Grumiplucite Mumme W G, Watts J A Acta Crystallographica B36 (1980) 1300-1304 HgBi2S4: Crystal structure and relationship with the pavonite homologous series Locality: synthetic _database_code_amcsd 0009710 CELL PARAMETERS: 14.1700 4.0600 13.9900 90.000 118.270 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 708.850 Density (g/cm3): 6.997 MAX. ABS. INTENSITY / VOLUME**2: 100.0607640 RIR: 4.656 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.19 5.01 6.2399 2 0 0 2 14.38 27.55 6.1607 0 0 2 2 14.66 1.78 6.0424 -2 0 2 2 18.74 25.43 4.7357 2 0 1 2 19.45 14.64 4.5642 -2 0 3 2 23.04 11.88 3.8608 1 1 0 4 23.11 16.42 3.8486 -1 1 1 4 24.65 62.01 3.6115 2 0 2 2 25.16 42.61 3.5400 -4 0 2 2 25.16 58.65 3.5392 1 1 1 4 25.37 11.84 3.5112 -1 1 2 4 25.47 67.93 3.4966 -2 0 4 2 25.93 6.37 3.4365 -4 0 1 2 26.45 8.89 3.3693 -4 0 3 2 28.61 6.79 3.1200 4 0 0 2 28.99 11.92 3.0803 0 0 4 2 29.04 13.55 3.0750 1 1 2 4 29.15 6.82 3.0634 -3 1 1 4 29.33 100.00 3.0452 -3 1 2 4 29.34 30.84 3.0445 -1 1 3 4 29.57 2.80 3.0212 -4 0 4 2 30.77 47.50 2.9056 3 1 0 4 31.23 4.16 2.8639 2 0 3 2 31.28 53.25 2.8596 -3 1 3 4 32.12 4.12 2.7869 -2 0 5 2 32.78 4.91 2.7322 4 0 1 2 33.96 29.41 2.6396 3 1 1 4 34.04 1.62 2.6334 -4 0 5 2 34.48 12.41 2.6008 -1 1 4 4 34.73 1.00 2.5827 -3 1 4 4 38.22 15.75 2.3547 2 0 4 2 38.57 2.13 2.3340 -6 0 2 2 38.83 10.02 2.3191 -5 1 2 4 39.06 1.35 2.3060 -5 1 3 4 39.13 3.37 2.3021 -6 0 4 2 39.15 14.15 2.3009 -2 0 6 2 40.01 3.12 2.2532 -5 1 1 4 40.03 16.81 2.2523 1 1 4 4 40.42 15.64 2.2318 -6 0 1 2 40.44 14.23 2.2307 -1 1 5 4 40.69 3.61 2.2175 -5 1 4 4 41.48 12.40 2.1770 -6 0 5 2 42.52 19.00 2.1263 5 1 0 4 43.51 6.61 2.0800 6 0 0 2 43.58 4.91 2.0768 -5 1 5 4 43.71 5.46 2.0709 3 1 3 4 43.98 4.69 2.0587 4 0 3 2 44.10 7.71 2.0536 0 0 6 2 44.64 32.34 2.0300 0 2 0 2 45.01 7.22 2.0141 -6 0 6 2 45.53 3.21 1.9922 2 0 5 2 45.63 4.79 1.9881 -4 0 7 2 46.16 1.62 1.9666 5 1 1 4 46.50 1.04 1.9529 -2 0 7 2 46.54 18.15 1.9516 1 1 5 4 46.97 7.34 1.9344 -1 1 6 4 47.14 2.17 1.9280 0 2 2 4 47.55 33.58 1.9121 -5 1 6 4 48.81 3.54 1.8658 2 2 1 4 49.12 2.23 1.8548 -2 2 3 4 49.52 1.38 1.8406 -6 0 7 2 50.55 2.56 1.8057 4 0 4 2 50.68 14.76 1.8013 -7 1 4 4 50.76 22.71 1.7986 5 1 2 4 51.00 9.60 1.7907 -3 1 7 4 51.31 8.63 1.7807 -7 1 2 4 51.65 14.10 1.7696 2 2 2 4 51.91 2.43 1.7613 -8 0 3 2 51.92 10.11 1.7610 -4 2 2 4 52.10 16.28 1.7556 -2 2 4 4 52.33 4.27 1.7483 -4 0 8 2 52.34 1.75 1.7478 -4 2 1 4 52.50 6.77 