[Cr(C3H10N2)2F(H2O)][Cr(C3H10N2)2F(OH)](ClO4)3 Marsh R E, Herbstein F H Acta Crystallographica B44 (1988) 77-88 More space-group changes _database_code_amcsd 0009821 CELL PARAMETERS: 10.7100 9.0470 8.7850 111.250 100.440 86.600 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 780.180 Density (g/cm3): 1.550 MAX. ABS. INTENSITY / VOLUME**2: 4.573252944 RIR: 0.960 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.40 12.20 10.5324 1 0 0 2 10.49 9.24 8.4317 0 1 0 2 10.97 93.34 8.0661 0 0 1 2 12.17 7.50 7.2737 0 -1 1 2 12.63 1.68 7.0112 -1 0 1 2 13.41 14.74 6.6047 -1 1 0 2 13.50 6.88 6.5601 1 1 0 2 13.73 4.83 6.4508 -1 -1 1 2 14.94 48.72 5.9312 1 0 1 2 15.80 14.96 5.6077 1 -1 1 2 16.84 2.65 5.2662 2 0 0 2 17.73 7.97 5.0018 0 1 1 2 18.47 1.70 4.8032 -2 0 1 2 18.78 41.33 4.7252 -1 1 1 2 19.28 100.00 4.6034 -2 -1 1 2 19.81 69.88 4.4806 -2 1 0 2 19.94 18.55 4.4527 2 1 0 2 19.97 69.61 4.4471 0 -2 1 2 20.48 22.31 4.3362 1 1 1 2 20.73 5.06 4.2845 0 -1 2 2 20.94 34.43 4.2423 -1 -1 2 2 22.04 1.01 4.0331 0 0 2 2 22.21 5.94 4.0028 -1 0 2 2 22.27 47.51 3.9927 2 -1 1 2 22.37 1.91 3.9744 1 -2 1 2 22.66 9.10 3.9234 -1 2 0 2 22.77 29.50 3.9046 1 2 0 2 23.13 5.10 3.8452 -2 1 1 2 23.78 14.12 3.7420 1 -1 2 2 24.48 9.58 3.6369 0 -2 2 2 24.96 11.15 3.5674 1 0 2 2 25.06 5.87 3.5541 -2 -2 1 2 25.37 5.63 3.5108 3 0 0 2 25.41 2.90 3.5056 -2 0 2 2 25.88 2.66 3.4426 -3 0 1 2 27.84 21.72 3.2044 -1 1 2 2 29.08 12.98 3.0704 1 2 1 2 29.13 1.58 3.0659 2 -1 2 2 29.42 6.55 3.0358 -3 1 1 2 29.44 6.46 3.0342 3 0 1 2 29.68 5.36 3.0102 0 -3 1 2 29.86 2.57 2.9923 3 -1 1 2 29.88 2.45 2.9904 -3 -1 2 2 30.69 28.18 2.9131 -1 -1 3 2 30.76 4.12 2.9067 -3 0 2 2 31.05 1.41 2.8806 -3 -2 1 2 31.37 4.44 2.8520 1 -3 1 2 31.62 3.91 2.8300 0 -3 2 2 31.84 1.61 2.8106 0 3 0 2 32.65 1.34 2.7429 -2 -1 3 2 32.74 3.90 2.7349 3 1 1 2 32.93 12.25 2.7202 -1 3 0 2 32.94 4.12 2.7195 -1 0 3 2 33.04 7.79 2.7108 1 3 0 2 33.44 1.43 2.6796 -2 -3 1 2 33.95 1.40 2.6404 -4 0 1 2 34.00 6.34 2.6369 -2 -2 3 2 34.05 13.67 2.6331 4 0 0 2 34.23 2.58 2.6198 -2 -3 2 2 35.01 1.14 2.5632 1 -2 3 2 35.10 1.70 2.5563 -3 1 2 2 35.65 3.77 2.5184 -4 1 0 2 35.85 4.16 2.5048 3 -1 2 2 35.98 2.92 2.4961 -1 2 2 2 36.61 2.01 2.4543 -3 -1 3 2 36.77 1.09 2.4440 -4 1 1 2 37.47 2.18 2.4003 0 3 1 2 37.86 2.45 2.3764 -3 -2 3 2 