(NH4)6H6W12O42(H2O)10 Averbuch-Pouchot M, Tordjman I, Durif A, Guitel J Acta Crystallographica B35 (1979) 1675-1677 Structure d'un paratungstate d'ammonium (NH4)6H6W12O42(H2O)10 _cod_database_code 1007039 _database_code_amcsd 0009686 CELL PARAMETERS: 11.9400 13.2100 16.6300 102.460 97.310 88.610 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 2540.396 Density (g/cm3): 4.081 MAX. ABS. INTENSITY / VOLUME**2: 73.50329030 RIR: 5.865 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 5.49 3.45 16.1110 0 0 1 2 6.85 1.84 12.8988 0 1 0 2 7.81 100.00 11.3236 0 -1 1 2 8.70 37.97 10.1679 -1 0 1 2 9.66 48.95 9.1565 0 1 1 2 9.81 53.64 9.0194 1 0 1 2 10.12 1.41 8.7380 -1 1 0 2 10.16 19.88 8.7093 1 1 0 2 10.34 8.51 8.5555 -1 -1 1 2 10.98 34.61 8.0555 0 0 2 2 11.26 2.84 7.8578 1 -1 1 2 11.77 2.43 7.5157 -1 1 1 2 12.49 2.22 7.0852 -1 0 2 2 12.65 9.77 6.9996 1 1 1 2 13.73 7.09 6.4494 0 2 0 2 14.96 12.36 5.9214 2 0 0 2 15.26 2.14 5.8053 -1 -2 1 2 15.28 2.16 5.7975 -2 0 1 2 15.65 18.38 5.6618 0 -2 2 2 15.88 11.16 5.5798 1 -2 1 2 16.29 10.91 5.4405 -2 -1 1 2 16.58 6.96 5.3458 2 0 1 2 17.23 2.50 5.1479 -1 -1 3 2 17.23 3.15 5.1475 -2 1 1 2 17.26 1.64 5.1385 -1 0 3 2 17.44 3.13 5.0840 -2 0 2 2 17.89 4.89 4.9594 -2 -1 2 2 17.93 3.24 4.9472 1 -2 2 2 18.43 7.00 4.8138 2 1 1 2 18.98 1.90 4.6761 1 0 3 2 19.10 1.83 4.6459 0 -2 3 2 19.22 3.31 4.6187 0 1 3 2 19.69 5.03 4.5097 2 0 2 2 20.05 2.39 4.4295 2 -1 2 2 20.20 5.30 4.3957 0 -3 1 2 20.28 1.73 4.3797 -1 2 2 2 20.33 2.66 4.3690 -2 2 0 2 20.66 4.75 4.2996 0 3 0 2 20.78 1.29 4.2744 2 -2 1 2 21.27 1.95 4.1774 1 -2 3 2 21.31 6.33 4.1687 1 2 2 2 21.34 1.35 4.1629 -1 -3 1 2 21.66 6.12 4.1032 0 -1 4 2 22.02 5.90 4.0372 1 3 0 2 22.09 2.26 4.0239 -1 -3 2 2 22.37 1.99 3.9735 2 2 1 2 22.41 2.22 3.9674 -1 0 4 2 22.52 1.05 3.9486 0 3 1 2 23.05 3.59 3.8587 -2 -2 3 2 23.10 1.56 3.8505 -2 1 3 2 23.22 6.60 3.8301 -3 -1 1 2 23.40 1.28 3.8022 0 -2 4 2 23.59 1.89 3.7713 3 1 0 2 23.68 1.07 3.7578 -2 2 2 2 23.72 1.16 3.7515 2 0 3 2 23.73 4.81 