data_global
_amcsd_formula_title 'Sb2(S2O7)3'
loop_
_publ_author_name
'Douglade J'
'Mercier R'
_journal_name_full 'Acta Crystallographica, Section B'
_journal_volume 35 
_journal_year 1979
_journal_page_first 1062
_journal_page_last 1067
_publ_section_title
;
 Structure cristalline du disulfate d'antimoine(III) Sb2(S2O7)3
;
_database_code_amcsd 0009666
_chemical_formula_sum 'Sb2 S6 O21'
_cell_length_a 6.644
_cell_length_b 12.390
_cell_length_c 9.678
_cell_angle_alpha 92.69
_cell_angle_beta 82.29
_cell_angle_gamma 96.88
_cell_volume 783.412
_exptl_crystal_density_diffrn      3.272
_symmetry_space_group_name_H-M 'P -1'
loop_
_space_group_symop_operation_xyz
  'x,y,z'
  '-x,-y,-z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
Sb1  -0.27750   0.21130  -0.09170   0.01558
Sb2   0.26100   0.24300   0.41390   0.01267
S1   0.03780   0.04560  -0.27440   0.01013
S2   0.39050  -0.04210  -0.19900   0.00950
S3   0.16050   0.25780   0.06400   0.01001
S4   0.41480   0.42280   0.17880   0.01216
S5   0.06940   0.40670   0.68720   0.01026
S6  -0.21350   0.28910   0.52810   0.01039
O1  -0.08460   0.09830  -0.15510   0.01938
O2   0.18590   0.12020  -0.34940   0.02267
O3  -0.08470  -0.02920  -0.35090   0.02216
O4   0.15200  -0.02410  -0.17690   0.01925
O5   0.50590   0.06320  -0.20030   0.01950
O6   0.42500  -0.10760  -0.32180   0.02622
O7   0.39980  -0.09830  -0.07070   0.01925
O8  -0.05980   0.25170   0.05860   0.01621
O9   0.20140   0.20320   0.18560   0.01621
O10   0.28080   0.22850  -0.06180   0.01836
O11   0.21630   0.38530   0.09560   0.01507
O12   0.44400   0.53680   0.16520   0.02140
O13   0.56960   0.35680   0.12260   0.02166
O14   0.32790   0.39440   0.32600   0.01494
O15   0.22190   0.34850   0.59950   0.01849
O16  -0.01340   0.34690   0.81020   0.02026
O17   0.12650   0.51850   0.70760   0.02356
O18  -0.11970   0.40280   0.59190   0.01406
O19  -0.24760   0.21170   0.63610   0.02204
O20  -0.38590   0.31710   0.47180   0.02115
O21  -0.05210   0.26070   0.41540   0.01912