 52.32 2.70 1.7485 2 2 6 4 52.69 2.51 1.7373 6 0 6 2 52.91 1.25 1.7304 6 2 4 4 52.93 4.55 1.7299 -13 1 1 4 53.24 3.10 1.7204 -3 3 4 4 53.77 2.31 1.7048 -1 3 4 4 54.19 1.20 1.6926 11 1 2 4 54.20 14.07 1.6922 5 3 1 4 54.81 1.28 1.6749 -12 2 5 4 54.92 1.09 1.6718 -7 3 2 4 54.94 6.11 1.6712 8 2 3 4 55.17 1.44 1.6647 -7 3 3 4 55.24 1.91 1.6628 -8 2 8 4 55.24 2.12 1.6628 -12 2 2 4 55.56 1.04 1.6541 13 1 0 4 55.99 1.40 1.6423 -1 1 9 4 56.17 1.87 1.6376 -7 3 4 4 56.25 1.81 1.6353 -5 3 5 4 56.45 1.56 1.6300 5 3 2 4 56.71 3.42 1.6233 10 0 4 2 56.96 3.14 1.6168 -15 1 4 4 56.96 2.67 1.6166 -7 1 10 4 57.46 2.03 1.6037 -10 2 8 4 57.51 1.05 1.6025 -15 1 6 4 57.58 7.03 1.6007 -5 1 10 4 57.62 2.35 1.5998 2 2 7 4 57.87 2.46 1.5934 -7 3 5 4 58.47 6.76 1.5784 3 1 8 4 58.49 2.92 1.5781 -12 0 10 2 58.75 1.51 1.5716 7 1 6 4 58.86 3.12 1.5690 -15 1 7 4 59.28 6.69 1.5589 -15 1 2 4 59.55 1.90 1.5525 -11 1 10 4 60.51 3.01 1.5300 9 1 5 4 60.70 3.70 1.5257 -9 3 5 4 60.89 5.25 1.5214 -15 1 8 4 61.30 4.55 1.5122 -10 2 9 4 61.51 2.01 1.5075 -16 0 8 2 61.64 1.55 1.5046 9 3 0 4 62.65 1.79 1.4829 -13 1 10 4 62.66 3.88 1.4825 13 1 2 4 62.84 1.37 1.4788 -7 1 11 4 62.87 1.43 1.4783 5 3 4 4 63.30 1.02 1.4692 11 1 4 4 64.28 1.01 1.4491 15 1 0 4 64.35 1.70 1.4477 5 1 8 4 64.46 1.32 1.4456 -11 1 11 4 65.29 1.23 1.4291 6 0 8 2 66.39 1.04 1.4081 -18 0 6 2 66.41 2.02 1.4078 10 2 4 4 66.59 1.31 1.4043 -5 3 8 4 67.32 2.37 1.3908 -6 0 12 2 67.51 1.53 1.3874 -3 3 8 4 67.69 1.68 1.3842 1 3 7 4 67.76 1.30 1.3829 -16 2 5 4 67.96 1.59 1.3793 -4 4 1 4 68.14 1.44 1.3762 -14 2 9 4 68.97 1.25 1.3615 -16 2 3 4 70.16 2.76 1.3414 14 2 1 4 70.22 4.51 1.3405 -6 4 2 4 70.43 1.30 1.3369 -18 0 2 2 71.09 1.81 1.3261 7 1 8 4 71.14 1.96 1.3253 -5 3 9 4 71.64 2.83 1.3173 3 3 7 4 71.92 2.28 1.3128 13 1 4 4 72.22 2.63 1.3081 -13 3 1 4 72.32 1.75 1.3065 -2 0 12 2 73.47 1.02 1.2888 2 4 4 4 74.21 1.12 1.2779 0 4 5 4 74.30 1.01 1.2766 -2 2 11 4 74.62 1.40 1.2719 4 2 9 4 74.82 1.62 1.2690 -1 3 9 4 74.86 2.34 1.2684 -20 0 6 2 75.07 1.47 1.2653 -15 1 12 4 75.25 1.50 1.2628 -4 4 6 4 75.44 1.29 1.2601 -18 2 5 4 76.21 1.86 1.2493 18 0 0 2 76.70 2.06 1.2425 4 4 4 4 77.27 1.12 1.2348 -10 4 3 4 77.31 2.75 1.2342 -15 3 7 4 77.83 1.09 1.2272 -3 3 10 4 78.77 1.12 1.2150 9 3 5 4 81.57 1.52 1.1801 2 0 12 2 81.76 1.08 1.1779 -10 2 13 4 82.11 1.53 1.1738 -6 4 8 4 82.73 1.10 1.1666 10 2 7 4 82.90 1.69 1.1646 -6 2 13 4 85.22 1.32 1.1387 10 4 2 4 85.42 1.41 1.1366 -20 0 12 2 87.69 2.09 1.1129 1 5 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.