3.7491 -1 -2 4 2 23.87 1.03 3.7280 3 0 1 2 24.00 2.08 3.7086 1 3 1 2 24.13 1.18 3.6881 -1 -3 3 2 24.21 1.77 3.6758 1 0 4 2 24.50 3.32 3.6329 3 -1 1 2 25.37 6.64 3.5110 1 -3 3 2 25.42 3.18 3.5038 1 -2 4 2 25.49 2.97 3.4945 0 3 2 2 25.61 2.01 3.4787 2 -3 1 2 25.72 2.23 3.4639 2 1 3 2 25.86 5.23 3.4449 -3 -2 1 2 26.17 2.14 3.4047 -1 3 2 2 26.29 1.25 3.3903 -3 -1 3 2 26.29 2.59 3.3893 -3 0 3 2 26.35 8.94 3.3818 3 0 2 2 26.51 1.50 3.3620 3 2 0 2 26.62 1.19 3.3484 3 -1 2 2 26.98 9.96 3.3043 -2 2 3 2 26.99 3.25 3.3040 3 -2 1 2 27.05 3.19 3.2968 0 -1 5 2 27.14 1.11 3.2857 -1 -1 5 2 27.50 2.34 3.2433 0 -4 2 2 27.68 5.81 3.2222 0 0 5 2 27.90 8.08 3.1984 -1 -4 1 2 27.98 1.13 3.1893 2 -1 4 2 28.07 3.56 3.1787 -3 -2 3 2 28.18 1.32 3.1668 0 -2 5 2 28.22 5.59 3.1618 1 -4 1 2 28.28 5.42 3.1563 -1 -2 5 2 28.31 4.61 3.1522 2 0 4 2 28.53 3.16 3.1281 0 2 4 2 28.64 1.10 3.1164 3 -2 2 2 28.76 9.17 3.1045 -3 2 2 2 28.88 1.13 3.0914 1 -4 2 2 28.92 1.94 3.0874 -2 3 2 2 29.02 1.22 3.0767 1 -1 5 2 29.08 1.47 3.0705 0 -4 3 2 29.26 2.05 3.0522 0 3 3 2 29.30 6.81 3.0478 2 2 3 2 29.35 2.57 3.0433 -3 -1 4 2 29.39 1.71 3.0390 0 4 1 2 29.53 1.40 3.0253 -2 -3 4 2 29.64 4.13 3.0139 -3 0 4 2 29.69 1.15 3.0095 -1 3 3 2 29.87 2.32 2.9916 -2 0 5 2 29.99 1.40 2.9795 0 1 5 2 30.00 2.12 2.9789 -4 0 1 2 30.16 2.00 2.9628 -1 4 1 2 30.19 6.63 2.9607 4 0 0 2 30.26 4.72 2.9533 1 2 4 2 30.35 4.02 2.9449 -2 -2 5 2 30.43 1.45 2.9373 2 3 2 2 30.56 3.68 2.9249 1 4 1 2 30.57 6.40 2.9241 1 -4 3 2 30.70 1.36 2.9126 -3 -2 4 2 30.85 2.16 2.8988 -4 0 2 2 30.98 1.00 2.8868 3 2 2 2 31.00 2.16 2.8849 -1 -3 5 2 31.01 1.04 2.8836 4 1 0 2 31.37 2.07 2.8518 -3 -3 3 2 31.61 2.51 2.8309 0 -4 4 2 31.64 1.51 2.8281 2 4 0 2 31.89 1.02 2.8067 4 -1 1 2 32.03 1.42 2.7941 0 4 2 2 32.12 5.46 2.7868 3 -3 2 2 32.46 3.32 2.7585 4 1 1 2 32.57 5.76 2.7491 0 -1 6 2 32.59 1.15 2.7480 -1 4 2 2 32.61 1.01 2.7459 3 3 1 2 32.66 1.24 2.7418 -4 -1 3 2 32.93 2.99 2.7203 -4 -2 2 2 33.28 2.74 2.6918 1 4 2 2 33.37 1.16 2.6852 0 0 6 2 33.51 