As6 H30 N4 O34 V4 Durif A, Averbuch-Pouchot M Acta Crystallographica B35 (1979) 1441-1444 Structure d'un arsenato vanadate d'ammonium. (NH4)4H6(As6V4O30)(H2O)4 _cod_database_code 1007036 _database_code_amcsd 0009671 CELL PARAMETERS: 14.4000 16.3100 9.8310 90.000 136.290 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 1595.503 Density (g/cm3): 2.608 MAX. ABS. INTENSITY / VOLUME**2: 30.14981879 RIR: 3.764 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.41 100.00 8.4945 1 1 0 4 10.52 9.00 8.4093 -1 1 1 4 10.85 30.39 8.1550 0 2 0 2 12.29 7.00 7.1993 -2 0 1 2 13.03 25.11 6.7933 0 0 1 2 16.42 13.57 5.3971 -2 2 1 4 17.83 4.17 4.9753 2 0 0 2 20.28 1.86 4.3784 -3 1 1 4 20.45 3.58 4.3433 -3 1 2 4 20.92 24.45 4.2472 2 2 0 4 21.13 6.20 4.2047 -2 2 2 4 21.35 17.25 4.1609 -1 1 2 4 21.80 8.76 4.0775 0 4 0 2 25.48 15.02 3.4961 0 4 1 4 25.68 8.92 3.4693 -3 3 2 4 26.24 3.53 3.3967 0 0 2 2 26.28 2.22 3.3905 1 3 1 4 26.41 6.57 3.3742 -1 3 2 4 27.08 5.59 3.2931 -4 2 2 4 27.81 8.66 3.2076 -3 1 3 4 27.89 1.67 3.1990 -4 0 1 2 28.22 5.38 3.1627 -4 0 3 2 28.30 8.99 3.1537 2 4 0 4 28.46 23.09 3.1361 -2 4 2 4 28.47 7.62 3.1355 0 2 2 4 28.84 2.53 3.0955 -1 5 1 4 28.91 1.94 3.0884 2 0 1 2 29.23 2.52 3.0557 -2 0 3 2 30.01 3.33 2.9781 -4 2 1 4 30.96 10.59 2.8882 2 2 1 4 31.26 1.92 2.8614 -2 2 3 4 31.60 2.79 2.8315 3 3 0 4 31.93 3.01 2.8031 -3 3 3 4 32.16 10.48 2.7836 -5 1 2 4 32.95 1.08 2.7183 0 6 0 2 33.20 4.27 2.6985 -4 4 2 4 33.82 1.60 2.6501 -3 5 1 4 33.93 4.67 2.6423 -3 5 2 4 34.11 2.03 2.6287 -1 1 3 4 34.36 1.08 2.6098 0 4 2 4 34.50 4.62 2.5995 -1 5 2 4 35.82 3.10 2.5068 -5 3 2 4 35.94 1.62 2.4991 -4 4 3 4 35.98 2.29 2.4958 -5 3 3 4 37.60 2.38 2.3919 -1 3 3 4 37.71 4.67 2.3855 2 6 0 4 37.83 1.11 2.3779 -2 6 2 4 38.99 3.73 2.3099 -3 5 3 4 39.13 1.39 2.3022 -6 2 3 4 39.66 4.39 2.2726 -6 0 2 2 40.02 4.89 2.2530 -6 0 4 2 40.45 1.62 2.2302 -5 3 1 4 41.24 2.25 2.1892 -6 2 2 4 41.38 1.71 2.1819 0 2 3 4 41.43 2.30 2.1793 3 3 1 4 41.63 1.90 2.1693 -4 6 2 4 43.74 1.73 2.0697 -3 7 2 4 43.75 6.63 2.0693 1 5 2 4 44.40 2.25 2.0405 2 6 1 4 44.44 2.35 2.0387 0 8 0 2 45.01 1.39 2.0141 -7 1 4 4 47.51 1.52 1.9138 1 1 3 4 47.70 1.81 1.9066 3 7 0 4 49.11 3.18 1.8550 -4 2 5 4 50.79 2.68 1.7975 -5 7 2 4 50.92 1.14 1.7934 -5 7 3 4 52.03 1.52 1.7575 -8 2 4 4 52.04 3.04 1.7572 -6 4 5 4 52.16 2.19 1.7537 -1 7 3 4 52.48 2.76 1.7435 4 4 1 4 54.07 1.90 1.6960 -8 2 5 4 54.38 2.45 1.6871 -2 6 4 4 54.39 1.62 1.6869 -5 7 1 4 55.37 1.07 1.6592 1 5 3 4 55.41 1.54 1.6581 2 0 3 2 55.53 2.16 1.6549 -3 7 4 4 55.84 2.04 1.6466 -8 4 4 4 56.42 2.21 1.6310 0 10 0 2 56.43 2.90 1.6306 -7 5 2 4 58.20 1.68 1.5853 -3 9 3 4 59.23 1.09 1.5600 -4 6 5 4 59.55 1.08 1.5524 -8 2 6 4 61.04 1.02 1.5181 -6 4 6 4 61.78 1.49 1.5017 -4 2 6 4 61.82 2.53 1.5007 -8 6 4 4 61.98 1.24 1.4972 1 1 4 4 62.36 1.88 1.4890 -8 4 2 4 62.70 1.45 1.4818 -1 7 4 4 63.66 1.35 1.4618 -8 6 5 4 64.19 1.09 1.4508 5 5 1 4 64.53 1.47 1.4441 4 4 2 4 65.99 1.41 1.4157 6 6 0 4 66.72 1.93 1.4018 -1 11 2 4 71.92 2.14 1.3129 -5 11 2 4 75.03 1.50 1.2659 -2 4 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.