Arrojadite-(KFe) Merlino S, Mellini M, Zanazzi P F Acta Crystallographica B37 (1981) 1733-1736 Structure of arrojadite, KNa4CaMn4Fe10Al(PO4)12(OH,F)2 Locality: Nickel Plate mine, Keystone, South Dakota, USA _database_code_amcsd 0009747 CELL PARAMETERS: 16.5260 10.0570 24.7300 90.000 105.780 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 3955.275 Density (g/cm3): 3.558 MAX. ABS. INTENSITY / VOLUME**2: 10.41416006 RIR: 0.953 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.43 12.93 11.8990 0 0 2 2 10.41 1.73 8.5000 1 1 0 4 11.13 6.80 7.9516 2 0 0 2 11.58 21.34 7.6404 -2 0 2 2 13.65 7.20 6.4850 1 1 2 4 14.89 11.19 5.9495 0 0 4 2 14.99 21.94 5.9103 2 0 2 2 15.99 27.12 5.5410 -2 0 4 2 16.90 4.00 5.2455 -1 1 4 4 17.64 19.21 5.0285 0 2 0 2 18.59 4.26 4.7720 -3 1 2 4 18.92 4.84 4.6895 3 1 0 4 19.16 4.74 4.6319 0 2 2 4 19.42 9.82 4.5719 1 1 4 4 19.54 1.16 4.5440 -3 1 3 4 20.92 1.74 4.2471 0 2 3 4 21.15 1.12 4.2004 -2 2 2 4 21.55 6.91 4.1229 -4 0 2 2 21.77 1.97 4.0824 2 2 1 4 22.36 1.70 3.9758 4 0 0 2 23.16 1.17 3.8405 0 2 4 4 23.33 1.14 3.8129 -1 1 6 4 23.90 1.57 3.7237 -2 2 4 4 25.69 3.33 3.4675 -3 1 6 4 25.77 2.64 3.4567 0 2 5 4 26.00 1.80 3.4272 -2 2 5 4 26.14 17.63 3.4094 1 1 6 4 26.89 8.13 3.3155 3 1 4 4 27.10 1.32 3.2909 -4 0 6 2 27.19 4.31 3.2802 1 3 0 4 27.51 2.69 3.2425 2 2 4 4 27.66 3.33 3.2251 1 3 1 4 27.73 31.68 3.2170 2 0 6 2 27.80 12.00 3.2087 -1 3 2 4 28.46 1.27 3.1360 -2 2 6 4 28.48 4.54 3.1340 -3 1 7 4 28.62 2.00 3.1187 4 2 0 4 28.63 2.76 3.1178 1 3 2 4 28.69 2.04 3.1111 -5 1 1 4 29.36 100.00 3.0419 -4 2 4 4 29.39 7.23 3.0395 -5 1 4 4 30.04 2.46 2.9748 0 0 8 2 30.06 1.01 2.9730 1 3 3 4 30.36 3.98 2.9444 -1 1 8 4 30.57 2.60 2.9241 -5 1 5 4 30.74 1.03 2.9085 -4 2 5 4 31.16 2.37 2.8704 4 2 2 4 31.37 23.79 2.8512 -3 3 2 4 31.50 7.70 2.8400 -3 1 8 4 31.58 9.98 2.8333 3 3 0 4 31.77 3.07 2.8164 0 2 7 4 31.88 10.20 2.8068 1 3 4 4 32.17 15.94 2.7822 -5 1 6 4 32.31 16.76 2.7705 -4 0 8 2 32.36 2.71 2.7666 3 3 1 4 32.52 1.99 2.7536 -4 2 6 4 32.55 17.91 2.7507 -6 0 2 2 32.90 2.88 2.7226 3 1 6 4 32.98 3.07 2.7159 -3 3 4 4 33.06 75.02 2.7099 2 2 6 4 33.56 3.81 2.6702 3 3 2 4 34.19 1.22 2.6227 -2 2 8 4 34.49 7.99 2.6004 -1 3 6 4 35.05 11.34 2.5603 0 2 8 4 35.23 23.36 2.5478 4 2 4 4 35.24 5.12 2.5468 -6 0 6 2 35.71 17.66 2.5143 0 4 0 2 36.34 2.28 2.4720 -2 0 10 2 36.58 2.88 2.4564 5 1 4 4 37.05 14.47 2.4266 -4 2 8 4 37.07 1.95 2.4249 3 3 4 4 37.26 12.41 2.4133 -6 2 2 4 37.66 2.02 2.3883 -2 4 2 4 37.70 5.55 2.3860 -6 2 4 4 37.74 1.85 2.3834 -1 1 10 4 38.50 2.28 2.3381 -6 2 5 4 38.89 3.32 2.3159 0 4 4 4 39.04 3.22 2.3074 5 3 0 4 39.20 1.80 2.2981 -7 1 3 4 39.22 1.53 2.2971 1 3 7 4 39.42 1.23 2.2860 2 2 8 4 39.59 1.57 2.2764 3 1 8 4 39.75 2.36 2.2678 -1 3 8 4 39.92 4.25 2.2585 -5 3 5 4 40.58 3.28 2.2231 0 4 5 4 40.67 1.54 2.2184 -2 2 10 4 40.72 1.52 2.2160 7 1 0 4 41.05 8.93 2.1988 -7 1 6 4 41.17 1.57 2.1924 -6 2 7 4 42.00 2.98 2.1511 0 2 10 4 42.09 1.60 2.1466 -4 4 2 4 42.51 2.63 2.1266 2 0 10 2 42.57 2.04 2.1235 0 4 6 4 42.62 1.91 2.1212 4 0 8 2 42.76 1.83 2.1145 6 2 3 4 42.80 2.40 2.1126 -5 3 7 4 43.07 3.75 2.1002 -4 4 4 4 43.92 2.34 2.0615 -8 0 4 2 44.00 1.19 2.0578 -7 1 8 4 44.83 1.38 2.0218 6 2 4 4 45.12 1.05 2.0095 -8 0 6 2 45.43 1.59 1.9966 -1 1 12 4 45.48 1.12 1.9942 -1 5 1 4 45.64 3.75 1.9879 8 0 0 2 45.83 1.16 1.9798 -1 3 10 4 45.85 4.95 1.9791 -1 5 2 4 46.11 1.45 1.9686 -3 3 10 4 46.36 5.06 1.9586 2 2 10 4 46.46 4.37 1.9544 4 2 8 4 46.67 2.35 1.9462 -2 4 8 4 47.20 1.11 1.9257 -7 3 2 4 47.34 2.80 1.9202 0 4 8 4 47.42 3.53 1.9172 3 3 8 4 47.43 1.15 1.9170 7 1 4 4 47.44 1.72 1.9166 -6 2 10 4 47.48 3.23 1.9150 4 4 4 4 47.61 6.86 1.9101 -8 0 8 2 47.64 1.08 1.9089 -7 3 1 4 48.26 1.07 1.8858 -3 5 2 4 48.40 2.48 1.8807 7 3 0 4 48.80 1.81 1.8660 -8 2 6 4 48.92 2.74 1.8619 -4 4 8 4 49.09 2.74 1.8558 -6 4 2 4 49.13 2.10 1.8544 -3 3 11 4 49.70 1.54 1.8343 6 2 6 4 50.83 3.05 1.7963 7 3 2 4 51.16 2.28 1.7856 -8 2 8 4 51.25 2.83 1.7827 -8 0 10 2 51.37 1.55 1.7786 -9 1 6 4 51.67 1.45 1.7691 4 4 6 4 51.75 1.30 1.7665 -3 5 6 4 51.85 5.93 1.7632 -2 0 14 2 51.87 9.21 1.7627 -2 4 10 4 52.00 1.44 1.7587 1 5 6 4 52.13 9.17 1.7545 6 4 2 4 52.32 3.01 1.7485 -3 3 12 4 52.34 2.01 1.7480 8 0 4 2 52.36 1.06 1.7473 7 1 6 4 52.59 1.09 1.7404 9 1 0 4 52.80 2.64 1.7337 -6 2 12 4 53.47 3.36 1.7136 -4 4 10 4 53.93 3.03 1.7000 5 5 0 4 54.49 7.31 1.6840 -1 5 8 4 54.62 