2.16 2.6745 -3 -3 4 2 33.53 3.92 2.6729 4 0 2 2 33.67 1.84 2.6616 2 -2 5 2 33.70 2.51 2.6596 2 2 4 2 33.79 2.62 2.6527 2 -4 3 2 34.15 1.37 2.6259 0 -5 2 2 34.15 4.32 2.6258 -4 -2 3 2 34.15 1.15 2.6256 -4 1 3 2 34.23 2.42 2.6193 3 -3 3 2 34.60 2.36 2.5924 3 -2 4 2 34.79 7.87 2.5787 -3 2 4 2 34.92 2.38 2.5692 -2 0 6 2 35.04 3.94 2.5606 -3 -4 1 2 35.06 2.82 2.5592 -4 -1 4 2 35.18 1.51 2.5508 1 0 6 2 35.22 2.16 2.5485 0 -5 3 2 35.29 1.96 2.5436 1 -5 2 2 35.39 1.06 2.5367 4 -2 2 2 35.41 2.00 2.5350 0 4 3 2 35.48 1.91 2.5299 -2 2 5 2 35.59 1.27 2.5224 -1 5 0 2 35.64 2.74 2.5189 1 5 0 2 35.72 2.49 2.5135 -2 3 4 2 35.84 3.86 2.5052 -3 3 3 2 35.90 2.21 2.5014 -3 4 0 2 37.37 1.16 2.4062 -1 -5 4 2 37.41 1.14 2.4036 1 5 1 2 37.69 1.15 2.3867 -5 0 1 2 38.20 1.30 2.3561 3 0 5 2 38.22 1.24 2.3548 0 -1 7 2 38.54 1.28 2.3359 3 -2 5 2 39.00 2.00 2.3094 0 2 6 2 39.34 1.45 2.2905 -2 -1 7 2 39.73 1.75 2.2688 -2 -2 7 2 39.83 1.72 2.2635 1 3 5 2 40.08 1.05 2.2495 -1 -3 7 2 40.53 1.32 2.2258 -5 2 0 2 40.54 1.01 2.2251 -3 -5 2 2 42.93 1.92 2.1069 -1 -4 7 2 43.65 1.05 2.0734 0 6 1 2 45.01 1.61 2.0139 0 0 8 2 45.64 1.01 1.9877 4 1 5 2 46.70 1.75 1.9451 -3 -4 7 2 46.82 2.29 1.9404 3 3 5 2 47.07 1.60 1.9307 -3 -5 6 2 47.76 2.11 1.9045 5 -4 1 2 47.79 1.66 1.9032 4 3 4 2 47.85 4.11 1.9010 6 1 1 2 48.13 1.08 1.8906 -3 6 0 2 48.86 1.15 1.8640 6 0 2 2 49.81 2.25 1.8308 0 -7 4 2 51.02 1.96 1.7901 0 0 9 2 51.21 1.49 1.7838 0 -5 8 2 51.50 2.34 1.7744 -6 -2 5 2 51.56 1.21 1.7724 3 -4 7 2 52.28 1.61 1.7499 4 4 4 2 52.50 1.35 1.7429 -1 6 4 2 52.52 1.28 1.7423 -1 -4 9 2 52.86 1.76 1.7320 4 2 6 2 53.15 1.46 1.7232 2 -7 4 2 53.33 1.06 1.7180 0 7 2 2 54.07 1.70 1.6960 -3 -5 8 2 54.49 1.13 1.6839 1 -4 9 2 55.07 1.03 1.6676 2 -7 5 2 55.52 1.04 1.6552 -1 -5 9 2 56.11 1.16 1.6393 -3 7 1 2 56.42 1.01 1.6309 4 3 6 2 56.60 1.56 1.6262 -7 2 2 2 58.51 1.03 1.5776 -3 2 9 2 58.57 1.48 1.5761 4 0 8 2 60.96 1.28 1.5198 3 -4 9 2 62.64 1.12 1.4831 7 -2 4 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.