Minasragrite Tachez M, Theobald F R, Watson K J, Mercier R Acta Crystallographica B35 (1979) 1545-1550 Redetermination de la structure du sulfate de vanadyle pentahydrate VOSO4*5H2O Locality: synthetic Note: anisoB's from ICSD _database_code_amcsd 0009674 CELL PARAMETERS: 6.9760 9.7160 12.9020 90.000 110.900 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 816.945 Density (g/cm3): 2.057 MAX. ABS. INTENSITY / VOLUME**2: 7.120603757 RIR: 1.127 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.70 7.31 7.5644 0 1 1 4 13.59 2.49 6.5170 1 0 0 2 14.70 16.93 6.0266 0 0 2 2 15.84 6.52 5.5955 -1 1 1 4 16.08 17.88 5.5121 -1 0 2 2 16.38 64.63 5.4123 1 1 0 4 17.32 100.00 5.1214 0 1 2 4 18.26 2.03 4.8580 0 2 0 2 19.70 1.07 4.5058 0 2 1 4 19.87 3.98 4.4675 1 1 1 4 22.44 16.14 3.9616 -1 2 1 4 22.83 56.83 3.8949 1 2 0 4 23.34 30.03 3.8114 -1 1 3 4 23.41 20.21 3.8002 1 0 2 2 23.52 7.88 3.7822 0 2 2 4 23.97 20.86 3.7128 0 1 3 4 24.42 37.61 3.6446 -1 2 2 4 25.16 10.27 3.5391 1 1 2 4 25.49 16.56 3.4946 1 2 1 4 26.04 18.43 3.4223 -2 0 2 2 27.27 5.57 3.2705 -2 1 1 4 27.84 1.55 3.2051 -1 0 4 2 28.31 5.04 3.1525 -1 2 3 4 28.54 8.64 3.1277 0 3 1 4 28.90 3.60 3.0894 2 1 0 4 29.34 8.26 3.0437 -1 1 4 4 29.65 22.19 3.0133 0 0 4 2 29.93 15.32 2.9851 -2 1 3 4 30.83 13.01 2.9003 1 3 0 4 31.07 7.38 2.8780 0 1 4 4 31.36 1.12 2.8528 0 3 2 4 31.67 14.37 2.8254 -2 2 1 4 31.99 6.91 2.7978 -2 2 2 4 32.89 1.59 2.7232 1 3 1 4 33.10 9.36 2.7061 2 2 0 4 33.81 1.28 2.6514 -2 1 4 4 35.04 1.25 2.5607 0 2 4 4 35.17 1.19 2.5517 -1 3 3 4 35.61 1.72 2.5215 0 3 3 4 35.69 5.52 2.5154 2 0 2 2 36.11 1.41 2.4876 2 2 1 4 36.91 4.24 2.4351 2 1 2 4 37.01 4.70 2.4290 0 4 0 2 37.07 1.89 2.4253 1 0 4 2 37.78 6.76 2.3811 0 4 1 4 37.99 5.39 2.3687 -2 3 1 4 38.25 1.26 2.3531 1 1 4 4 38.26 7.66 2.3523 -2 3 2 4 39.22 5.57 2.2971 2 3 0 4 39.56 1.65 2.2781 -1 3 4 4 39.86 9.55 2.2615 -3 1 2 4 40.02 1.15 2.2532 -2 3 3 4 40.38 2.82 2.2337 2 2 2 4 40.56 2.25 2.2242 -3 1 1 4 40.59 2.58 2.2228 -1 4 2 4 40.62 1.23 2.2211 -3 1 3 4 40.91 2.14 2.2061 0 3 4 4 41.27 2.61 2.1874 1 4 1 4 41.57 1.47 