1.77 1.6802 -5 1 14 4 54.76 2.03 1.6763 -5 3 12 4 54.96 1.02 1.6706 5 3 8 4 55.20 5.76 1.6639 -2 2 14 4 55.21 3.23 1.6637 -3 5 8 4 55.35 3.77 1.6598 0 6 2 4 55.47 3.52 1.6565 1 3 12 4 55.64 2.35 1.6519 -5 5 6 4 55.67 8.47 1.6511 8 2 4 4 55.72 2.34 1.6497 5 5 2 4 55.74 1.06 1.6491 -6 0 14 2 55.88 1.69 1.6454 -8 0 12 2 56.08 1.17 1.6398 -4 4 11 4 56.15 1.43 1.6379 -10 0 6 2 56.18 1.30 1.6372 -2 6 2 4 56.39 2.52 1.6316 1 5 8 4 56.54 1.02 1.6278 -9 1 10 4 56.59 1.03 1.6263 -3 1 15 4 56.75 1.29 1.6221 1 1 14 4 57.22 1.05 1.6100 -9 3 4 4 57.28 7.50 1.6085 4 0 12 2 57.84 1.60 1.5943 -10 0 8 2 57.84 2.19 1.5941 -8 4 4 4 57.99 1.00 1.5903 10 0 0 2 58.60 1.68 1.5752 5 5 4 4 58.77 4.83 1.5711 6 0 10 2 59.07 2.91 1.5638 -8 2 12 4 59.26 2.01 1.5594 8 4 0 4 59.28 1.54 1.5589 2 6 4 4 59.34 3.42 1.5574 -10 2 6 4 60.30 2.86 1.5349 -4 6 4 4 60.42 2.85 1.5320 4 2 12 4 60.60 1.03 1.5281 -10 0 10 2 60.65 1.42 1.5269 -7 5 4 4 60.83 1.70 1.5229 10 0 2 2 61.34 1.89 1.5114 4 6 2 4 61.61 2.03 1.5053 8 4 2 4 61.68 1.50 1.5038 9 3 2 4 62.34 2.46 1.4895 -5 5 10 4 62.48 3.35 1.4865 2 6 6 4 62.49 1.45 1.4863 5 5 6 4 62.78 1.23 1.4801 -9 3 10 4 63.08 1.39 1.4737 -9 1 13 4 63.16 1.16 1.4722 -2 2 16 4 63.37 1.92 1.4678 -11 1 7 4 63.73 1.25 1.4603 0 6 8 4 63.84 1.33 1.4580 4 6 4 4 63.87 1.79 1.4575 10 2 2 4 64.40 1.31 1.4468 -8 2 14 4 64.56 2.66 1.4436 -2 4 14 4 65.03 1.63 1.4341 -4 6 8 4 65.31 1.49 1.4288 4 0 14 2 65.44 3.46 1.4263 0 2 16 4 65.47 3.64 1.4256 -6 6 4 4 65.89 4.61 1.4176 8 2 8 4 66.68 1.06 1.4026 -9 3 12 4 67.44 1.35 1.3888 -3 7 2 4 68.98 1.35 1.3614 -9 3 13 4 69.25 1.26 1.3567 -11 3 7 4 69.36 3.71 1.3549 4 4 12 4 69.50 1.17 1.3525 9 1 8 4 69.86 1.57 1.3464 -10 4 8 4 70.41 2.02 1.3372 -6 0 18 2 70.46 1.18 1.3364 7 3 10 4 70.47 1.44 1.3362 -1 1 18 4 70.71 1.65 1.3324 6 4 10 4 71.04 1.20 1.3269 1 3 16 4 71.14 2.58 1.3253 12 0 0 2 71.49 1.10 1.3196 -9 3 14 4 72.24 1.14 1.3077 10 2 6 4 73.25 1.58 1.2923 -6 2 18 4 76.85 2.00 1.2404 -7 1 19 4 77.64 1.11 1.2298 -13 1 1 4 80.47 1.04 1.1935 0 6 14 4 83.48 1.36 1.1579 0 2 20 4 85.91 1.16 1.1314 -9 7 4 4 86.78 1.17 1.1222 4 8 6 4 88.22 1.66 1.1076 -4 8 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.