Mo3 O25 P5.8 Rb Si2 Leclaire A, Monier J, Raveau B Acta Crystallographica B40 (1984) 180-185 A molybdosilicophosphate with an intersecting - tunnel structure, which exhibits ion - exchange properties, a Mo3 P5.8 Si2 O25 (A = Rb, Tl) _cod_database_code 1001852 _database_code_amcsd 0009803 CELL PARAMETERS: 8.2905 8.2905 17.4390 90.000 90.000 120.000 SPACE GROUP: P-31c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1038.039 Density (g/cm3): 3.230 MAX. ABS. INTENSITY / VOLUME**2: 23.65485364 RIR: 2.385 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.14 27.86 8.7195 0 0 2 2 12.33 57.37 7.1798 1 0 0 6 13.34 7.77 6.6391 1 0 1 12 15.99 2.78 5.5426 1 0 2 12 19.65 11.83 4.5179 1 0 3 12 21.44 98.38 4.1452 1 1 0 6 23.77 26.73 3.7437 2 -1 2 6 23.77 44.02 3.7437 1 1 2 6 23.88 57.31 3.7265 1 0 4 12 24.80 2.86 3.5899 2 0 0 6 25.33 3.60 3.5162 2 0 1 12 28.45 4.45 3.1372 1 0 5 12 29.24 13.14 3.0544 2 0 3 12 29.74 39.75 3.0041 2 -1 4 6 29.74 60.25 3.0041 1 1 4 6 30.76 4.97 2.9065 0 0 6 2 32.30 32.12 2.7713 2 0 4 12 33.01 2.54 2.7137 2 1 0 12 33.42 7.77 2.6814 2 1 1 12 34.62 3.79 2.5911 3 -1 2 12 35.90 7.31 2.5016 2 0 5 12 36.54 5.31 2.4590 3 -1 3 12 37.58 32.04 2.3933 3 0 0 6 37.80 4.41 2.3798 1 1 6 6 37.95 2.51 2.3710 3 0 1 12 39.10 5.67 2.3039 3 -1 4 12 39.10 5.80 2.3039 2 1 4 12 40.77 5.98 2.2130 3 0 3 12 41.42 4.82 2.1799 0 0 8 2 42.19 1.70 2.1418 2 1 5 12 43.12 12.52 2.0979 3 0 4 12 43.67 8.64 2.0726 2 2 0 6 44.25 5.88 2.0467 2 0 7 12 44.95 1.52 2.0164 2 2 2 6 45.55 3.68 1.9913 3 1 0 12 47.10 1.21 1.9294 1 1 8 6 47.10 8.44 1.9294 2 -1 8 6 48.64 16.44 1.8719 4 -2 4 6 48.64 10.62 1.8719 2 2 4 6 48.67 2.64 1.8707 1 0 9 12 48.88 1.60 1.8633 2 0 8 12 49.32 2.40 1.8475 3 0 6 12 49.68 4.63 1.8352 2 1 7 12 49.68 5.70 1.8352 3 -1 7 12 50.38 4.95 1.8113 4 -1 4 12 50.38 4.37 1.8113 3 1 4 12 50.87 2.13 1.7949 4 0 0 6 51.16 1.09 1.7855 4 0 1 12 52.95 5.94 1.7293 3 1 5 12 53.76 1.93 1.7051 2 0 9 12 53.95 2.75 1.6995 2 1 8 12 53.95 5.44 1.6995 3 -1 8 12 54.37 1.10 1.6875 4 -2 6 6 55.35 1.29 1.6598 4 0 4 12 55.81 1.42 1.6472 3 2 0 12 55.98 1.30 1.6427 3 1 6 12 56.08 1.48 1.6399 5 -2 1 12 57.16 12.09 1.6116 3 0 8 12 57.32 2.24 1.6074 2 -1 10 6 57.77 1.33 1.5960 4 0 5 12 58.22 2.78 1.5848 3 2 3 12 58.53 1.81 1.5769 3 -1 9 12 58.53 2.48 1.5769 2 1 9 12 58.87 3.72 1.5686 2 0 10 12 58.95 18.75 1.5668 4 1 0 12 59.42 4.19 1.5555 4 -1 7 12 59.42 4.55 1.5555 3 1 7 12 59.73 1.69 1.5481 1 0 11 12 60.04 2.51 1.5409 3 2 4 12 60.04 3.70 1.5409 5 -2 4 12 61.76 2.19 1.5021 2 2 8 6 63.05 6.57 1.4744 4 1 4 12 63.05 5.48 1.4744 5 -1 4 12 63.25 1.97 1.4702 3 1 8 12 63.40 1.35 1.4671 2 1 10 12 63.92 3.36 1.4563 4 0 7 12 64.22 2.59 1.4502 2 0 11 12 67.44 1.69 1.3887 4 -1 9 12 67.61 1.30 1.3856 4 0 8 12 67.83 7.41 1.3817 3 3 0 6 68.41 4.08 1.3714 1 1 12 6 68.55 2.40 1.3689 2 1 11 12 68.55 1.77 1.3689 3 -1 11 12 68.79 1.24 1.3647 6 -3 2 6 68.84 2.31 1.3639 5 0 4 12 70.58 1.02 1.3344 2 2 10 6 71.55 1.18 1.3186 1 0 13 12 71.65 1.47 1.3172 3 3 4 6 71.67 1.72 1.3168 4 0 9 12 71.98 1.75 1.3119 3 1 10 12 73.03 1.28 1.2956 6 -2 4 12 73.03 1.84 1.2956 4 2 4 12 74.60 2.48 1.2722 5 -1 8 12 75.52 1.82 1.2589 6 -1 3 12 75.80 1.37 1.2550 5 -2 9 12 76.47 1.62 1.2456 0 0 14 2 76.72 1.04 1.2422 3 0 12 12 77.13 2.73 1.2366 6 -1 4 12 77.13 2.86 1.2366 5 1 4 12 79.19 1.80 1.2095 6 -1 5 12 79.74 1.56 1.2026 3 -1 13 12 80.15 1.43 1.1975 3 2 10 12 80.22 3.60 1.1966 6 0 0 6 80.76 1.14 1.1899 4 -2 12 6 82.69 1.34 1.1670 3 3 8 6 83.84 1.31 1.1540 6 0 4 12 84.22 1.11 1.1497 5 2 0 12 84.40 1.54 1.1477 1 0 15 12 84.90 1.75 1.1422 5 -2 11 12 84.90 1.41 1.1422 3 2 11 12 87.81 1.03 1.1117 -2 -5 4 12 87.83 1.35 1.1114 4 2 9 12 88.49 2.36 1.1049 3 0 14 12 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.