37.97 1.69 2.3697 -1 3 1 2 38.04 4.36 2.3658 4 -1 1 2 38.09 1.15 2.3626 -2 2 2 2 38.17 1.50 2.3578 -4 -2 1 2 38.52 6.01 2.3371 -3 0 3 2 38.62 1.78 2.3313 0 1 3 2 38.96 2.32 2.3119 1 3 1 2 39.14 1.70 2.3017 -4 -2 2 2 40.19 1.39 2.2437 2 0 3 2 40.73 1.53 2.2150 -1 -4 2 2 40.74 13.25 2.2147 -1 -4 1 2 41.29 2.15 2.1867 3 3 0 2 41.35 6.92 2.1837 4 -2 1 2 41.46 2.89 2.1778 -1 -1 4 2 41.49 3.07 2.1767 -1 -2 4 2 42.11 1.80 2.1459 -4 -1 3 2 43.44 2.18 2.0833 4 -1 2 2 43.74 5.35 2.0697 -1 4 0 2 43.86 1.57 2.0642 1 4 0 2 44.26 2.49 2.0465 -1 0 4 2 44.32 1.33 2.0437 -1 -3 4 2 44.40 1.44 2.0404 -5 -1 2 2 44.49 2.96 2.0363 2 -4 1 2 44.66 1.11 2.0292 1 -1 4 2 44.83 1.09 2.0219 2 1 3 2 45.31 5.42 2.0014 -2 0 4 2 45.42 1.66 1.9970 -2 -3 4 2 45.44 2.40 1.9962 -3 -1 4 2 45.47 1.65 1.9949 0 3 2 2 45.49 4.79 1.9941 -3 -2 4 2 45.90 1.79 1.9771 3 0 3 2 46.38 4.09 1.9576 5 0 1 2 46.39 1.21 1.9573 -3 -4 2 2 47.13 4.10 1.9281 -2 2 3 2 47.58 2.16 1.9111 4 1 2 2 48.44 2.29 1.8791 5 2 0 2 48.71 1.13 1.8692 3 -3 3 2 48.72 1.82 1.8689 -5 -1 3 2 49.03 2.87 1.8580 3 -4 1 2 50.61 1.16 1.8036 -2 -4 4 2 50.64 1.39 1.8025 0 -5 2 2 51.09 1.39 1.7877 4 -1 3 2 51.72 2.16 1.7675 -1 -5 1 2 51.72 2.29 1.7675 -6 -1 1 2 52.06 2.43 1.7566 1 -5 2 2 52.34 3.84 1.7481 5 0 2 2 53.23 3.05 1.7209 -6 1 0 2 53.41 1.25 1.7155 5 -2 2 2 53.41 2.35 1.7154 5 2 1 2 53.88 2.05 1.7017 -2 -5 3 2 53.98 2.19 1.6986 3 -2 4 2 55.08 1.10 1.6673 0 3 3 2 55.66 1.29 1.6513 6 -1 1 2 55.68 1.13 1.6507 -3 -5 2 2 56.00 1.13 1.6422 0 4 2 2 56.22 1.34 1.6363 -6 -1 3 2 56.74 1.78 1.6224 -2 0 5 2 57.27 1.62 1.6086 0 2 4 2 57.52 1.10 1.6022 -2 2 4 2 57.73 3.58 1.5969 -2 -5 4 2 58.66 1.38 1.5739 -6 -3 2 2 58.78 1.52 1.5709 3 -5 1 2 58.84 1.44 1.5694 5 -1 3 2 58.89 1.02 1.5683 -5 -4 1 2 59.62 1.01 1.5508 5 -2 3 2 59.92 1.12 1.5436 0 5 1 2 61.77 1.06 1.5019 -1 -6 2 2 62.00 1.05 1.4968 -2 1 5 2 62.02 1.11 1.4964 -7 0 2 2 62.07 1.01 1.4952 -5 4 0 2 62.57 1.08 1.4846 2 -5 4 2 63.78 1.07 1.4593 -4 -5 4 2 65.71 2.09 1.4211 -7 0 3 2 66.03 1.18 1.4150 0 -6 4 2 66.19 1.24 1.4118 -2 3 4 2 66.89 1.25 1.3988 7 1 1 2 69.31 1.33 1.3558 3 -6 2 2 70.18 1.88 1.3411 5 -5 1 2 73.09 1.04 1.2947 4 2 4 2 75.81 1.33 1.2548 6 4 1 2 76.28 1.05 1.2483 -4 -6 5 2 77.16 1.16 1.2362 -3 -7 3 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.