2.1723 3 0 0 2 41.62 1.07 2.1699 1 2 4 4 42.17 2.74 2.1427 -2 2 5 4 42.65 1.07 2.1200 3 1 0 4 42.76 2.91 2.1146 -3 1 4 4 43.10 1.55 2.0989 -2 3 4 4 43.54 1.68 2.0786 0 4 3 4 43.84 1.15 2.0651 -3 2 3 4 44.73 3.02 2.0262 -2 1 6 4 44.92 1.99 2.0180 -1 3 5 4 45.13 3.57 2.0089 0 0 6 2 45.57 8.05 1.9905 -2 4 1 4 45.75 4.69 1.9831 3 2 0 4 45.81 4.23 1.9808 -2 4 2 4 45.86 3.23 1.9787 -3 2 4 4 45.98 2.21 1.9740 3 1 1 4 46.14 14.20 1.9672 0 1 6 4 46.22 6.36 1.9641 -1 2 6 4 46.64 3.74 1.9475 2 4 0 4 46.93 2.55 1.9359 -1 4 4 4 47.33 4.40 1.9205 -2 4 3 4 47.72 1.53 1.9057 -2 2 6 4 48.18 2.61 1.8889 -3 3 2 4 48.35 1.36 1.8823 1 4 3 4 48.83 2.13 1.8652 -3 3 3 4 48.84 1.70 1.8648 2 1 4 4 48.91 2.90 1.8622 1 5 0 4 48.91 1.43 1.8621 3 2 1 4 49.27 2.20 1.8494 0 5 2 4 49.41 1.20 1.8445 3 0 2 2 50.05 1.51 1.8223 -2 4 4 4 50.34 4.12 1.8127 1 5 1 4 50.65 2.17 1.8023 -1 1 7 4 51.27 3.25 1.7820 -2 1 7 4 51.98 1.61 1.7593 -1 5 3 4 52.43 1.70 1.7452 -2 3 6 4 52.71 2.21 1.7366 -4 0 2 2 53.12 1.88 1.7240 1 1 6 4 53.56 1.03 1.7110 0 4 5 4 54.08 2.24 1.6958 -2 5 1 4 54.45 1.37 1.6852 -4 1 4 4 55.02 1.46 1.6690 2 5 0 4 55.19 1.75 1.6643 -3 4 1 4 56.12 3.91 1.6389 2 3 4 4 56.26 5.83 1.6353 -4 2 2 4 57.34 1.18 1.6068 4 1 0 4 57.51 1.03 1.6025 -2 0 8 2 58.08 1.75 1.5881 -2 5 4 4 58.52 1.31 1.5772 -1 1 8 4 58.58 2.90 1.5758 -1 6 1 4 59.60 2.13 1.5513 3 4 1 4 59.73 1.17 1.5481 -3 4 5 4 60.04 1.10 1.5409 1 3 6 4 60.49 1.82 1.5305 -4 3 2 4 61.03 1.04 1.5183 -1 2 8 4 61.27 2.41 1.5130 -4 3 4 4 61.48 1.76 1.5082 -1 6 3 4 62.26 2.14 1.4911 -3 5 2 4 64.07 2.11 1.4534 3 2 4 4 64.10 2.56 1.4528 -2 4 7 4 64.33 1.33 1.4482 -3 2 8 4 65.57 2.13 1.4237 2 2 6 4 65.90 1.72 1.4173 -2 5 6 4 66.11 1.02 1.4134 2 6 1 4 66.15 1.04 1.4127 -4 4 2 4 67.53 1.33 1.3871 1 3 7 4 68.78 1.53 1.3649 1 0 8 2 69.84 1.03 1.3467 1 6 4 4 69.89 1.52 1.3460 -1 7 2 4 70.38 1.03 1.3376 -2 4 8 4 70.43 1.26 1.3369 -5 2 4 4 73.47 2.00 1.2889 -2 7 1 4 74.80 1.56 1.2693 -5 3 2 4 74.89 2.29 1.2680 -4 3 8 4 77.50 1.08 1.2316 -5 3 6 4 81.46 1.21 1.1815 -1 3 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.