As2(SO4)3 Douglade J, Mercier R Acta Crystallographica B38 (1982) 720-723 Structure cristalline et covalence des liaisons dans le sulfate d'arsenic(III), As2(SO4)3 Note: anisoB's from ICSD _database_code_amcsd 0009755 CELL PARAMETERS: 9.3890 5.2550 19.3550 90.000 91.880 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 954.446 Density (g/cm3): 3.048 MAX. ABS. INTENSITY / VOLUME**2: 13.91799900 RIR: 1.487 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.93 4.55 6.8483 -1 0 2 2 17.49 1.45 5.0712 0 1 1 4 18.35 76.38 4.8361 0 0 4 2 18.91 3.00 4.6920 2 0 0 2 19.22 16.91 4.6175 0 1 2 4 19.36 100.00 4.5850 1 1 0 4 19.97 19.60 4.4455 1 1 1 4 20.38 2.96 4.3574 -1 0 4 2 20.77 26.17 4.2770 -2 0 2 2 20.94 7.08 4.2425 1 0 4 2 21.31 54.43 4.1690 -1 1 2 4 21.58 20.18 4.1176 1 1 2 4 21.82 57.21 4.0736 0 1 3 4 25.02 15.91 3.5585 0 1 4 4 25.45 6.21 3.4999 2 1 0 4 25.76 19.88 3.4589 -2 1 1 4 26.02 21.10 3.4242 -2 0 4 2 26.57 21.28 3.3543 -1 1 4 4 26.88 5.98 3.3172 -2 1 2 4 27.01 23.65 3.3010 1 1 4 4 27.67 11.40 3.2241 0 0 6 2 28.54 11.73 3.1280 3 0 0 2 28.99 3.98 3.0804 -1 0 6 2 29.33 5.19 3.0449 2 1 3 4 29.59 1.45 3.0189 1 0 6 2 30.32 2.60 2.9480 3 0 2 2 30.47 5.36 2.9338 1 1 5 4 31.18 2.62 2.8689 -2 1 4 4 31.93 1.44 2.8029 2 1 4 4 33.19 6.67 2.6989 -2 0 6 2 33.33 29.31 2.6879 3 1 0 4 33.53 2.10 2.6726 -3 1 1 4 33.61 2.21 2.6667 -3 0 4 2 33.73 3.87 2.6575 -1 1 6 4 34.12 2.66 2.6275 0 2 0 2 34.26 10.11 2.6177 1 1 6 4 34.26 23.39 2.6174 2 0 6 2 34.38 15.00 2.6088 -3 1 2 4 34.66 3.37 2.5880 3 0 4 2 34.90 16.48 2.5711 3 1 2 4 34.99 6.72 2.5645 2 1 5 4 35.75 5.46 2.5117 -1 2 1 4 37.18 15.10 2.4181 0 0 8 2 37.46 1.01 2.4008 -2 1 6 4 37.74 1.17 2.3838 -1 1 7 4 37.83 8.01 2.3780 -3 1 4 4 38.13 2.08 2.3604 -1 0 8 2 38.30 1.28 2.3502 1 1 7 4 38.37 12.01 2.3460 4 0 0 2 38.42 2.11 2.3429 2 1 6 4 38.79 16.33 2.3217 3 1 4 4 39.01 6.08 2.3088 0 2 4 4 39.22 1.81 2.2972 -4 0 2 2 39.51 2.79 2.2809 -2 2 1 4 39.66 3.61 2.2723 2 2 1 4 40.28 17.90 2.2388 -2 2 2 4 40.31 1.76 2.2372 -3 1 5 4 40.38 1.00 2.2338 1 2 4 4 40.59 18.28 2.2227 2 2 2 4 41.44 1.46 2.1787 -2 0 8 2 41.60 1.00 2.1711 -2 2 3 4 41.96 13.01 2.1531 -1 1 8 4 42.04 10.08 2.1492 2 2 3 4 42.26 6.87 2.1385 -4 0 4 2 42.31 1.31 2.1362 -4 1 1 4 42.55 5.69 2.1248 1 1 8 4 43.21 4.03 2.0938 -3 1 6 4 43.42 2.80 2.0841 4 0 4 2 44.99 1.19 2.0150 4 1 3 4 45.06 1.25 2.0119 3 2 0 4 45.37 1.89 1.9990 -1 2 6 4 45.42 1.31 1.9968 3 2 1 4 46.46 2.60 1.9545 -3 1 7 4 47.76 7.41 1.9042 0 2 7 4 47.87 2.31 1.9002 3 1 7 4 47.92 2.29 1.8984 -4 1 5 4 48.35 5.93 1.8826 -2 2 6 4 49.13 1.34 1.8544 2 2 6 4 49.23 1.68 1.8508 4 1 5 4 49.79 1.52 1.8312 5 0 2 2 50.02 2.90 1.8234 -3 1 8 4 50.43 5.56 1.8095 -2 0 10 2 51.35 3.27 1.7793 0 