Xanthiosite Barbier J, Frampton C Acta Crystallographica B47 (1991) 457-462 Structures of orthorhombic and monoclinic Ni3(AsO4)2 Locality: synthetic Note: AnisoU's taken from ICSD _database_code_amcsd 0009846 CELL PARAMETERS: 5.7640 9.5590 10.1940 90.000 92.950 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 560.925 Density (g/cm3): 5.374 MAX. ABS. INTENSITY / VOLUME**2: 38.00252369 RIR: 2.302 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 15.39 5.62 5.7564 1 0 0 2 19.76 2.43 4.4929 0 1 2 4 20.35 13.73 4.3632 1 1 1 4 20.53 11.42 4.3264 0 2 1 4 22.72 7.02 3.9145 -1 0 2 2 23.92 5.20 3.7194 1 0 2 2 24.20 14.59 3.6772 1 2 0 4 25.57 7.65 3.4843 0 2 2 4 25.70 40.29 3.4663 1 1 2 4 26.03 6.08 3.4227 1 2 1 4 27.90 11.40 3.1980 0 1 3 4 29.37 9.69 3.0409 0 3 1 4 29.50 4.22 3.0284 -1 2 2 4 30.45 4.85 2.9353 1 2 2 4 32.11 4.92 2.7877 1 3 0 4 32.35 11.11 2.7670 0 2 3 4 32.49 27.35 2.7560 2 1 0 4 32.69 37.40 2.7397 1 1 3 4 33.10 9.92 2.7060 -1 3 1 4 33.17 4.09 2.7008 0 3 2 4 33.26 34.46 2.6939 -2 1 1 4 33.54 39.73 2.6719 1 3 1 4 34.12 25.20 2.6278 2 1 1 4 35.40 100.00 2.5357 -1 2 3 4 36.29 3.36 2.4752 -2 1 2 4 36.36 2.12 2.4712 -1 3 2 4 36.53 1.14 2.4594 0 1 4 4 37.14 1.80 2.4209 -2 2 1 4 37.16 8.41 2.4198 1 3 2 4 37.64 5.81 2.3898 0 4 0 2 37.88 1.73 2.3750 2 1 2 4 37.91 3.16 2.3734 -1 0 4 2 37.92 1.98 2.3725 2 2 1 4 38.70 1.03 2.3265 0 4 1 4 39.11 2.11 2.3034 -1 1 4 4 40.14 2.04 2.2465 0 2 4 4 40.60 10.82 2.2221 1 1 4 4 40.89 4.57 2.2071 1 4 0 4 41.70 2.02 2.1659 -1 4 1 4 41.76 2.90 2.1632 0 4 2 4 42.06 6.24 2.1482 1 4 1 4 42.32 12.01 2.1358 2 3 0 4 42.47 4.37 2.1282 1 3 3 4 42.53 1.29 2.1257 -1 2 4 4 42.93 5.48 2.1066 -2 3 1 4 43.30 1.16 2.0895 2 1 3 4 43.63 3.13 2.0745 2 3 1 4 44.41 2.26 2.0397 -1 4 2 4 45.09 1.48 2.0105 1 4 2 4 45.42 4.39 1.9969 -2 3 2 4 45.55 7.19 1.9914 0 1 5 4 45.62 3.81 1.9886 0 3 4 4 46.47 1.23 1.9542 2 2 3 4 46.48 4.86 1.9539 0 4 3 4 46.75 4.05 1.9432 2 3 2 4 47.38 1.43 1.9188 3 0 0 2 47.41 1.53 1.9175 -2 1 4 4 47.56 1.12 1.9120 -1 1 5 4 48.60 1.03 1.8732 0 2 5 4 49.06 7.78 1.8567 1 3 4 4 49.16 1.55 1.8534 1 1 5 4 50.13 2.62 1.8198 -2 4 1 4 50.29 1.77 1.8144 1 5 0 4 50.75 2.56 