1.7429 -8 0 5 2 52.64 2.60 1.7388 -4 2 3 4 53.32 1.02 1.7183 -8 0 2 2 53.53 1.93 1.7120 1 1 6 4 53.88 1.87 1.7015 4 2 0 4 53.99 6.01 1.6983 -1 1 7 4 54.11 3.69 1.6950 0 2 4 4 54.47 2.17 1.6846 -8 0 6 2 55.48 1.18 1.6561 2 2 3 4 55.78 3.84 1.6479 -8 0 1 2 56.05 1.28 1.6408 -2 2 5 4 56.36 1.15 1.6324 7 1 0 4 56.38 1.65 1.6318 3 1 5 4 56.47 1.81 1.6295 4 2 1 4 57.61 1.26 1.6000 4 0 5 2 57.73 4.77 1.5968 -3 1 8 4 58.47 3.67 1.5786 6 0 3 2 59.23 2.92 1.5600 8 0 0 2 60.07 4.27 1.5402 0 0 8 2 60.19 6.62 1.5375 2 2 4 4 60.84 1.37 1.5226 -6 2 4 4 60.85 6.22 1.5222 -2 2 6 4 60.89 2.00 1.5214 -6 0 9 2 61.37 1.25 1.5106 -8 0 8 2 61.78 7.51 1.5017 -6 2 1 4 62.56 6.07 1.4847 -6 2 5 4 63.54 6.76 1.4642 3 1 6 4 63.57 1.29 1.4637 8 0 1 2 64.10 3.27 1.4528 6 2 0 4 64.46 2.53 1.4455 4 2 3 4 64.55 3.93 1.4437 0 2 6 4 64.96 1.93 1.4356 -9 1 6 4 65.15 3.21 1.4319 4 0 6 2 65.26 3.76 1.4298 -6 2 6 4 65.66 1.78 1.4219 2 2 5 4 65.74 2.72 1.4204 -4 2 7 4 65.78 2.97 1.4196 -9 1 2 4 66.13 2.14 1.4129 -8 0 9 2 66.14 2.21 1.4127 -10 0 4 2 67.18 3.13 1.3934 -4 0 10 2 68.55 1.10 1.3690 -10 0 7 2 69.39 3.35 1.3543 -1 1 9 4 69.69 1.56 1.3492 4 2 4 4 70.38 7.50 1.3378 -9 1 8 4 70.83 1.61 1.3304 -8 2 3 4 70.84 2.40 1.3302 1 3 1 4 71.17 2.70 1.3247 -4 2 8 4 71.23 1.10 1.3239 3 1 7 4 71.32 4.52 1.3224 -8 2 5 4 71.96 5.85 1.3122 9 1 0 4 72.79 1.03 1.2993 -3 1 10 4 72.85 4.72 1.2984 -3 3 2 4 72.85 1.66 1.2984 -1 3 3 4 72.98 1.44 1.2964 -8 2 6 4 73.19 1.43 1.2932 4 0 7 2 73.53 6.59 1.2880 -7 1 10 4 73.60 2.56 1.2869 3 3 0 4 73.87 3.05 1.2829 -3 3 3 4 74.11 2.73 1.2794 -8 2 1 4 75.36 1.22 1.2612 -4 0 11 2 75.37 2.00 1.2610 3 3 1 4 76.43 2.82 1.2461 6 2 3 4 77.08 7.11 1.2373 7 1 4 4 77.11 2.19 1.2369 8 2 0 4 77.28 3.43 1.2346 1 1 9 4 77.85 3.23 1.2270 0 2 8 4 78.12 2.42 1.2234 -11 1 6 4 78.38 2.02 1.2200 -11 1 4 4 78.58 1.58 1.2174 -6 2 9 4 79.12 1.44 1.2105 1 3 4 4 79.36 2.79 1.2074 -11 1 7 4 79.38 1.38 1.2071 -1 3 5 4 79.89 2.93 1.2008 -11 1 3 4 80.78 1.90 1.1897 5 3 0 4 80.98 1.08 1.1872 8 2 1 4 81.17 1.28 1.1850 -3 1 11 4 82.42 2.75 1.1701 4 2 6 4 83.33 1.91 1.1597 -8 2 9 4 83.63 2.41 1.1563 1 3 5 4 84.30 2.76 1.1488 -4 2 10 4 84.37 4.32 1.1480 -5 3 6 4 86.33 1.43 1.1270 1 1 10 4 86.61 1.39 1.1239 10 0 2 2 86.74 1.05 1.1226 -7 -3 4 4 86.81 3.28 1.1219 5 3 2 4 86.99 1.51 1.1200 -3 3 7 4 87.70 1.52 1.1128 2 0 10 2 89.37 1.03 1.0963 -1 3 7 4 89.96 1.45 1.0907 4 2 7 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.