2 8 4 51.38 3.32 1.7785 -2 2 7 4 51.55 6.87 1.7730 3 1 8 4 51.57 9.16 1.7722 1 1 10 4 51.65 1.14 1.7698 3 2 5 4 51.70 3.95 1.7681 2 0 10 2 51.72 3.27 1.7675 5 1 0 4 51.80 1.06 1.7651 -5 1 1 4 52.25 1.40 1.7507 2 2 7 4 52.28 10.19 1.7500 4 2 0 4 52.33 4.77 1.7482 -5 1 2 4 53.14 3.15 1.7236 0 3 2 4 53.45 1.41 1.7142 1 3 1 4 54.16 2.88 1.6935 1 3 2 4 54.23 1.47 1.6913 5 1 3 4 54.74 1.28 1.6768 -5 1 4 4 54.99 2.21 1.6699 -3 0 10 2 55.12 3.80 1.6661 -1 3 3 4 55.40 6.04 1.6586 -4 2 4 4 55.46 1.28 1.6568 4 0 8 2 55.82 2.32 1.6470 0 3 4 4 55.94 1.39 1.6438 5 1 4 4 55.96 1.09 1.6431 -3 2 7 4 56.20 1.10 1.6367 -2 3 1 4 56.35 4.78 1.6328 4 2 4 4 56.63 1.48 1.6253 -1 3 4 4 56.87 2.45 1.6191 1 3 4 4 57.14 3.15 1.6120 0 0 12 2 57.64 1.40 1.5993 5 0 6 2 57.95 5.38 1.5915 -3 1 10 4 58.04 1.44 1.5892 5 1 5 4 58.80 1.24 1.5704 -5 1 6 4 59.57 2.01 1.5520 -6 0 2 2 60.11 1.41 1.5392 0 3 6 4 60.25 2.43 1.5360 6 0 2 2 60.58 1.64 1.5285 -1 1 12 4 61.25 1.04 1.5134 -3 3 2 4 61.26 1.72 1.5132 1 1 12 4 61.59 1.70 1.5059 3 3 2 4 62.30 3.25 1.4903 -2 2 10 4 62.70 1.86 1.4818 3 3 3 4 63.41 2.86 1.4669 2 2 10 4 63.48 2.27 1.4654 -1 3 7 4 63.55 1.28 1.4641 -3 3 4 4 63.63 1.16 1.4624 4 2 7 4 64.32 2.69 1.4484 -5 1 8 4 65.02 1.97 1.4344 -4 2 8 4 65.28 1.14 1.4293 -3 3 5 4 65.47 2.04 1.4257 -6 0 6 2 66.48 1.48 1.4064 5 1 8 4 66.75 5.71 1.4015 4 2 8 4 66.82 1.18 1.4000 -3 1 12 4 67.39 2.03 1.3897 -3 3 6 4 67.40 1.18 1.3894 6 0 6 2 68.26 2.87 1.3741 0 2 12 4 68.28 1.61 1.3736 -4 2 9 4 68.74 2.06 1.3656 3 1 12 4 70.40 2.05 1.3374 -2 0 14 2 70.47 2.27 1.3363 -6 2 2 4 70.95 1.45 1.3284 3 3 7 4 71.09 1.61 1.3261 6 2 2 4 71.65 3.29 1.3172 1 1 14 4 71.86 1.22 1.3138 2 0 14 2 72.05 1.41 1.3107 0 4 1 4 72.18 1.86 1.3087 4 0 12 2 72.81 1.26 1.2990 7 1 0 4 73.21 3.31 1.2928 -7 1 2 4 73.55 1.18 1.2877 -1 2 13 4 73.72 2.75 1.2852 5 1 10 4 73.89 1.05 1.2827 3 3 8 4 73.91 1.38 1.2824 1 3 10 4 73.93 1.79 1.2820 7 1 2 4 74.03 1.46 1.2806 5 3 0 4 74.35 1.17 1.2759 5 3 1 4 75.04 1.34 1.2658 5 3 2 4 75.12 1.31 1.2646 -7 1 4 4 75.73 1.17 1.2559 -4 2 11 4 75.74 1.24 1.2558 -2 4 2 4 75.94 1.69 1.2531 -6 2 6 4 75.94 1.47 1.2530 2 4 2 4 76.54 2.24 1.2446 7 1 4 4 76.63 1.16 1.2435 -2 4 3 4 76.65 2.92 1.2432 -3 1 14 4 77.16 2.74 1.2362 -6 0 10 2 77.26 1.08 1.2349 -1 4 5 4 77.32 1.06 1.2341 -1 3 11 4 79.26 1.18 1.2087 -3 3 10 4 79.92 2.21 1.2004 -4 2 12 4 80.00 1.34 1.1993 2 4 5 4 80.60 1.20 1.1919 -2 2 14 4 80.76 1.02 1.1900 3 3 10 4 81.49 1.96 1.1811 5 3 6 4 81.55 1.76 1.1804 -1 3 12 4 82.18 1.05 1.1730 8 0 0 2 82.27 1.17 1.1719 -5 3 7 4 82.31 1.07 1.1715 4 2 12 4 84.32 1.75 1.1486 -8 0 4 2 86.09 1.66 1.1294 7 1 8 4 89.54 1.36 1.0946 -7 1 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.