C16H25NO Marsh R E, Herbstein F H Acta Crystallographica B44 (1988) 77-88 More space-group changes _database_code_amcsd 0009818 CELL PARAMETERS: 24.2800 8.7600 14.0300 90.000 108.000 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2838.029 Density (g/cm3): 1.040 MAX. ABS. INTENSITY / VOLUME**2: 1.790777883 RIR: 0.561 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.66 25.42 11.5458 2 0 0 2 10.80 34.80 8.1904 1 1 0 4 12.04 7.58 7.3487 -1 1 1 4 13.12 70.11 6.7505 -2 0 2 2 13.27 17.71 6.6717 0 0 2 2 13.29 60.89 6.6623 1 1 1 4 15.22 67.94 5.8213 -3 1 1 4 15.32 100.00 5.7822 3 1 0 4 15.35 49.68 5.7729 4 0 0 2 16.19 53.77 5.4749 -1 1 2 4 16.92 55.91 5.2396 -4 0 2 2 17.28 29.25 5.1305 2 0 2 2 17.82 95.38 4.9788 -3 1 2 4 18.05 14.97 4.9156 1 1 2 4 18.08 31.41 4.9062 3 1 1 4 20.27 5.93 4.3800 0 2 0 2 21.35 8.49 4.1615 0 2 1 4 21.67 9.09 4.1017 -1 1 3 4 21.70 8.12 4.0952 2 2 0 4 21.75 7.52 4.0853 5 1 0 4 21.99 4.91 4.0412 -2 2 1 4 22.19 43.08 4.0056 -5 1 2 4 22.21 4.70 4.0030 -3 1 3 4 22.57 5.95 3.9402 3 1 2 4 23.11 1.86 3.8486 6 0 0 2 23.41 22.11 3.7999 2 2 1 4 24.31 13.32 3.6615 0 2 2 4 24.47 3.48 3.6379 5 1 1 4 25.14 8.41 3.5416 -4 2 1 4 25.40 5.45 3.5067 -2 0 4 2 25.53 3.26 3.4893 4 2 0 4 27.61 8.93 3.2313 4 2 1 4 27.75 4.71 3.2150 -1 1 4 4 27.95 1.01 3.1921 -2 2 3 4 28.12 1.41 3.1732 -7 1 2 4 28.60 4.58 3.1208 0 2 3 4 28.92 13.35 3.0872 7 1 0 4 29.58 3.23 3.0197 -5 1 4 4 29.68 4.03 3.0097 -8 0 2 2 30.01 1.86 2.9775 1 1 4 4 30.07 1.49 2.9719 -6 2 1 4 30.10 4.88 2.9694 2 0 4 2 30.93 2.09 2.8911 6 2 0 4 31.06 7.00 2.8790 4 2 2 4 31.34 1.78 2.8540 -1 3 1 4 32.71 4.93 2.7375 -2 2 4 4 32.79 3.95 2.7309 -6 2 3 4 32.80 3.39 2.7301 3 3 0 4 33.20 1.74 2.6989 6 2 1 4 33.52 2.90 2.6735 -4 2 4 4 33.78 3.48 2.6538 0 2 4 4 34.00 1.43 2.6367 3 1 4 4 34.09 1.49 2.6298 -3 3 2 4 34.18 4.18 2.6235 -1 1 5 4 34.24 5.08 2.6190 3 3 1 4 36.08 1.35 2.4897 -9 1 3 4 36.08 3.25 2.4894 -6 2 4 4 36.12 1.91 2.4867 -8 2 1 4 36.49 3.06 2.4623 9 1 0 4 36.54 1.44 2.4592 1 1 5 4 36.56 2.14 2.4578 2 2 4 4 36.92 1.83 2.4350 3 3 2 4 37.05 3.92 2.4262 -10 0 2 2 37.31 1.34 2.4102 8 2 0 4 37.58 3.83 2.3935 -8 2 3 4 37.64 2.28 2.3895 -7 1 5 4 37.71 1.11 2.3855 1 3 3 4 38.16 1.60 2.3582 5 3 1 4 38.47 4.15 2.3402 -9 1 4 4 38.80 2.04 2.3210 -2 0 6 2 39.12 2.50 2.3026 9 1 1 4 39.54 2.08 2.2790 0 2 5 4 39.68 1.76 2.2715 8 2 1 4 40.11 1.45 2.2483 -8 2 4 4 40.41 2.07 2.2319 -7 3 1 4 40.44 1.73 2.2305 -1 3 4 4 40.87 1.53 2.2083 -1 1 6 4 41.03 2.03 2.1996 5 3 2 4 42.75 1.78 2.1152 -11 1 1 4 42.92 1.71 2.1071 -10 2 1 4 42.99 1.82 2.1038 -8 0 6 2 44.00 1.29 2.0580 -4 4 1 4 44.66 1.13 2.0291 -7 3 4 4 44.81 2.73 2.0224 -3 3 5 4 45.28 1.39 2.0028 -10 2 4 4 45.76 1.37 1.9829 0 2 6 4 45.99 1.57 1.9735 -9 3 1 4 46.27 2.27 1.9622 7 3 2 4 47.19 2.31 1.9259 -6 4 1 4 47.23 1.17 1.9243 12 0 0 2 47.78 2.98 1.9034 6 4 0 4 48.02 1.09 1.8946 2 4 3 4 49.98 1.25 1.8250 -3 3 6 4 54.30 1.26 1.6894 10 2 3 4 54.44 1.83 1.6854 -7 1 8 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.