1.7990 2 4 1 4 50.89 2.04 1.7943 -3 1 2 4 51.03 2.78 1.7897 0 5 2 4 51.29 2.15 1.7812 1 5 1 4 51.31 1.05 1.7807 3 2 0 4 51.69 1.39 1.7684 -3 2 1 4 52.05 1.51 1.7570 1 2 5 4 52.53 1.13 1.7421 0 4 4 4 52.72 1.31 1.7363 3 1 2 4 53.55 1.59 1.7114 2 4 2 4 53.72 1.01 1.7064 -3 2 2 4 54.57 7.43 1.6817 -3 1 3 4 54.96 4.36 1.6706 0 1 6 4 55.48 1.06 1.6563 3 2 2 4 55.66 1.49 1.6514 1 4 4 4 55.68 2.91 1.6507 -1 0 6 2 56.10 1.82 1.6393 -2 4 3 4 56.30 5.40 1.6341 -3 3 1 4 56.64 8.00 1.6251 1 3 5 4 57.82 2.69 1.5948 2 4 3 4 58.22 1.72 1.5848 -3 3 2 4 58.65 2.64 1.5740 0 6 1 4 59.62 5.02 1.5507 -3 1 4 4 59.79 21.02 1.5467 3 2 3 4 60.41 14.49 1.5323 -2 5 2 4 60.57 10.62 1.5286 0 5 4 4 60.89 3.23 1.5214 -1 6 1 4 61.33 1.15 1.5115 -1 4 5 4 61.51 10.90 1.5077 2 5 2 4 61.60 1.15 1.5056 -3 3 3 4 61.96 3.39 1.4976 0 3 6 4 62.03 3.72 1.4962 3 4 0 4 62.05 16.60 1.4957 -2 0 6 2 62.37 1.18 1.4889 -3 4 1 4 62.37 3.48 1.4888 -1 5 4 4 62.69 1.80 1.4820 1 4 5 4 63.47 1.25 1.4657 -1 3 6 4 63.53 1.46 1.4645 1 6 2 4 64.63 3.99 1.4421 0 6 3 4 64.78 16.04 1.4391 4 0 0 2 64.85 5.10 1.4378 0 1 7 4 65.25 15.63 1.4298 2 0 6 2 66.32 2.96 1.4094 -3 3 4 4 66.49 3.64 1.4062 -1 6 3 4 68.62 1.84 1.3676 -2 5 4 4 69.17 2.42 1.3582 -1 4 6 4 69.47 3.04 1.3530 -2 6 2 4 69.62 1.95 1.3504 0 6 4 4 70.49 2.32 1.3359 2 6 2 4 70.66 1.01 1.3330 2 5 4 4 71.28 1.33 1.3231 0 3 7 4 71.75 4.55 1.3155 1 7 1 4 72.19 1.44 1.3086 -4 3 1 4 72.26 3.78 1.3075 -3 3 5 4 72.30 1.58 1.3068 1 6 4 4 72.56 1.61 1.3028 -1 3 7 4 72.79 1.83 1.2993 -4 2 3 4 74.19 1.67 1.2782 2 6 3 4 74.31 1.02 1.2765 1 3 7 4 74.90 1.25 1.2679 -2 4 6 4 77.41 1.65 1.2328 4 4 0 4 77.67 1.18 1.2294 -3 4 5 4 77.85 1.88 1.2270 2 4 6 4 77.94 1.08 1.2257 3 6 0 4 78.07 1.95 1.2241 -2 3 7 4 78.98 1.19 1.2122 3 6 1 4 80.36 1.12 1.1949 0 8 0 2 81.97 1.12 1.1755 -4 4 3 4 82.97 1.78 1.1638 -2 6 5 4 83.02 1.11 1.1633 0 8 2 4 84.84 1.44 1.1428 -1 8 2 4 85.02 1.71 1.1409 3 6 3 4 85.15 1.44 1.1395 4 1 5 4 85.38 1.31 1.1370 2 6 5 4 87.65 1.39 1.1133 -1 1 9 4 88.01 1.65 1.1096 -1 8 3 4 88.02 1.57 1.1096 -3 7 1 4 88.31 2.26 1.1067 1 7 5 4 88.66 1.46 1.1033 5 1 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.