Probertite Menchetti S, Sabelli C, Trosti-Ferroni R Acta Crystallographica B38 (1982) 3072-3075 Probertite, CaNa[B5O7(OH)4]*3H2O: a refinement _database_code_amcsd 0009784 CELL PARAMETERS: 6.5880 12.5600 13.4280 90.000 99.970 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1094.324 Density (g/cm3): 2.131 MAX. ABS. INTENSITY / VOLUME**2: 7.053957068 RIR: 1.078 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.71 100.00 9.1074 0 1 1 4 13.39 14.39 6.6126 0 0 2 2 13.65 4.12 6.4885 1 0 0 2 15.14 1.45 5.8512 0 1 2 4 15.37 7.75 5.7647 1 1 0 4 15.62 3.45 5.6729 0 2 1 4 17.41 1.95 5.0931 -1 0 2 2 17.70 6.36 5.0098 1 1 1 4 18.80 8.09 4.7198 -1 1 2 4 19.49 4.29 4.5537 0 2 2 4 19.67 7.20 4.5125 1 2 0 4 20.01 8.95 4.4372 -1 2 1 4 21.36 2.05 4.1596 0 1 3 4 21.96 10.80 4.0478 1 1 2 4 22.27 9.38 3.9914 0 3 1 4 23.44 5.14 3.7948 -1 1 3 4 25.18 4.20 3.5373 0 3 2 4 25.20 3.08 3.5345 1 2 2 4 25.32 8.96 3.5179 1 3 0 4 26.51 1.99 3.3622 -1 2 3 4 26.97 3.80 3.3063 0 0 4 2 27.58 6.79 3.2342 -1 3 2 4 28.09 2.34 3.1768 -1 0 4 2 28.47 3.50 3.1351 -2 0 2 2 28.99 3.44 3.0798 -1 1 4 4 29.23 3.91 3.0551 0 4 1 4 29.36 2.49 3.0418 -2 1 2 4 29.42 2.20 3.0358 0 3 3 4 30.33 5.93 2.9471 2 1 1 4 30.56 13.14 2.9256 0 2 4 4 30.71 5.22 2.9110 -2 2 1 4 31.00 17.66 2.8849 -1 3 3 4 31.54 1.86 2.8365 0 4 2 4 31.56 5.31 2.8347 -1 2 4 4 31.87 10.86 2.8076 -1 4 1 4 31.90 18.40 2.8050 -2 2 2 4 32.10 1.02 2.7886 -2 1 3 4 32.80 5.39 2.7302 2 2 1 4 32.90 1.06 2.7224 1 4 1 4 33.25 3.78 2.6947 1 1 4 4 33.57 3.78 2.6692 2 1 2 4 34.06 6.28 2.6319 1 3 3 4 34.66 6.23 2.5883 0 1 5 4 34.99 1.02 2.5644 2 3 0 4 35.08 4.47 2.5578 -1 1 5 4 35.24 1.17 2.5465 -2 0 4 2 35.47 2.63 2.5307 -1 3 4 4 35.54 6.04 2.5260 1 2 4 4 35.99 1.30 2.4958 -2 1 4 4 36.41 1.68 2.4679 0 5 1 4 36.87 2.63 2.4377 0 2 5 4 37.85 1.84 2.3768 2 1 3 4 38.13 1.88 2.3599 -2 2 4 4 38.33 2.88 2.3483 0 5 2 4 38.61 5.71 2.3318 -1 5 1 4 39.10 1.80 2.3037 1 3 4 4 39.39 2.36 2.2877 2 3 2 4 39.71 2.61 2.2699 -2 4 1 4 39.92 1.86 2.2586 2 2 3 4 40.02 2.20 2.2529 -1 5 2 4 40.33 2.06 2.2362 0 3 5 4 40.39 1.62 2.2332 -1 4 4 4 40.67 2.63 2.2186 -2 4 2 4 40.75 1.07 2.2144 -2 1 5 4 41.51 5.98 2.1757 -2 3 4 4 41.60 2.45 2.1710 0 1 6 4 41.60 1.56 2.1707 1 2 5 4 41.63 2.56 2.1697 -3 0 2 2 41.76 3.42 2.1631 -3 1 1 4 42.27 1.82 2.1380 2 0 4 2 42.27 3.60 2.1380 -3 1 2 4 42.56 2.02 2.1244 -1 5 3 4 42.69 3.98 2.1179 -2 2 5 4 43.22 1.10 2.0933 0 6 0 2 43.47 3.03 2.0819 -1 2 6 4 43.51 2.58 2.0798 0 2 6 4 43.67 2.43 2.0726 1 4 4 4 43.91 2.25 2.0617 -3 1 3 4 44.18 1.89 2.0501 3 1 1 4 44.29 1.15 2.0450 3 2 0 4 44.78 1.56 2.0239 2 2 4 4 44.94 4.61 2.0171 1 5 3 4 45.45 10.17 1.9955 -2 5 1 4 45.53 1.69 1.9922 1 6 0 4 45.58 1.05 1.9904 -2 0 6 2 45.68 3.73 1.9862 2 5 0 4 45.71 4.58 1.9850 1 0 6 2 46.01 2.73 1.9728 3 2 1 4 46.06 1.12 1.9704 -1 5 4 4 46.37 2.95 1.9580 3 0 2 2 46.71 2.62 1.9446 -3 3 1 4 46.93 1.79 1.9362 -1 6 2 4 46.98 1.61 1.9343 2 5 1 4 47.18 1.12 1.9263 -3 3 2 4 47.31 2.37 1.9216 3 3 0 4 47.77 1.34 1.9041 2 3 4 4 48.07 1.24 1.8927 1 2 6 4 48.41 1.18 1.8801 1 6 2 4 48.57 1.00 1.8744 2 1 5 4 48.72 2.14 1.8692 3 2 2 4 48.90 3.11 1.8625 1 4 5 4 49.04 1.08 1.8574 1 5 4 4 49.87 2.97 1.8287 -2 4 5 4 50.08 2.90 1.8215 0 5 5 4 50.18 1.02 1.8181 -3 1 5 4 50.40 3.50 1.8108 -1 5 5 4 50.60 7.01 1.8041 0 4 6 4 50.91 1.69 1.7936 1 3 6 4 51.18 1.14 1.7850 -3 4 2 4 51.29 1.37 1.7812 3 4 0 4 51.39 3.81 1.7780 0 7 1 4 52.14 1.38 1.7541 -2 1 7 4 52.80 1.04 1.7337 -1 3 7 4 54.01 2.24 1.6977 -3 0 6 2 54.58 1.88 1.6815 3 0 4 2 55.54 1.26 1.6545 1 7 2 4 56.75 1.05 1.6221 4 0 0 2 60.69 1.33 1.5260 1 8 0 4 61.05 1.20 1.5177 -1 5 7 4 62.05 1.90 1.4958 2 6 4 4 71.37 1.19 1.3216 -4 2 7 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.